#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:28:51 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1131 $
#$URL: svn://172.16.1.111/rod/cif/1/00/05/1000556.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000556
loop_
_publ_author_name
'Atencio, D.'
'Roberts, A. C.'
'Cooper, M. A.'
'Menezes, L. A. D.'
'Coutinho, J. M. V.'
'Stirling, J. A. R.'
'Venance, K. E.'
'Ball, N. A.'
'Moffatt, E.'
'Chaves, M. L. S. C.'
'Brandao, P. R. G.'
'Romano, A. W.'
_publ_section_title
;
 Carlosbarbosaite, ideally (UO2)2Nb2O6(OH)2*2H2O, a new hydrated uranyl
 niobate mineral with tunnels from Jaguaracu, Minas Gerais, Brazil:
 description and crystal structure
;
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              75
_journal_page_last               90
_journal_paper_doi               10.1180/minmag.2012.076.1.75
_journal_volume                  76
_journal_year                    2012
_chemical_compound_source        'Jaguaracu, Minas Gerais, Brazil'
_chemical_formula_sum
'Al0.1 Ca0.28 Ce0.02 Fe0.1 H6 Nb0.8 Nd0.02 O14 Si0.26 Ta0.52 Ti0.22 U1.44'
_chemical_name_mineral           Carlosbarbosaite
_space_group_IT_number           63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   14.150
_cell_length_b                   10.395
_cell_length_c                   7.529
_cell_volume                     1107.435
_exptl_crystal_density_diffrn    4.704
_cod_original_formula_sum
'U1.44 (Nb.8 Ta.52 Si.26 Ti.22 Al.1 Fe.1) Ca.28 Nd.02 Ce.02 O14 H6'
_cod_database_code               9015592
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110162.rod
_rod_data_source.block           3500000
_rod_database.code               1000556
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9015592 COD http://www.crystallography.net/cod/9015592.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
146.6430 0.0000000E+00
147.1251 0.1033940
147.6072 0.1598510
148.0893 0.1601560
148.5714 6.4331003E-02
149.0535 2.4410000E-03
149.5357 4.4739000E-02
150.0178 0.2550660
150.4999 0.9562990
150.9820 1.162354
151.4641 1.164978
151.9462 1.025879
152.4284 0.8154910
152.9105 0.5255130
153.3926 0.1593630
153.8747 0.1810910
154.3568 0.2360230
154.8389 0.2858280
155.3211 0.7717290
155.8032 1.270386
156.2853 1.697937
156.7674 1.922607
157.2495 1.867676
157.7316 1.614807
158.2138 1.515442
158.6959 1.498108
159.1780 1.671448
159.6601 2.104370
160.1422 2.751221
160.6243 3.594177
161.1065 4.756775
161.5886 6.005981
162.0707 6.421387
162.5528 5.100647
163.0349 3.874390
163.5170 3.970093
163.9991 5.270996
164.4813 6.655334
164.9634 7.581726
165.4455 8.061707
165.9276 8.150330
166.4097 7.528503
166.8918 6.766846
167.3740 6.587036
167.8561 7.088928
168.3382 7.603455
168.8203 7.614136
169.3024 7.431335
169.7845 7.451050
170.2667 7.917542
170.7488 8.622681
171.2309 9.070618
171.7130 9.119873
172.1951 9.165466
172.6772 9.357727
173.1594 9.645752
173.6415 9.977417
174.1236 10.36615
174.6057 10.77356
175.0878 10.93451
175.5699 10.54132
176.0521 10.25146
176.5342 10.30817
177.0163 10.58972
177.4984 10.86841
177.9805 10.96838
178.4626 10.88696
178.9448 10.92200
179.4269 11.16260
179.9090 11.42847
180.3911 11.63953
180.8732 11.82471
181.3553 12.20526
181.8375 12.99133
182.3196 14.08862
182.8017 14.50464
183.2838 13.53979
183.7659 12.84485
184.2480 13.29401
184.7301 14.78955
185.2123 16.47174
185.6944 17.44965
186.1765 17.49817
186.6586 17.67212
187.1407 18.41705
187.6228 19.48956
188.1050 20.71680
188.5871 22.36493
189.0692 23.83478
189.5513 24.43561
190.0334 24.30243
190.5155 23.96265
190.9977 23.06964
191.4798 22.17737
191.9619 22.12616
192.4440 23.17859
192.9261 24.18939
193.4082 23.55945
193.8904 21.84186
194.3725 20.80573
194.8546 21.66852
195.3367 23.46527
195.8188 24.19421
196.3009 23.34613
196.7831 22.18384
197.2652 21.54291
197.7473 21.31879
198.2294 21.31903
198.7115 21.47424
199.1936 21.77808
199.6758 22.24329
200.1579 23.08447
200.6400 23.77222
201.1221 24.15155
201.6042 24.19427
202.0863 23.83130
202.5685 22.85394
203.0506 21.30719
203.5327 20.00360
204.0148 18.76849
204.4969 18.14752
204.9790 18.52039
205.4612 19.54980
205.9433 20.46326
206.4254 20.60217
206.9075 19.92505
207.3896 19.25659
207.8717 18.61450
208.3539 17.96191
208.8360 17.27368
209.3181 16.56775
209.8002 15.90869
210.2823 15.39679
210.7644 15.10150
211.2466 14.37122
211.7287 12.75800
212.2108 11.16913
212.6929 9.975464
213.1750 9.142395
213.6571 8.476929
214.1393 7.848816
214.6214 7.321350
215.1035 6.315979
215.5856 4.141235
216.0677 2.202454
216.5498 1.330139
217.0320 1.426941
217.5141 1.767639
217.9962 1.722595
218.4783 1.240540
218.9604 0.6877440
219.4425 0.1691890
219.9247 0.9096070
220.4068 1.235352
220.8889 1.160950
221.3710 0.9346310
221.8531 0.7296750
222.3352 0.5552980
222.8174 0.5084840
223.2995 0.6907350
223.7816 0.9269410
224.2637 1.127319
224.7458 1.280518
225.2279 1.305969
225.7100 0.9843750
226.1922 0.4178470
226.6743 0.3655400
227.1564 1.572815
227.6385 2.898499
228.1206 3.147766
228.6027 2.217773
229.0849 1.105896
229.5670 0.6450810
230.0491 0.6780400
230.5312 0.5878300
231.0133 0.3667600
231.4954 0.1087650
231.9776 1.049988
232.4597 2.505737
232.9418 4.039917
233.4239 5.480103
233.9060 6.816650
234.3881 7.981750
234.8703 8.833008
235.3524 9.607788
235.8345 10.65552
236.3166 12.03638
236.7987 13.45520
237.2808 14.80273
237.7630 16.09265
238.2451 17.36383
238.7272 18.68646
239.2093 19.90942
239.6914 20.59406
240.1735 20.39453
240.6557 20.79926
241.1378 23.13763
241.6199 26.01880
242.1020 28.06085
242.5841 28.67993
243.0662 28.62543
243.5484 29.24658
244.0305 30.89886
244.5126 32.25525
244.9947 32.46204
245.4768 32.48438
245.9589 33.42731
246.4410 35.73456
246.9232 38.22894
247.4053 38.69873
247.8874 36.13220
248.3695 33.91199
248.8516 32.92505
249.3337 32.30298
249.8159 31.25360
250.2980 29.55591
250.7801 27.82904
251.2622 27.25549
251.7443 28.68347
252.2264 29.33606
252.7086 28.71680
253.1907 27.53314
253.6728 26.14056
254.1549 24.67993
254.6370 23.25635
255.1191 21.96088
255.6013 20.56110
256.0834 19.87970
256.5655 20.54236
257.0476 21.34778
257.5297 21.42377
258.0118 20.66046
258.4940 19.64276
258.9761 19.18585
259.4582 19.61957
259.9403 19.79169
260.4224 19.68640
260.9045 19.39709
261.3867 18.93164
261.8688 18.31830
262.3509 17.64996
262.8330 17.04462
263.3151 16.58002
263.7972 15.87317
264.2794 14.41919
264.7615 13.18945
265.2436 12.86469
265.7257 13.36682
266.2078 14.09778
266.6899 14.50244
267.1721 14.55896
267.6542 14.35992
268.1363 13.65369
268.6184 12.97394
269.1005 12.67627
269.5826 12.67633
270.0648 12.60315
270.5469 12.13446
271.0290 11.25586
271.5111 10.49542
271.9932 9.801819
272.4753 9.245422
272.9575 8.924683
273.4396 8.766052
273.9217 8.614929
274.4038 8.417358
274.8859 8.184814
275.3680 7.653564
275.8501 6.287292
276.3322 5.227234
276.8144 4.955017
277.2965 5.250366
277.7786 5.758789
278.2607 6.401489
278.7428 7.037048
279.2249 6.886414
279.7071 5.102356
280.1892 3.690613
280.6713 3.568237
281.1534 4.084412
281.6355 4.033813
282.1176 2.843994
282.5998 0.9967040
283.0819 0.2683720
283.5640 0.9257810
284.0461 1.121216
284.5282 0.3168330
285.0103 0.6699220
285.4925 0.5386350
285.9746 1.166138
286.4567 3.338440
286.9388 4.145752
287.4209 3.240906
287.9030 2.501282
288.3852 2.359131
288.8673 2.450012
289.3494 2.396362
289.8315 2.104736
290.3136 1.511292
290.7957 0.4152830
291.2779 1.288269
291.7600 2.474792
292.2421 2.696472
292.7242 2.538940
293.2063 2.428162
293.6884 2.430054
294.1706 2.773132
294.6527 3.851135
295.1348 5.659241
295.6169 6.869934
296.0990 6.895874
296.5811 6.701599
297.0633 7.016663
297.5454 7.853699
298.0275 8.881775
298.5096 9.924500
298.9917 10.96832
299.4738 11.95306
299.9560 12.77887
300.4381 13.63153
300.9202 14.63373
301.4023 15.76398
301.8844 16.94086
302.3665 18.15283
302.8487 19.36230
303.3308 20.44202
303.8129 21.13190
304.2950 22.11029
304.7771 23.92554
305.2592 26.27716
305.7414 28.39709
306.2235 29.99493
306.7056 31.22534
307.1877 32.37189
307.6698 33.49298
308.1519 34.39539
308.6341 34.66339
309.1162 34.74329
309.5983 35.50116
310.0804 37.23944
310.5625 39.32166
311.0446 40.94696
311.5268 42.13770
312.0089 43.09015
312.4910 43.64087
312.9731 44.06213
313.4552 44.75598
313.9373 45.79108
314.4195 46.76025
314.9016 47.31104
315.3837 47.43481
315.8658 47.30530
316.3479 46.35547
316.8300 45.56470
317.3121 46.08966
317.7943 47.84003
318.2764 49.26947
318.7585 49.24512
319.2406 48.03156
319.7227 47.19714
320.2048 46.97937
320.6870 46.88898
321.1691 46.79639
321.6512 46.64734
322.1333 46.20416
322.6154 45.30035
323.0975 44.10675
323.5797 43.09271
324.0618 42.32678
324.5439 41.55212
325.0260 40.47992
325.5081 39.36267
325.9902 38.75592
326.4724 38.91138
326.9545 39.33588
327.4366 39.24762
327.9187 38.59607
328.4008 37.88251
328.8829 37.25629
329.3651 36.58636
329.8472 35.61426
330.3293 34.29327
330.8114 33.03845
331.2935 32.24615
331.7756 31.96521
332.2578 31.87872
332.7399 32.14911
333.2220 32.48035
333.7041 32.69043
334.1862 32.76544
334.6683 32.71930
335.1505 32.54956
335.6326 32.26312
336.1147 31.95563
336.5968 31.68268
337.0789 31.33301
337.5610 30.59662
338.0432 29.73822
338.5253 29.45630
339.0074 30.14105
339.4895 31.44165
339.9716 32.41461
340.4537 32.84094
340.9359 33.39124
341.4180 34.42920
341.9001 35.57489
342.3822 36.24072
342.8643 36.24036
343.3464 36.07458
343.8286 36.44763
344.3107 37.60785
344.7928 38.48132
345.2749 38.61359
345.7570 38.85510
346.2391 40.01019
346.7213 42.03778
347.2034 44.19464
347.6855 45.81555
348.1676 46.88110
348.6497 47.93658
349.1318 48.70184
349.6140 49.70850
350.0961 51.25281
350.5782 53.21783
351.0603 55.36145
351.5424 57.56079
352.0245 59.77197
352.5067 61.81354
352.9888 63.37067
353.4709 65.14404
353.9530 67.18225
354.4351 69.48895
354.9172 72.10150
355.3994 75.02643
355.8815 78.19031
356.3636 81.52881
356.8457 85.35553
357.3278 88.66272
357.8099 91.01764
358.2920 93.22528
358.7741 95.64453
359.2563 98.42108
359.7384 101.7545
360.2205 105.8779
360.7026 110.9016
361.1847 115.3557
361.6668 119.2928
362.1490 122.7216
362.6311 125.1356
363.1132 127.0187
363.5953 129.3045
364.0774 132.6403
364.5595 136.7399
365.0417 140.2673
365.5238 142.5167
366.0059 145.0405
366.4880 148.0628
366.9701 151.3976
367.4522 154.9531
367.9344 158.6660
368.4165 162.3703
368.8986 165.9059
369.3807 169.5563
369.8628 172.1671
370.3449 173.0721
370.8271 173.6379
371.3092 174.4997
371.7913 175.6689
372.2734 176.8752
372.7555 177.9591
373.2376 178.9021
373.7198 179.5193
374.2019 179.7098
374.6840 179.6360
375.1661 179.1890
375.6482 178.6071
376.1303 178.2621
376.6125 178.4430
377.0946 178.7701
377.5767 178.3234
378.0588 176.9334
378.5409 175.2303
379.0230 173.0981
379.5052 170.8945
379.9873 169.0484
380.4694 167.6310
380.9515 165.9621
381.4336 163.1191
381.9157 159.1263
382.3979 155.6418
382.8800 153.1707
383.3621 150.9180
383.8442 148.5354
384.3263 145.9528
384.8084 142.8636
385.2906 138.9596
385.7727 134.4917
386.2548 129.8408
386.7369 124.8546
387.2190 120.2974
387.7011 117.0533
388.1833 114.3833
388.6654 111.2189
389.1475 107.1904
389.6296 102.9435
390.1117 99.03375
390.5938 95.41162
391.0760 91.83154
391.5581 88.25854
392.0402 84.64160
392.5223 80.81476
393.0044 76.73871
393.4865 72.94666
393.9687 69.67023
394.4508 66.81000
394.9329 64.44012
395.4150 62.60907
395.8971 60.56897
396.3792 57.38995
396.8614 53.22430
397.3435 49.88867
397.8256 47.97528
398.3077 46.41736
398.7898 44.63568
399.2719 42.62836
399.7540 40.41107
400.2361 37.91547
400.7183 35.33606
401.2004 33.34418
401.6825 32.41663
402.1646 31.14008
402.6467 28.96698
403.1288 26.45581
403.6110 24.22791
404.0931 22.44196
404.5752 20.92383
405.0573 19.49567
405.5394 18.19788
406.0215 16.86267
406.5037 15.36682
406.9858 13.96588
407.4679 12.82880
407.9500 11.88782
408.4321 10.95593
408.9142 9.899109
409.3964 8.755249
409.8785 7.670715
410.3606 6.584717
410.8427 5.652435
411.3248 4.712036
411.8069 4.015228
412.2891 4.031433
412.7712 4.781677
413.2533 5.529755
413.7354 5.155945
414.2175 3.220642
414.6996 1.910126
415.1818 1.928894
415.6639 1.941071
416.1460 1.278809
416.6281 0.1811220
417.1102 0.6597900
417.5923 0.7389830
418.0745 0.3082280
418.5566 0.3003850
419.0387 1.004761
419.5208 1.476501
420.0029 0.9919430
420.4850 0.3828430
420.9672 0.5324100
421.4493 1.668732
421.9314 2.981506
422.4135 3.639099
422.8956 3.667908
423.3777 3.651947
423.8599 3.640686
424.3420 3.646332
424.8241 3.854218
425.3062 4.133575
425.7883 3.993561
426.2704 2.792480
426.7526 1.247803
427.2347 0.5151370
427.7168 0.6405940
428.1989 0.7833560
428.6810 0.3969420
429.1631 0.1978150
429.6453 0.2332460
430.1274 0.6654360
430.6095 1.279968
431.0916 0.6590580
431.5737 0.6193850
432.0558 1.269775
432.5380 0.8975220
433.0201 0.4066160
433.5022 0.9819030
433.9843 2.832397
434.4664 3.950989
434.9485 3.515839
435.4307 2.967468
435.9128 3.443085
436.3949 4.684296
436.8770 5.562286
437.3591 5.331512
437.8412 4.425873
438.3234 4.520996
438.8055 6.857178
439.2876 8.620422
439.7697 9.392303
440.2518 9.645111
440.7339 9.647247
441.2160 9.541290
441.6982 9.596283
442.1803 10.17822
442.6624 11.40433
443.1445 12.31586
443.6266 12.50949
444.1087 12.80597
444.5909 13.44626
445.0730 14.36118
445.5551 15.47391
446.0372 16.77457
446.5193 18.08121
447.0014 18.90222
447.4836 18.97513
447.9657 19.36160
448.4478 20.68707
448.9299 22.07010
449.4120 22.76126
449.8941 22.82089
450.3763 23.14352
450.8584 24.72186
451.3405 27.19656
451.8226 28.94354
452.3047 29.72769
452.7868 30.26370
453.2690 30.87350
453.7511 31.52176
454.2332 32.14523
454.7153 32.67181
455.1974 33.31696
455.6795 34.23029
456.1617 35.34113
456.6438 36.67615
457.1259 38.32300
457.6080 40.02982
458.0901 41.47958
458.5722 42.69382
459.0544 43.77475
459.5365 44.57965
460.0186 45.36069
460.5007 46.42706
460.9828 47.73392
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