#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:36:24 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1185 $ #$URL: svn://172.16.1.111/rod/cif/1/00/06/1000601.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000601 loop_ _publ_author_name 'Grice, J. D.' 'Rowe, R.' 'Poirier, G.' 'Pratt, A.' 'Francis, J.' _publ_section_title ; Bussyite-(Ce), a new beryllium silicate mineral species from Mont Saint-Hilaire, Quebec Locality: Poudrette quarry, Mont Saint-Hilaire, Quebec, Canada ; _journal_issue 1 _journal_name_full 'The Canadian Mineralogist' _journal_page_first 193 _journal_page_last 204 _journal_paper_doi 10.3749/canmin.47.1.193 _journal_volume 47 _journal_year 2009 _chemical_compound_source R120059 _chemical_formula_sum 'Be5.176 Ca0.764 Ce0.824 Eu0.008 F4 Gd0.078 H7.72 La0.236 Mg0.012 Mn0.485 Na3.652 Nd0.374 O33.15 Pr0.114 Si8.824 Sm0.08 Th0.174 Y0.242' _chemical_name_mineral Bussyite-(Ce) _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 96.127 _cell_angle_gamma 90 _cell_length_a 11.6445 _cell_length_b 13.9212 _cell_length_c 16.5909 _cell_volume 2674.112 _exptl_crystal_density_diffrn 3.368 _cod_original_formula_sum ;Be5.176 Ca0.764 Ce0.824 Eu0.008 F4 Gd0.078 H7.72 La0.236 Mg0.012 Mn0.485 Na3.652 Nd0.374 O33.15 Pr0.114 Si8.824 Sm0.08 Th0.174 Y0.242 ; _cod_database_code 9013787 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R120059.rod _rod_data_source.block 3500000 _rod_database.code 1000601 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9013787 COD http://www.crystallography.net/cod/9013787.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 110.8882 0.0000000E+00 111.3703 1.182617 111.8524 0.1197510 112.3345 8.4778003E-02 112.8167 3.077942 113.2988 5.793945 113.7809 7.630066 114.2630 8.922241 114.7451 10.13983 115.2272 11.58209 115.7094 13.21265 116.1915 14.58710 116.6736 15.84845 117.1557 16.75073 117.6378 17.11261 118.1199 16.99878 118.6021 16.59406 119.0842 15.94690 119.5663 15.04358 120.0484 14.71753 120.5305 15.19110 121.0126 16.07062 121.4948 17.18530 121.9769 18.56058 122.4590 19.75052 122.9411 20.17694 123.4232 20.01233 123.9053 19.66971 124.3875 19.24924 124.8696 18.74521 125.3517 18.05606 125.8338 16.82108 126.3159 15.88208 126.7980 15.84525 127.2802 16.63354 127.7623 17.64447 128.2444 18.72928 128.7265 20.04459 129.2086 20.74841 129.6907 19.89926 130.1729 18.92682 130.6550 18.74792 131.1371 19.29883 131.6192 19.75040 132.1013 18.82776 132.5834 15.31897 133.0656 12.80429 133.5477 11.45889 134.0298 10.84506 134.5119 10.76065 134.9940 11.09766 135.4761 11.70258 135.9583 12.31506 136.4404 13.52859 136.9225 14.02036 137.4046 13.54675 137.8867 12.87949 138.3688 12.55560 138.8510 13.26468 139.3331 14.26910 139.8152 14.53448 140.2973 14.20721 140.7794 13.60641 141.2615 13.02606 141.7437 12.50827 142.2258 11.88342 142.7079 10.93661 143.1900 10.00418 143.6721 9.799225 144.1542 10.91739 144.6364 12.19006 145.1185 12.40869 145.6006 11.44104 146.0827 10.15149 146.5648 8.546173 147.0469 6.996124 147.5291 5.985901 148.0112 5.890778 148.4933 6.250671 148.9754 5.914703 149.4575 4.282684 149.9396 2.972443 150.4218 2.575653 150.9039 2.712006 151.3860 2.918549 151.8681 2.945465 152.3502 2.818451 152.8323 2.723328 153.3145 2.658356 153.7966 2.563629 154.2787 2.341614 154.7608 2.057770 155.2429 1.905426 155.7250 2.113831 156.2072 2.374176 156.6893 2.527710 157.1714 2.853516 157.6535 2.811279 158.1356 2.731476 158.6177 2.775421 159.0999 2.879211 159.5820 2.979523 160.0641 3.003754 160.5462 2.525879 161.0283 0.9536130 161.5104 0.5797420 161.9926 0.9792180 162.4747 9.2377000E-02 162.9568 0.9893800 163.4389 0.9801030 163.9210 4.6386998E-02 164.4031 0.8033140 164.8853 0.8600460 165.3674 0.5965880 165.8495 0.6143490 166.3316 1.137512 166.8137 1.569794 167.2958 1.062195 167.7780 0.1263120 168.2601 0.9331670 168.7422 0.8324890 169.2243 0.1653440 169.7064 0.4821470 170.1885 0.5143740 170.6707 1.693359 171.1528 2.281677 171.6349 2.375214 172.1170 2.418732 172.5991 2.853821 173.0812 3.713440 173.5634 4.229431 174.0455 3.642578 174.5276 3.272766 175.0097 3.796478 175.4918 5.148804 175.9739 6.787750 176.4561 8.204590 176.9382 9.453491 177.4203 10.24472 177.9024 10.26184 178.3845 10.12021 178.8666 10.07324 179.3488 10.19345 179.8309 10.45425 180.3130 10.86343 180.7951 11.58649 181.2772 12.07285 181.7593 12.15100 182.2415 12.13995 182.7236 12.29349 183.2057 12.66440 183.6878 13.11499 184.1699 13.45917 184.6520 13.78171 185.1342 13.79535 185.6163 13.31598 186.0984 12.60208 186.5805 11.93326 187.0626 11.39557 187.5447 10.87326 188.0269 10.12256 188.5090 9.047668 188.9911 8.142242 189.4732 7.588623 189.9553 7.266113 190.4374 7.024445 190.9196 6.851715 191.4017 6.646027 191.8838 6.239746 192.3659 5.643036 192.8480 4.933228 193.3301 4.035095 193.8123 3.030182 194.2944 2.200317 194.7765 1.644012 195.2586 1.278625 195.7407 0.9856260 196.2228 0.7679440 196.7050 0.5963130 197.1871 0.5006710 197.6692 0.4817200 198.1513 0.3898010 198.6334 0.2295840 199.1155 6.3446000E-02 199.5977 0.6849820 200.0798 1.603775 200.5619 2.335098 201.0440 2.204727 201.5261 1.003418 202.0082 0.3737950 202.4904 1.583328 202.9725 2.653854 203.4546 2.334778 203.9367 0.5988620 204.4188 1.443146 204.9009 2.381561 205.3831 1.833389 205.8652 1.335907 206.3473 0.8334660 206.8294 0.4665990 207.3115 0.2678380 207.7936 0.2766720 208.2758 0.5837550 208.7579 1.426208 209.2400 3.466843 209.7221 4.511322 210.2042 3.878677 210.6863 2.902908 211.1685 2.431717 211.6506 2.654404 212.1327 3.267105 212.6148 3.849136 213.0969 4.467972 213.5790 4.875839 214.0612 4.779510 214.5433 4.673904 215.0254 5.056213 215.5075 6.012558 215.9896 7.083817 216.4717 7.622604 216.9539 7.382263 217.4360 7.115555 217.9181 6.743546 218.4002 6.384247 218.8823 6.136276 219.3644 6.002777 219.8466 5.970840 220.3287 6.088821 220.8108 6.334259 221.2929 6.587448 221.7750 6.786102 222.2571 6.952850 222.7393 7.249756 223.2214 7.755142 223.7035 8.213638 224.1856 8.192963 224.6677 7.732773 225.1498 7.411728 225.6320 7.511139 226.1141 7.796753 226.5962 7.939240 227.0783 7.839828 227.5604 7.640350 228.0425 7.507538 228.5247 7.421692 229.0068 7.379227 229.4889 7.347977 229.9710 7.363480 230.4531 7.545532 230.9352 8.005829 231.4174 8.423477 231.8995 8.598969 232.3816 8.551849 232.8637 8.300171 233.3458 7.664139 233.8279 6.817032 234.3101 6.303101 234.7922 6.214233 235.2743 6.386749 235.7564 6.787949 236.2385 7.307907 236.7206 7.786942 237.2028 8.151459 237.6849 8.417892 238.1670 8.634445 238.6491 8.811249 239.1312 8.919510 239.6133 8.705597 240.0955 8.445297 240.5776 8.681778 241.0597 9.993912 241.5418 11.99977 242.0239 12.73476 242.5060 11.13260 242.9882 9.639618 243.4703 8.937622 243.9524 8.796921 244.4345 8.871628 244.9166 8.981598 245.3987 9.128708 245.8809 9.337311 246.3630 9.721222 246.8451 10.02025 247.3272 10.30850 247.8093 10.45612 248.2914 10.20641 248.7736 9.381851 249.2557 8.213165 249.7378 7.673019 250.2199 8.567993 250.7020 9.113586 251.1841 8.874832 251.6663 8.231277 252.1484 7.594315 252.6305 7.156570 253.1126 6.932724 253.5947 6.965866 254.0768 7.989426 254.5590 8.374710 255.0411 7.379333 255.5232 5.970963 256.0053 5.285141 256.4874 5.791504 256.9695 6.963562 257.4517 7.540268 257.9338 6.570206 258.4159 6.094116 258.8980 6.763626 259.3801 7.817688 259.8622 8.279755 260.3444 7.780518 260.8265 6.764038 261.3086 6.057785 261.7907 5.859894 262.2728 5.848740 262.7549 5.989975 263.2371 6.256042 263.7192 6.765900 264.2013 7.563248 264.6834 8.214752 265.1655 7.994232 265.6476 6.348938 266.1298 5.181259 266.6119 4.703110 267.0940 4.684479 267.5761 4.920990 268.0582 5.393951 268.5403 5.790680 269.0225 5.718338 269.5046 5.038818 269.9867 4.552856 270.4688 4.549057 270.9509 4.578430 271.4330 4.127762 271.9152 3.164322 272.3973 2.248703 272.8794 1.949738 273.3615 2.336823 273.8436 2.670715 274.3257 2.718948 274.8079 2.833954 275.2900 3.488815 275.7721 4.678223 276.2542 5.611618 276.7363 5.608307 277.2184 4.744354 277.7006 4.135712 278.1827 3.941040 278.6648 3.882324 279.1469 3.853607 279.6290 3.830475 280.1111 3.622192 280.5933 2.941284 281.0754 2.058334 281.5575 1.845108 282.0396 2.906738 282.5217 3.894745 283.0038 3.768555 283.4860 2.748215 283.9681 2.008881 284.4502 2.178101 284.9323 2.880493 285.4144 3.303787 285.8965 3.431320 286.3787 3.350555 286.8608 2.934967 287.3429 2.308350 287.8250 1.919495 288.3071 1.937622 288.7892 2.244324 289.2714 2.728561 289.7535 3.435593 290.2356 3.953537 290.7177 4.155655 291.1998 4.024216 291.6819 3.393539 292.1641 1.972534 292.6462 0.5509950 293.1283 1.3855000E-02 293.6104 0.2623140 294.0925 0.7963560 294.5746 1.603348 295.0568 2.532135 295.5389 3.279770 296.0210 3.793030 296.5031 4.176453 296.9852 4.653915 297.4673 5.110382 297.9495 5.128174 298.4316 4.160919 298.9137 2.842087 299.3958 2.170807 299.8779 2.269287 300.3600 2.486511 300.8422 2.300995 301.3243 1.965958 301.8064 1.951462 302.2885 2.604431 302.7706 3.386597 303.2527 3.652390 303.7349 3.372803 304.2170 3.005127 304.6991 2.669434 305.1812 2.417114 305.6633 2.306946 306.1454 2.343033 306.6276 2.526367 307.1097 3.023651 307.5918 3.801971 308.0739 4.210205 308.5560 3.780426 309.0381 3.085754 309.5203 2.884705 310.0024 3.259094 310.4845 3.461853 310.9666 2.813354 311.4487 1.498535 311.9308 0.4187320 312.4130 0.2692720 312.8951 0.6405640 313.3772 0.7170100 313.8593 0.5347600 314.3414 0.3273470 314.8235 0.2768250 315.3057 0.2857970 315.7878 2.3209000E-02 316.2699 0.9353180 316.7520 1.553284 317.2341 0.7557370 317.7162 0.8441160 318.1984 1.889130 318.6805 1.511093 319.1626 0.4710390 319.6447 5.2184999E-02 320.1268 0.4074400 320.6089 0.6079860 321.0911 0.1598660 321.5732 1.339920 322.0553 2.192963 322.5374 2.607498 323.0195 2.599258 323.5016 1.826447 323.9838 0.2746430 324.4659 0.5168300 324.9480 0.6989290 325.4301 2.526062 325.9122 3.127060 326.3943 2.197601 326.8765 1.171600 327.3586 1.185226 327.8407 2.050323 328.3228 2.743896 328.8049 3.108139 329.2870 3.098969 329.7692 2.584961 330.2513 1.613907 330.7334 0.7050170 331.2155 3.3966001E-02 331.6976 0.5148620 332.1797 0.4411930 332.6619 0.3647310 333.1440 1.320114 333.6261 1.875595 334.1082 2.200256 334.5903 2.775467 335.0724 3.879532 335.5546 5.082214 336.0367 5.914215 336.5188 6.356003 337.0009 6.811890 337.4830 7.595901 337.9651 8.534622 338.4473 9.260056 338.9294 9.592300 339.4115 9.886490 339.8936 10.36386 340.3757 11.00844 340.8578 11.85426 341.3400 13.02827 341.8221 14.33955 342.3042 15.46106 342.7863 16.36243 343.2684 17.37715 343.7505 18.71333 344.2327 20.22343 344.7148 21.61604 345.1969 22.78737 345.6790 23.99135 346.1611 25.40105 346.6432 26.94492 347.1254 28.66626 347.6075 30.50761 348.0896 32.62682 348.5717 35.13283 349.0538 38.03204 349.5359 41.30219 350.0181 45.14240 350.5002 49.35701 350.9823 53.09824 351.4644 55.74208 351.9465 58.43495 352.4286 62.23242 352.9108 66.85799 353.3929 71.11984 353.8750 74.47400 354.3571 77.02063 354.8392 79.11572 355.3214 80.99326 355.8035 82.04713 356.2856 81.60663 356.7677 80.26425 357.2498 79.15262 357.7319 78.64484 358.2141 78.14963 358.6962 76.72600 359.1783 74.18907 359.6604 71.91277 360.1425 70.12892 360.6246 68.62067 361.1068 67.21330 361.5889 65.87363 362.0710 64.67966 362.5531 63.78424 363.0352 63.15842 363.5173 62.00522 363.9995 59.96404 364.4816 57.80437 364.9637 55.75186 365.4458 53.86649 365.9279 52.24136 366.4100 50.92081 366.8922 49.90498 367.3743 49.24976 367.8564 49.55792 368.3385 49.35245 368.8206 48.06143 369.3027 46.31885 369.7849 44.90569 370.2670 44.01559 370.7491 43.20088 371.2312 41.82227 371.7133 39.63947 372.1954 37.67725 372.6776 36.04474 373.1597 34.51067 373.6418 32.93246 374.1239 31.33101 374.6060 29.80264 375.0881 28.43329 375.5703 27.15834 376.0524 25.82272 376.5345 24.15709 377.0166 22.94482 377.4987 22.87567 377.9808 23.14223 378.4630 22.51360 378.9451 20.45972 379.4272 17.64816 379.9093 15.75220 380.3914 15.61050 380.8735 14.99553 381.3557 13.32036 381.8378 11.53952 382.3199 10.43282 382.8020 10.12637 383.2841 9.954056 383.7662 9.155792 384.2484 7.573837 384.7305 6.446136 385.2126 6.170120 385.6947 5.983109 386.1768 5.774124 386.6589 5.463943 387.1411 4.906296 387.6232 3.947922 388.1053 2.775406 388.5874 2.084488 389.0695 2.053024 389.5516 2.137177 390.0338 2.701904 390.5159 3.118698 390.9980 2.461334 391.4801 0.5009310 391.9622 1.537292 392.4443 1.958282 392.9265 0.5566100 393.4086 0.4949800 393.8907 0.9023740 394.3728 0.8860320 394.8549 0.3815160 395.3370 0.4747310 395.8192 1.233398 396.3013 1.656479 396.7834 1.761124 397.2655 1.519699 397.7476 0.7559970 398.2297 0.1063540 398.7119 7.6614000E-02 399.1940 4.7928002E-02 399.6761 0.3859560 400.1582 1.076401 400.6403 1.612839 401.1224 1.177841 401.6046 0.1439210 402.0867 0.7474210 402.5688 0.3091580 403.0509 1.776382 403.5330 2.042953 404.0151 1.085785 404.4973 0.2658540 404.9794 0.5515440 405.4615 1.256226 405.9436 0.9895940 406.4257 0.5261080 406.9078 2.019958 407.3900 2.311584 407.8721 1.638474 408.3542 1.361176 408.8363 1.757019 409.3184 2.407288 409.8005 3.314209 410.2827 4.309235 410.7648 4.679657 411.2469 3.944168 411.7290 2.742859 412.2111 2.675537 412.6932 4.397568 413.1754 5.446564 413.6575 4.692444 414.1396 3.439194 414.6217 3.041046 415.1038 3.724411 415.5859 4.953430 416.0681 6.285431 416.5502 7.761856 417.0323 8.788605 417.5144 9.063095 417.9965 9.280579 418.4786 9.711884 418.9608 10.29309 419.4429 10.88222 419.9250 11.40892 420.4071 11.87228 420.8892 12.27225 421.3713 12.63255 421.8535 12.87749 422.3356 12.79152 422.8177 12.74718 423.2998 13.03146 423.7819 13.67859 424.2640 14.54521 424.7462 15.52649 425.2283 16.64508 425.7104 17.60580 426.1925 18.53246 426.6746 19.13266 427.1567 19.15811 427.6389 18.84285 428.1210 18.51343 428.6031 18.31058 429.0852 18.23463 429.5673 18.33936 430.0494 18.71780 430.5316 18.94316 431.0137 18.66580 431.4958 18.37239 431.9779 18.54413 432.4600 19.14481 432.9421 19.46945 433.4243 18.61340 433.9064 16.95703 434.3885 16.24489 434.8706 16.87212 435.3527 17.71049 435.8348 18.13298 436.3170 18.26097 436.7991 18.25725 437.2812 18.11798 437.7633 17.91626 438.2454 17.69199 438.7275 17.45218 439.2097 17.29218 439.6918 17.34055 440.1739 17.34009 440.6560 16.75685 441.1381 15.51669 441.6202 14.63629 442.1024 14.55685 442.5845 14.89731 443.0666 15.33658 443.5487 15.81607 444.0308 16.15036 444.5129 16.13759 444.9951 15.84117 445.4772 15.86868 445.9593 16.80525 446.4414 17.34282 446.9235 16.75233 447.4056 15.60922 447.8878 14.79964 448.3699 14.62318 448.8520 14.71146 449.3341 14.44348 449.8162 13.35532 450.2983 13.10454 450.7805 14.58273 451.2626 16.04926 451.7447 16.42549 452.2268 15.99770 452.7089 15.75169 453.1910 16.37492 453.6732 17.57262 454.1553 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