#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:36:54 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1193 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000607.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000607
loop_
_publ_author_name
'Onac, B. P.'
'Effenberger, H. S.'
_publ_section_title
;
 Re-examination of berlinite (AlPO4) from the Cioclovina Cave, Romania
 Locality: Cioclovina Cave, Romania
;
_journal_name_full               'American Mineralogist'
_journal_page_first              1998
_journal_page_last               2001
_journal_paper_doi               10.2138/am.2007.2581
_journal_volume                  92
_journal_year                    2007
_chemical_compound_source        R130243
_chemical_formula_sum            'Al O4 P'
_chemical_name_mineral           Berlinite
_space_group_IT_number           152
_symmetry_space_group_name_Hall  'P 31 2"'
_symmetry_space_group_name_H-M   'P 31 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   4.9458
_cell_length_b                   4.9458
_cell_length_c                   10.9526
_cell_volume                     232.018
_exptl_crystal_density_diffrn    2.618
_cod_original_formula_sum        'Al P O4'
_cod_database_code               9010367
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R130243.rod
_rod_data_source.block           3500000
_rod_database.code               1000607
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9010367 COD http://www.crystallography.net/cod/9010367.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
102.1665 0.0000000E+00
102.6486 0.1837540
103.1307 2.038139
103.6128 6.232872
104.0950 11.98030
104.5771 18.96748
105.0592 27.35200
105.5413 36.59993
106.0234 46.15533
106.5055 57.23634
106.9877 68.62032
107.4698 75.44530
107.9519 76.36086
108.4340 73.65451
108.9161 67.22081
109.3982 58.09637
109.8804 48.62395
110.3625 40.53606
110.8446 33.64758
111.3267 29.10072
111.8088 27.33997
112.2909 27.23812
112.7731 28.40139
113.2552 30.74966
113.7373 34.48726
114.2194 40.11532
114.7015 48.73516
115.1836 58.49599
115.6658 69.59565
116.1479 81.43169
116.6300 93.83873
117.1121 107.1461
117.5942 120.2065
118.0763 130.1855
118.5584 138.6453
119.0406 142.1116
119.5227 138.5461
120.0048 129.2675
120.4869 116.5939
120.9690 100.1318
121.4511 81.81573
121.9333 65.37777
122.4154 50.72829
122.8975 38.08381
123.3796 28.02578
123.8617 20.66972
124.3438 14.66721
124.8260 9.897858
125.3081 6.056404
125.7902 3.032608
126.2723 0.8758160
126.7544 0.5358010
127.2365 1.376305
127.7187 1.342903
128.2008 1.199986
128.6829 1.173168
129.1650 1.203892
129.6471 1.202927
130.1292 1.103024
130.6114 0.9159970
131.0935 0.8213460
131.5756 0.9116250
132.0577 1.001663
132.5398 1.061199
133.0219 1.084614
133.5041 1.074474
133.9862 1.035084
134.4683 0.9686360
134.9504 0.8484000
135.4325 0.6414490
135.9146 0.3028220
136.3968 0.5793340
136.8789 1.928078
137.3610 3.314255
137.8431 4.510864
138.3252 5.340214
138.8073 5.859058
139.2895 6.457169
139.7716 7.122143
140.2537 7.750404
140.7358 8.315765
141.2179 9.001442
141.7000 10.09172
142.1821 11.53948
142.6643 13.05973
143.1464 14.61132
143.6285 16.15619
144.1106 17.57201
144.5927 18.80853
145.0748 19.91614
145.5570 21.01657
146.0391 22.10573
146.5212 23.02163
147.0033 23.49108
147.4854 23.44178
147.9675 23.66696
148.4497 24.41238
148.9318 25.44222
149.4139 26.72958
149.8960 28.24765
150.3781 29.87147
150.8602 31.34917
151.3424 32.44953
151.8245 33.97204
152.3066 35.97735
152.7887 38.34342
153.2708 41.04077
153.7529 44.03653
154.2351 47.26401
154.7172 50.54078
155.1993 53.42777
155.6814 56.94661
156.1635 61.07645
156.6456 65.86957
157.1278 71.41406
157.6099 77.77456
158.0920 84.83662
158.5741 92.16728
159.0562 99.86633
159.5383 107.6796
160.0205 115.7591
160.5026 123.9106
160.9847 132.2084
161.4668 140.9194
161.9489 149.5431
162.4310 156.1382
162.9131 162.6693
163.3953 165.6780
163.8774 163.1783
164.3595 155.3004
164.8416 142.9523
165.3237 124.4936
165.8058 102.1491
166.2880 81.23244
166.7701 61.53737
167.2522 43.96882
167.7343 29.74884
168.2164 19.09670
168.6985 10.88024
169.1807 5.460991
169.6628 1.878376
170.1449 0.7683790
170.6270 2.668232
171.1091 3.900372
171.5912 4.607845
172.0734 4.677235
172.5555 4.375160
173.0376 3.825417
173.5197 3.047901
174.0018 2.045460
174.4839 0.7812230
174.9661 0.7009770
175.4482 2.117138
175.9303 3.390480
176.4124 4.686424
176.8945 5.978065
177.3766 7.327061
177.8588 8.830807
178.3409 10.59196
178.8230 12.61731
179.3051 14.49937
179.7872 16.14563
180.2693 17.74461
180.7515 19.21084
181.2336 20.65369
181.7157 22.30697
182.1978 24.40391
182.6799 27.01126
183.1620 29.38467
183.6441 31.12412
184.1263 33.00130
184.6084 35.45683
185.0905 38.45688
185.5726 41.59287
186.0547 44.38970
186.5368 46.76244
187.0190 49.62556
187.5011 53.10975
187.9832 56.94489
188.4653 60.95620
188.9474 65.09959
189.4296 69.42461
189.9117 73.99158
190.3938 78.80085
190.8759 83.87453
191.3580 89.13034
191.8401 94.67187
192.3223 100.7190
192.8044 107.3684
193.2865 114.2346
193.7686 121.1775
194.2507 128.1347
194.7328 134.6684
195.2150 141.0706
195.6971 146.9108
196.1792 151.3248
196.6613 154.0902
197.1434 155.6697
197.6255 155.9400
198.1077 155.3365
198.5898 154.9539
199.0719 155.1498
199.5540 155.9780
200.0361 157.6433
200.5182 160.1541
201.0004 163.6496
201.4825 168.1605
201.9646 173.5493
202.4467 179.4349
202.9288 185.4792
203.4109 191.7249
203.8930 198.7397
204.3752 206.5328
204.8573 215.2057
205.3394 224.9727
205.8215 235.5954
206.3036 246.6281
206.7857 257.6417
207.2679 268.6133
207.7500 280.0330
208.2321 292.2588
208.7142 304.6521
209.1963 317.1122
209.6784 329.5569
210.1606 341.8959
210.6427 354.1180
211.1248 366.2055
211.6069 377.6544
212.0890 388.8685
212.5711 399.1353
213.0533 408.4054
213.5354 416.5161
214.0175 423.2263
214.4996 428.2214
214.9817 431.3115
215.4638 433.8251
215.9460 436.2336
216.4281 437.8314
216.9102 437.8637
217.3923 436.5884
217.8744 435.1319
218.3565 434.5519
218.8387 434.9984
219.3208 435.0222
219.8029 434.4329
220.2850 433.6317
220.7671 433.0947
221.2492 432.7302
221.7314 431.8424
222.2135 429.9338
222.6956 426.8425
223.1777 422.5184
223.6598 416.4955
224.1419 409.6096
224.6240 402.4769
225.1062 395.1104
225.5883 387.2766
226.0704 378.7868
226.5525 369.6323
227.0346 359.8846
227.5167 348.7382
227.9989 337.4134
228.4810 327.3997
228.9631 318.8724
229.4452 310.5198
229.9273 301.5101
230.4094 292.0000
230.8916 282.3719
231.3737 272.4917
231.8558 262.7009
232.3379 253.4778
232.8200 244.8970
233.3021 236.3206
233.7843 227.1629
234.2664 217.7688
234.7485 208.6425
235.2306 199.9358
235.7127 191.5221
236.1948 183.0506
236.6770 174.2999
237.1591 166.1953
237.6412 159.5224
238.1233 153.6369
238.6054 147.8391
239.0875 141.8305
239.5697 135.9362
240.0518 130.7781
240.5339 126.5133
241.0160 122.4288
241.4981 118.2468
241.9802 114.0966
242.4624 110.1004
242.9445 106.3082
243.4266 102.7031
243.9087 99.30898
244.3908 96.24811
244.8729 93.07252
245.3550 89.60810
245.8372 86.02283
246.3193 82.41199
246.8014 78.79259
247.2835 75.26407
247.7656 71.95744
248.2477 68.95909
248.7299 66.00687
249.2120 63.10135
249.6941 60.20043
250.1762 57.24059
250.6583 54.20268
251.1404 51.20080
251.6226 48.38824
252.1047 45.79099
252.5868 43.38110
253.0689 41.19580
253.5510 39.13413
254.0331 37.11120
254.5153 35.11419
254.9974 33.17964
255.4795 31.35580
255.9616 29.69976
256.4437 28.04926
256.9258 26.31623
257.4080 24.66050
257.8901 23.18835
258.3722 21.91531
258.8543 20.75949
259.3364 19.60094
259.8185 18.37365
260.3007 17.30697
260.7828 16.48005
261.2649 15.70637
261.7470 14.83611
262.2291 13.87328
262.7112 12.98278
263.1934 12.38155
263.6755 12.22568
264.1576 11.77306
264.6397 10.75911
265.1218 9.724806
265.6039 9.021023
266.0861 8.622208
266.5682 8.234295
267.0503 7.548410
267.5324 6.480413
268.0145 5.689964
268.4966 5.310383
268.9788 5.023304
269.4609 4.705429
269.9430 4.347534
270.4251 3.983477
270.9072 3.643074
271.3893 3.331173
271.8715 2.973133
272.3536 2.530359
272.8357 2.090740
273.3178 1.659489
273.7999 1.258663
274.2820 0.9527360
274.7642 0.8035370
275.2463 0.7896270
275.7284 0.6447790
276.2105 0.2254960
276.6926 0.1384050
277.1747 0.3195670
277.6568 0.3628290
278.1389 0.3630200
278.6211 0.3626610
279.1032 0.3712390
279.5853 0.4364930
280.0674 0.5983850
280.5495 0.7578790
281.0316 0.9282530
281.5138 1.075609
281.9959 1.115017
282.4780 0.9930780
282.9601 0.7973690
283.4422 0.7663460
283.9243 0.9996010
284.4065 1.181759
284.8886 1.187294
285.3707 1.119442
285.8528 1.156986
286.3349 1.371767
286.8170 1.623106
287.2992 1.656363
287.7813 1.412739
288.2634 1.177444
288.7455 1.007414
289.2276 0.8631820
289.7097 0.6758020
290.1919 0.4250130
290.6740 0.1948510
291.1561 0.1172920
291.6382 0.2239230
292.1203 0.2423310
292.6024 0.1363220
293.0846 6.4856999E-02
293.5667 0.3778500
294.0488 0.7989940
294.5309 1.184599
295.0130 1.371250
295.4951 1.361464
295.9773 1.488569
296.4594 1.804390
296.9415 2.212765
297.4236 2.694212
297.9057 3.232891
298.3878 3.712910
298.8700 4.018267
299.3521 4.188257
299.8342 4.475412
300.3163 4.924532
300.7984 5.443995
301.2805 6.022842
301.7627 6.642269
302.2448 7.226591
302.7269 7.733025
303.2090 8.180714
303.6911 8.642788
304.1732 9.177231
304.6554 9.638435
305.1375 10.00053
305.6196 10.24349
306.1017 10.31165
306.5838 10.17883
307.0659 9.868986
307.5481 9.404480
308.0302 8.774208
308.5123 8.095545
308.9944 7.398623
309.4765 6.680372
309.9586 5.938774
310.4408 5.173515
310.9229 4.395882
311.4050 3.597746
311.8871 2.764946
312.3692 2.062096
312.8513 1.577709
313.3335 1.215076
313.8156 0.8620990
314.2977 0.5039140
314.7798 0.1608980
315.2619 0.1757070
315.7440 0.4941560
316.2262 0.6731050
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317.6725 0.3604370
318.1546 0.2534980
318.6367 0.1596680
319.1188 7.2467998E-02
319.6010 1.9440000E-03
320.0831 4.6698000E-02
320.5652 2.7725000E-02
321.0473 1.3824000E-02
321.5294 2.3512000E-02
322.0115 6.4787000E-02
322.4937 0.1651730
322.9758 0.3361260
323.4579 0.5779670
323.9400 0.8894840
324.4221 1.288311
324.9042 1.703888
325.3864 2.100853
325.8685 2.499554
326.3506 2.954395
326.8327 3.493511
327.3148 4.053951
327.7969 4.516294
328.2791 4.849407
328.7612 5.273254
329.2433 5.841614
329.7254 6.514355
330.2075 7.225599
330.6896 7.973677
331.1718 8.862186
331.6539 10.02722
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332.6181 13.05383
333.1002 14.63110
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335.5108 23.74617
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336.4750 25.13360
336.9572 24.85925
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337.9214 22.56476
338.4035 20.57844
338.8856 18.42584
339.3677 16.19709
339.8499 13.96625
340.3320 12.03237
340.8141 10.45516
341.2962 9.081039
341.7783 7.911009
342.2604 6.900080
342.7426 6.021540
343.2247 5.272377
343.7068 4.616978
344.1889 4.006603
344.6710 3.440615
345.1531 2.957201
345.6353 2.653551
346.1174 2.397745
346.5995 2.067343
347.0816 1.663660
347.5637 1.283033
348.0458 1.012640
348.5280 0.8533330
349.0101 0.7433800
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349.9743 0.6697120
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353.8312 0.6424100
354.3134 0.8677860
354.7955 1.282763
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355.7597 2.528074
356.2418 3.268318
356.7239 3.964689
357.2061 4.664482
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363.4735 14.10981
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365.8841 19.03106
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367.3305 24.12815
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369.2589 36.18356
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370.7053 52.84499
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373.1159 88.93851
373.5980 95.62679
374.0801 99.27364
374.5622 98.90847
375.0443 96.35052
375.5265 91.00182
376.0086 84.28831
376.4907 78.18563
376.9728 73.48688
377.4549 70.24225
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379.3834 71.30397
379.8655 69.77843
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380.8297 59.14008
381.3119 51.18275
381.7940 42.66774
382.2761 33.60780
382.7582 25.78779
383.2403 19.53591
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387.5794 0.1618210
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389.0257 0.6899620
389.5078 1.071981
389.9900 1.432625
390.4721 1.653090
390.9542 1.746304
391.4363 1.806219
391.9184 1.863628
392.4005 1.897892
392.8827 1.877249
393.3648 1.799656
393.8469 1.714415
394.3290 1.628881
394.8111 1.551130
395.2932 1.548651
395.7754 1.648687
396.2575 1.621216
396.7396 1.194092
397.2217 0.4031160
397.7038 0.2380790
398.1859 0.5761220
398.6681 0.8812890
399.1501 1.297909
399.6323 1.827044
400.1144 2.468475
400.5965 3.241598
401.0786 4.094725
401.5607 4.866110
402.0428 5.529772
402.5250 6.171782
403.0071 6.751490
403.4892 7.344313
403.9713 8.023151
404.4534 8.803785
404.9355 9.683529
405.4177 10.67075
405.8998 11.78397
406.3819 12.89471
406.8640 13.87783
407.3461 14.97385
407.8282 16.30807
408.3104 17.85669
408.7925 19.53454
409.2746 21.30769
409.7567 23.18664
410.2388 25.22969
410.7209 27.31085
411.2031 29.73567
411.6852 32.57104
412.1673 35.74603
412.6494 39.24801
413.1315 43.04726
413.6136 47.01760
414.0958 51.01389
414.5779 55.06903
415.0600 59.07988
415.5421 63.03222
416.0242 66.93379
416.5063 71.29533
416.9885 75.63473
417.4706 78.86445
417.9527 80.35401
418.4348 80.21117
418.9169 78.68575
419.3990 75.37571
419.8812 71.55203
420.3633 67.21278
420.8454 62.80285
421.3275 58.72773
421.8096 55.08741
422.2917 51.78579
422.7739 48.73162
423.2560 45.93325
423.7381 43.43430
424.2202 41.23606
424.7023 39.37967
425.1844 37.74074
425.6666 36.38456
426.1487 35.57370
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