#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:28:26 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1124 $ #$URL: svn://172.16.1.111/rod/cif/1/00/05/1000553.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000553 loop_ _publ_author_name 'Burns, P. C.' 'Smith, J. V.' 'Steele, I. M.' _publ_section_title ; Arizona porphyry copper/hydrothermal deposits I. The structure of chenevixite and luetheite Note: Luetheite-chenevixite series Locality: Humboldt mine, Patagonia, Arizona ; _journal_name_full 'Mineralogical Magazine' _journal_page_first 25 _journal_page_last 30 _journal_paper_doi 10.1180/002646100549102 _journal_volume 64 _journal_year 2000 _chemical_compound_source R100177 _chemical_formula_sum 'Al0.635 As Cu Fe0.365 H2 O6' _chemical_name_mineral Luetheite _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb (1/2*x,y,-1/2*x+z)' _symmetry_space_group_name_H-M 'B 1 21 1' _cell_angle_alpha 90 _cell_angle_beta 89.99 _cell_angle_gamma 90 _cell_length_a 5.7012 _cell_length_b 5.1801 _cell_length_c 29.265 _cell_volume 864.277 _exptl_crystal_density_diffrn 4.211 _cod_original_formula_sum 'Cu (Al.635 Fe.365) As O6 H2' _cod_database_code 9009514 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R100177.rod _rod_data_source.block 3500000 _rod_database.code 1000553 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9009514 COD http://www.crystallography.net/cod/9009514.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 104.5868 0.0000000E+00 105.0690 1.972328 105.5511 4.322319 106.0332 6.212738 106.5153 6.809631 106.9974 7.339890 107.4795 5.426918 107.9617 3.231712 108.4438 0.8975180 108.9259 0.4876480 109.4080 0.3849870 109.8901 2.065987 110.3722 2.719116 110.8544 2.021606 111.3365 1.377716 111.8186 2.064915 112.3007 3.519485 112.7828 4.517895 113.2649 4.468895 113.7471 3.380646 114.2292 2.897655 114.7113 3.865200 115.1934 4.580715 115.6755 4.904854 116.1576 4.911812 116.6397 4.708595 117.1219 4.437725 117.6040 4.141369 118.0861 3.620544 118.5682 2.351662 119.0503 1.170799 119.5324 0.7506980 120.0146 1.196156 120.4967 1.953880 120.9788 2.297115 121.4609 1.755901 121.9430 1.465729 122.4251 1.809345 122.9073 2.331303 123.3894 2.341736 123.8715 1.512417 124.3536 0.3696670 124.8357 0.3457680 125.3178 1.878536 125.8000 3.268303 126.2821 3.805634 126.7642 3.653252 127.2463 3.428169 127.7284 3.442863 128.2105 3.589619 128.6927 3.889828 129.1748 4.555904 129.6569 5.042664 130.1390 5.413124 130.6211 5.620319 131.1032 5.901749 131.5854 6.580608 132.0675 7.316376 132.5496 7.923981 133.0317 8.464176 133.5138 8.855747 133.9959 8.690655 134.4781 7.338837 134.9602 6.393871 135.4423 6.636345 135.9244 7.441242 136.4065 7.957722 136.8886 7.618324 137.3708 6.514160 137.8529 5.852203 138.3350 6.321167 138.8171 6.587627 139.2992 6.165314 139.7813 5.262127 140.2635 4.382225 140.7456 3.953720 141.2277 4.026100 141.7098 4.173676 142.1919 4.508987 142.6740 4.811272 143.1561 4.878601 143.6383 4.731350 144.1204 4.649540 144.6025 4.972942 145.0846 5.794643 145.5667 6.354553 146.0488 6.572384 146.5310 6.537594 147.0131 6.287983 147.4952 5.798946 147.9773 5.251575 148.4594 4.947311 148.9415 4.834602 149.4237 4.484268 149.9058 3.485165 150.3879 2.107811 150.8700 1.168770 151.3521 1.030861 151.8342 1.042160 152.3164 0.5510640 152.7985 0.3700290 153.2806 1.184406 153.7627 1.393772 154.2448 0.9844550 154.7269 0.7135890 155.2091 0.8477440 155.6912 1.024372 156.1733 1.073490 156.6554 0.9780620 157.1375 0.8078380 157.6196 0.6499670 158.1018 0.5318570 158.5839 0.3461040 159.0660 9.6938998E-02 159.5481 0.2167660 160.0302 0.6635510 160.5123 1.236366 160.9945 1.798382 161.4766 2.096371 161.9587 1.919868 162.4408 1.944118 162.9229 1.883186 163.4050 1.891186 163.8871 2.180477 164.3693 2.825581 164.8514 3.624489 165.3335 4.098072 165.8156 3.917152 166.2977 3.855778 166.7798 4.037182 167.2620 4.429024 167.7441 4.833584 168.2262 5.173836 168.7083 5.447132 169.1904 5.625740 169.6725 5.548859 170.1547 5.680099 170.6368 6.348309 171.1189 7.406467 171.6010 8.366825 172.0831 9.018631 172.5652 9.429165 173.0474 9.778267 173.5295 9.999496 174.0116 10.27850 174.4937 10.78131 174.9758 11.50761 175.4579 12.26622 175.9401 13.03535 176.4222 13.76013 176.9043 14.38411 177.3864 14.91420 177.8685 15.33485 178.3506 15.55749 178.8328 15.48812 179.3149 15.53813 179.7970 15.93298 180.2791 16.47660 180.7612 17.02201 181.2433 17.52134 181.7255 17.96013 182.2076 18.27169 182.6897 18.26932 183.1718 18.58112 183.6539 19.69821 184.1360 20.97173 184.6181 21.68048 185.1003 21.45512 185.5824 20.57631 186.0645 20.04205 186.5466 20.16957 187.0287 20.28289 187.5108 20.21793 187.9930 20.10688 188.4751 20.10035 188.9572 20.27886 189.4393 20.65134 189.9214 21.27261 190.4035 22.70491 190.8857 23.76217 191.3678 23.94749 191.8499 23.62000 192.3320 23.42931 192.8141 23.79575 193.2962 24.61915 193.7784 25.07893 194.2605 24.94210 194.7426 24.78193 195.2247 24.72453 195.7068 24.78888 196.1889 25.03714 196.6711 25.56932 197.1532 26.28421 197.6353 26.69530 198.1174 26.61308 198.5995 26.43847 199.0816 26.40020 199.5638 26.47723 200.0459 26.50195 200.5280 26.27868 201.0101 25.97205 201.4922 26.04744 201.9743 26.97935 202.4565 27.83888 202.9386 27.65526 203.4207 26.39583 203.9028 25.23930 204.3849 24.97907 204.8670 25.16758 205.3492 25.15297 205.8313 24.70486 206.3134 24.17418 206.7955 24.14115 207.2776 24.78934 207.7597 25.07236 208.2419 23.97521 208.7240 22.44997 209.2061 21.44689 209.6882 21.34314 210.1703 21.72958 210.6524 21.89264 211.1346 21.72868 211.6167 21.62991 212.0988 21.84853 212.5809 22.18150 213.0630 22.38586 213.5451 22.33107 214.0273 22.13909 214.5094 22.23002 214.9915 22.96808 215.4736 23.33956 215.9557 22.75014 216.4378 21.93079 216.9200 21.67728 217.4021 22.34815 217.8842 23.53728 218.3663 24.16756 218.8484 23.73574 219.3305 23.42014 219.8127 23.45331 220.2948 23.62194 220.7769 23.68959 221.2590 23.54950 221.7411 23.27748 222.2232 23.09318 222.7054 23.12623 223.1875 23.09078 223.6696 23.16888 224.1517 23.10059 224.6338 22.51108 225.1159 21.22841 225.5980 19.50916 226.0802 18.09390 226.5623 17.45076 227.0444 16.56258 227.5265 15.09287 228.0086 13.41143 228.4907 12.02476 228.9729 11.14902 229.4550 10.61192 229.9371 9.985527 230.4192 9.102997 230.9013 8.391884 231.3834 8.060478 231.8656 7.910892 232.3477 7.622581 232.8298 7.053532 233.3119 6.373173 233.7940 5.971882 234.2761 5.933178 234.7583 5.891586 235.2404 5.680153 235.7225 5.418377 236.2046 5.360302 236.6867 5.643436 237.1688 6.022186 237.6510 6.025784 238.1331 5.614670 238.6152 5.220772 239.0973 4.937679 239.5794 4.775669 240.0615 4.792072 240.5437 5.058380 241.0258 5.391895 241.5079 5.508801 241.9900 5.408703 242.4721 5.396465 242.9542 5.606293 243.4364 5.999462 243.9185 6.516834 244.4006 7.231728 244.8827 7.907772 245.3648 8.342190 245.8469 8.553791 246.3290 8.568790 246.8112 8.379719 247.2933 8.003181 247.7754 7.397182 248.2575 6.296501 248.7396 5.428135 249.2217 5.585266 249.7039 6.477730 250.1860 7.117126 250.6681 6.735313 251.1502 5.635002 251.6323 4.988255 252.1144 5.136730 252.5966 5.268314 253.0787 4.850132 253.5608 4.056866 254.0429 3.265678 254.5250 2.639175 255.0071 2.180622 255.4893 1.914879 255.9714 1.918423 256.4535 2.010456 256.9356 2.131557 257.4177 2.266361 257.8998 2.402351 258.3820 2.567665 258.8641 2.712322 259.3462 2.615692 259.8283 2.015102 260.3104 1.615856 260.7925 1.917282 261.2747 2.448669 261.7568 2.541180 262.2389 1.790157 262.7210 0.5309300 263.2031 0.2570760 263.6852 0.3374370 264.1674 0.3138960 264.6495 0.3236160 265.1316 0.3267560 265.6137 0.2692410 266.0958 0.1249080 266.5779 6.4960003E-02 267.0601 0.2122880 267.5422 0.3546220 268.0243 0.3701170 268.5064 0.2091140 268.9885 4.3892000E-02 269.4706 0.3924870 269.9528 0.8258550 270.4349 1.173538 270.9170 1.019516 271.3991 0.2058490 271.8812 0.7795680 272.3633 0.1695670 272.8455 0.7544560 273.3276 1.445072 273.8097 1.727543 274.2918 1.624149 274.7739 1.072155 275.2560 0.4149630 275.7382 1.288857 276.2202 1.273075 276.7024 0.9918330 277.1845 0.7134510 277.6666 0.5410190 278.1487 0.5570950 278.6308 0.8700330 279.1129 1.531265 279.5951 2.331398 280.0772 3.626022 280.5593 4.738308 281.0414 5.166531 281.5235 5.008400 282.0056 4.803303 282.4878 5.106594 282.9699 6.047981 283.4520 6.553791 283.9341 6.116428 284.4162 5.801300 284.8983 6.096027 285.3805 6.892735 285.8626 7.820232 286.3447 8.608646 286.8268 9.256721 287.3089 9.839916 287.7910 10.34739 288.2732 10.80785 288.7553 11.14710 289.2374 11.44714 289.7195 11.88765 290.2016 12.59958 290.6837 13.49165 291.1659 14.05902 291.6480 14.07670 292.1301 14.03146 292.6122 14.11192 293.0943 14.14714 293.5764 13.83945 294.0586 13.04050 294.5407 11.94957 295.0228 11.10279 295.5049 10.69347 295.9870 10.30832 296.4691 9.894577 296.9513 9.515247 297.4334 9.278473 297.9155 9.213634 298.3976 9.186489 298.8797 8.960182 299.3618 8.305965 299.8440 7.890316 300.3261 8.009857 300.8082 8.180866 301.2903 7.857414 301.7724 7.002392 302.2545 6.219463 302.7367 6.301620 303.2188 7.668957 303.7009 8.213783 304.1830 7.168209 304.6651 6.006367 305.1472 5.751431 305.6294 6.348278 306.1115 7.010647 306.5936 7.039394 307.0757 6.383938 307.5578 6.073811 308.0399 6.436340 308.5221 6.754761 309.0042 6.642971 309.4863 6.221214 309.9684 5.852890 310.4505 5.782249 310.9326 5.953876 311.4148 5.982235 311.8969 5.713654 312.3790 5.502758 312.8611 5.572826 313.3432 5.731289 313.8253 5.566185 314.3075 4.856503 314.7896 3.949329 315.2717 3.765999 315.7538 5.355648 316.2359 6.148247 316.7180 5.319492 317.2001 3.868488 317.6823 2.848209 318.1644 2.564518 318.6465 2.736053 319.1286 2.975918 319.6107 3.335793 320.0928 3.412582 320.5750 3.113766 321.0571 2.651424 321.5392 2.060364 322.0213 1.438831 322.5034 1.075584 322.9855 1.281651 323.4677 2.148861 323.9498 2.948792 324.4319 3.684505 324.9140 4.309349 325.3961 4.849834 325.8782 5.261314 326.3604 5.438919 326.8425 5.306328 327.3246 4.941551 327.8067 4.782211 328.2888 4.787785 328.7709 4.895050 329.2531 5.112495 329.7352 5.455643 330.2173 6.093094 330.6994 7.107174 331.1815 8.194454 331.6636 8.553207 332.1458 7.078514 332.6279 6.300346 333.1100 6.842758 333.5921 7.826157 334.0742 8.454906 334.5563 8.496468 335.0385 8.192524 335.5206 7.864922 336.0027 7.423508 336.4848 7.216343 336.9669 7.299370 337.4490 7.540531 337.9312 7.929649 338.4133 8.419636 338.8954 8.860790 339.3775 9.082859 339.8596 9.042797 340.3417 9.340092 340.8239 10.43475 341.3060 11.34408 341.7881 11.58186 342.2702 11.37275 342.7523 11.18517 343.2344 11.30115 343.7166 11.68592 344.1987 12.17257 344.6808 12.90210 345.1629 13.57893 345.6450 14.13436 346.1271 14.63721 346.6093 15.18340 347.0914 15.80113 347.5735 16.42284 348.0556 16.90812 348.5377 17.20182 349.0198 17.44946 349.5020 17.71884 349.9841 17.90303 350.4662 17.97605 350.9483 17.90685 351.4304 17.61209 351.9125 16.96873 352.3947 15.91673 352.8768 14.92442 353.3589 13.62256 353.8410 12.74441 354.3231 12.77265 354.8052 13.43073 355.2874 14.17190 355.7695 14.66301 356.2516 14.89402 356.7337 14.78255 357.2158 13.82649 357.6979 13.21870 358.1800 13.51857 358.6621 14.10628 359.1443 14.24216 359.6264 13.64499 360.1085 12.73222 360.5906 12.32435 361.0727 12.78021 361.5548 12.79210 362.0370 11.87589 362.5191 10.77615 363.0012 9.936562 363.4833 9.392403 363.9654 8.925114 364.4475 8.269958 364.9297 7.402355 365.4118 6.778940 365.8939 6.794821 366.3760 6.616665 366.8581 5.568655 367.3402 4.099760 367.8224 3.168230 368.3045 3.495043 368.7866 4.615297 369.2687 5.156723 369.7508 4.951992 370.2329 4.509554 370.7151 3.794350 371.1972 3.045311 371.6793 2.494904 372.1614 2.221561 372.6435 2.105125 373.1256 2.052429 373.6078 2.074783 374.0899 2.006422 374.5720 1.831087 375.0541 1.522762 375.5362 0.9116130 376.0183 5.8568999E-02 376.5005 0.5249820 376.9826 0.2626300 377.4647 0.5720200 377.9468 0.9480190 378.4289 0.6962870 378.9110 0.2179850 379.3932 0.3355690 379.8753 0.9086880 380.3574 1.393381 380.8395 1.807844 381.3216 2.072395 381.8037 2.045397 382.2859 1.722534 382.7680 1.310513 383.2501 0.7313120 383.7322 0.2390060 384.2143 0.2801270 384.6964 1.054371 385.1786 1.680922 385.6607 1.501284 386.1428 0.7826310 386.6249 0.2309190 387.1070 2.3031000E-02 387.5891 2.1470999E-02 388.0713 3.7636001E-02 388.5534 3.0634001E-02 389.0355 0.1721820 389.5176 0.6961940 389.9997 1.261036 390.4818 1.504309 390.9640 1.418222 391.4461 1.207262 391.9282 0.9091430 392.4103 0.6204410 392.8924 0.7773090 393.3745 1.994278 393.8567 2.946798 394.3388 2.951826 394.8209 2.344021 395.3030 1.689854 395.7851 1.164152 396.2672 0.8679830 396.7494 1.012239 397.2315 1.827187 397.7136 2.549313 398.1957 3.119812 398.6778 3.609241 399.1599 4.105404 399.6420 4.600258 400.1241 4.971447 400.6063 5.074604 401.0884 4.894508 401.5705 4.996086 402.0526 5.691730 402.5347 6.282719 403.0168 6.433203 403.4990 6.363207 403.9811 6.467146 404.4632 6.936863 404.9453 7.596001 405.4274 8.014050 405.9095 8.056524 406.3917 8.063931 406.8738 7.803087 407.3559 7.688299 407.8380 8.220499 408.3201 9.323694 408.8022 10.31467 409.2844 10.41969 409.7665 9.555376 410.2486 9.138058 410.7307 9.649508 411.2128 10.10585 411.6949 10.05354 412.1771 9.787714 412.6592 9.847473 413.1413 10.54966 413.6234 11.54490 414.1055 12.01873 414.5876 11.73903 415.0698 11.65242 415.5519 12.08589 416.0340 12.72271 416.5161 13.40301 416.9982 14.09886 417.4803 14.77364 417.9625 15.38594 418.4446 15.94527 418.9267 16.53068 419.4088 17.13260 419.8909 17.78493 420.3730 18.56701 420.8552 19.40591 421.3373 20.13135 421.8194 20.59173 422.3015 21.01148 422.7836 21.64408 423.2657 22.48768 423.7479 23.46873 424.2300 24.57386 424.7121 25.79598 425.1942 27.20404 425.6763 28.89466 426.1584 30.27293 426.6406 30.90270 427.1227 31.10774 427.6048 31.37730 428.0869 31.78676 428.5690 32.36731 429.0511 33.21064 429.5333 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