#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:40:44 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1219 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000632.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000632
loop_
_publ_author_name
'Moore, P. B.'
'Araki, T.'
_publ_section_title
;
 Bahianite, Al5Sb3O14(O,OH)2, a novel hexagonal close-packed oxide
 structure Locality: Serra de Mangabeira, Bahia, Brazil
;
_journal_name_full
'Neues Jahrbuch fur Mineralogie, Abhandlungen'
_journal_page_first              113
_journal_page_last               125
_journal_volume                  126
_journal_year                    1976
_chemical_compound_source        R050627
_chemical_formula_sum            'Al4.76 Fe0.34 O16 Sb2.9'
_chemical_name_mineral           Bahianite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.94
_cell_angle_gamma                90
_cell_length_a                   9.406
_cell_length_b                   11.541
_cell_length_c                   4.410
_cell_volume                     478.662
_exptl_crystal_density_diffrn    5.249
_cod_original_formula_sum        'Sb2.9 Fe.34 Al4.76 O16'
_cod_database_code               9009247
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050627.rod
_rod_data_source.block           3500000
_rod_database.code               1000632
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009247 COD http://www.crystallography.net/cod/9009247.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
149.9194 0.0000000E+00
150.4015 0.9215700
150.8836 0.9170530
151.3657 8.2824998E-02
151.8479 0.1137700
152.3300 1.803406
152.8121 6.146912
153.2942 9.656860
153.7763 11.63867
154.2584 13.72241
154.7406 16.68524
155.2227 20.49323
155.7048 24.56677
156.1869 28.23102
156.6690 31.50958
157.1511 36.31366
157.6333 42.88104
158.1154 49.87903
158.5975 56.19934
159.0796 61.62433
159.5617 66.96692
160.0438 73.31686
160.5260 81.00192
161.0081 89.59204
161.4902 99.74619
161.9723 110.8013
162.4544 122.0864
162.9365 134.8454
163.4187 147.1486
163.9008 157.3009
164.3829 164.5582
164.8650 167.0134
165.3471 163.0704
165.8292 153.5510
166.3113 142.6080
166.7935 130.7791
167.2756 118.2720
167.7577 104.8434
168.2398 90.50110
168.7219 76.41705
169.2040 63.48178
169.6862 51.43655
170.1683 41.27350
170.6504 34.04236
171.1325 28.48856
171.6146 24.47406
172.0967 21.85101
172.5789 19.82663
173.0610 17.30634
173.5431 14.16721
174.0252 10.75427
174.5073 6.479309
174.9894 2.333221
175.4716 1.039124
175.9537 3.399323
176.4358 4.879791
176.9179 5.716614
177.4000 5.629028
177.8821 5.160187
178.3643 4.186310
178.8464 2.918152
179.3285 1.654053
179.8106 0.5160830
180.2927 0.7481690
180.7748 2.848511
181.2570 7.043640
181.7391 10.52185
182.2212 12.80899
182.7033 14.21857
183.1854 15.06516
183.6675 15.39752
184.1497 15.47012
184.6318 16.12915
185.1139 17.51352
185.5960 19.07831
186.0781 21.11606
186.5602 23.26889
187.0423 24.31198
187.5245 23.14587
188.0066 20.97452
188.4887 20.57938
188.9708 22.28116
189.4529 25.04645
189.9350 28.46539
190.4172 32.49850
190.8993 36.81335
191.3814 41.39545
191.8635 46.11914
192.3456 50.69455
192.8277 54.80637
193.3099 59.32257
193.7920 65.23303
194.2741 72.68213
194.7562 80.59381
195.2383 88.88873
195.7204 97.31339
196.2026 105.9594
196.6847 115.1969
197.1668 123.7361
197.6489 129.6235
198.1310 132.4919
198.6131 133.5889
199.0953 133.0754
199.5774 131.2695
200.0595 128.4476
200.5416 124.7465
201.0237 119.8635
201.5058 113.0347
201.9880 103.3438
202.4701 93.13440
202.9522 81.68378
203.4343 70.53497
203.9164 61.09940
204.3985 54.00095
204.8807 49.17352
205.3628 46.58505
205.8449 48.04529
206.3270 49.63370
206.8091 50.75610
207.2912 51.80991
207.7733 53.67038
208.2555 56.16516
208.7376 59.21069
209.2197 62.51926
209.7018 65.82901
210.1839 69.74323
210.6660 74.50598
211.1482 79.87091
211.6303 85.43292
212.1124 90.97797
212.5945 96.68192
213.0766 103.4730
213.5587 112.6096
214.0409 121.1718
214.5230 128.3672
215.0051 134.6350
215.4872 140.7973
215.9693 147.2398
216.4514 153.8813
216.9336 160.4105
217.4157 167.5840
217.8978 173.8103
218.3799 178.6964
218.8620 182.2578
219.3441 184.7065
219.8263 186.3351
220.3084 186.5371
220.7905 184.1569
221.2726 179.6522
221.7547 172.3889
222.2368 161.4588
222.7190 147.3171
223.2011 131.4933
223.6832 113.6687
224.1653 95.36243
224.6474 78.98529
225.1295 64.26379
225.6117 51.94531
226.0938 43.26331
226.5759 37.89310
227.0580 33.26694
227.5401 28.30820
228.0222 23.88760
228.5043 21.01651
228.9865 20.01926
229.4686 19.56055
229.9507 18.42450
230.4328 16.61960
230.9149 15.43634
231.3970 15.80826
231.8792 16.58801
232.3613 16.62509
232.8434 15.69040
233.3255 14.74500
233.8076 14.83310
234.2897 16.07193
234.7719 17.71313
235.2540 19.45538
235.7361 21.84091
236.2182 25.21201
236.7003 29.65079
237.1824 35.08258
237.6646 41.76852
238.1467 50.06195
238.6288 57.84888
239.1109 65.13770
239.5930 71.58636
240.0751 76.77887
240.5573 80.74118
241.0394 84.06110
241.5215 87.15594
242.0036 89.77209
242.4857 93.26083
242.9678 98.61658
243.4500 104.1168
243.9321 108.8163
244.4142 112.6873
244.8963 116.4117
245.3784 120.5756
245.8605 124.9373
246.3427 130.6473
246.8248 138.4509
247.3069 146.8776
247.7890 155.1774
248.2711 163.3721
248.7532 171.9413
249.2354 181.4891
249.7175 192.0989
250.1996 203.3525
250.6817 214.8997
251.1638 227.2443
251.6459 239.9443
252.1281 253.4821
252.6102 269.1415
253.0923 288.4716
253.5744 311.9453
254.0565 335.8198
254.5386 361.0968
255.0208 385.8098
255.5029 411.1360
255.9850 435.6552
256.4671 456.4323
256.9492 471.8433
257.4313 482.5939
257.9135 477.1726
258.3956 452.7237
258.8777 419.1612
259.3598 376.1780
259.8419 326.8083
260.3240 277.0984
260.8062 231.0657
261.2883 188.7013
261.7704 153.1223
262.2525 124.5922
262.7346 100.3667
263.2167 79.88641
263.6989 62.87250
264.1810 49.41299
264.6631 39.81668
265.1452 33.71460
265.6273 27.71933
266.1094 21.15112
266.5916 15.38565
267.0737 11.19955
267.5558 8.236481
268.0379 5.620972
268.5200 2.880798
269.0021 0.1668400
269.4843 1.774414
269.9664 3.055237
270.4485 3.588837
270.9306 3.189270
271.4127 2.144806
271.8948 0.9899600
272.3770 1.3062000E-02
272.8591 0.9810180
273.3412 2.691681
273.8233 5.620880
274.3054 8.031281
274.7875 8.871582
275.2697 8.913391
275.7518 9.626770
276.2339 11.59683
276.7160 14.20972
277.1981 16.34409
277.6802 18.05392
278.1623 19.47318
278.6444 20.18451
279.1266 20.74103
279.6087 22.33517
280.0908 25.51022
280.5729 28.87466
281.0550 30.03656
281.5371 28.96851
282.0193 28.85327
282.5014 30.84976
282.9835 34.15128
283.4656 37.82687
283.9477 41.81842
284.4298 45.62158
284.9120 48.42740
285.3941 50.39542
285.8762 52.62698
286.3583 55.31830
286.8404 58.40207
287.3225 61.76459
287.8047 65.38791
288.2868 69.42838
288.7689 74.22977
289.2510 79.60132
289.7331 84.95999
290.2152 90.49493
290.6974 95.77158
291.1795 100.4969
291.6616 104.6839
292.1437 107.8876
292.6258 110.1457
293.1079 111.0229
293.5901 109.7901
294.0722 106.1169
294.5543 100.5857
295.0364 93.18231
295.5185 83.96219
296.0006 74.44873
296.4828 65.11560
296.9649 56.04233
297.4470 47.04254
297.9291 37.52399
298.4112 29.45758
298.8933 25.02579
299.3755 23.67480
299.8576 21.85992
300.3397 18.18463
300.8218 13.78052
301.3039 9.971222
301.7860 6.693268
302.2682 4.428772
302.7503 3.706238
303.2324 4.252838
303.7145 5.255463
304.1966 6.943573
304.6787 8.355255
305.1609 8.129822
305.6430 6.481598
306.1251 5.317169
306.6072 6.012360
307.0893 7.703888
307.5714 8.271149
308.0536 7.013672
308.5357 5.951172
309.0178 7.159790
309.4999 9.965515
309.9820 12.73511
310.4641 14.86572
310.9463 16.68170
311.4284 18.64908
311.9105 20.80096
312.3926 22.91940
312.8747 24.55820
313.3568 26.11661
313.8390 28.35577
314.3211 31.71072
314.8032 35.49991
315.2853 39.24362
315.7674 42.94165
316.2495 46.07526
316.7317 47.66769
317.2138 49.00058
317.6959 52.37610
318.1780 59.03751
318.6601 64.91016
319.1422 66.45526
319.6243 64.20386
320.1064 61.84088
320.5886 60.70691
321.0707 59.62292
321.5528 57.42285
322.0349 54.15384
322.5170 49.52783
322.9991 42.60486
323.4813 34.17465
323.9634 26.23099
324.4455 18.97556
324.9276 12.72635
325.4097 8.272797
325.8918 5.275024
326.3740 2.366669
326.8561 1.483826
327.3382 5.390381
327.8203 7.750854
328.3024 8.219971
328.7845 8.246429
329.2667 9.181519
329.7488 10.49863
330.2309 10.82657
330.7130 9.088257
331.1951 6.845245
331.6772 5.924316
332.1594 6.299164
332.6415 6.075317
333.1236 3.865784
333.6057 0.5531010
334.0878 1.843597
334.5699 2.804291
335.0521 3.666962
335.5342 5.331940
336.0163 7.638123
336.4984 10.02505
336.9805 12.49542
337.4626 14.65417
337.9448 15.73288
338.4269 15.59906
338.9090 15.62750
339.3911 16.26492
339.8732 17.45380
340.3553 19.19733
340.8375 21.58658
341.3196 24.14185
341.8017 26.24405
342.2838 27.94696
342.7659 29.94064
343.2480 32.11972
343.7302 34.78589
344.2123 38.62930
344.6944 43.65683
345.1765 48.39398
345.6586 51.57626
346.1407 53.44354
346.6229 55.95752
347.1050 59.40689
347.5871 63.23218
348.0692 67.04950
348.5513 70.92117
349.0334 75.44806
349.5156 81.31726
349.9977 87.51038
350.4798 91.16351
350.9619 91.91461
351.4440 91.52396
351.9261 90.28394
352.4083 88.30920
352.8904 85.97412
353.3725 83.47958
353.8546 80.03964
354.3367 74.09259
354.8188 64.84082
355.3010 56.54968
355.7831 49.81381
356.2652 44.07083
356.7473 38.94635
357.2294 34.34988
357.7115 30.05823
358.1937 25.80322
358.6758 21.59436
359.1579 18.09637
359.6400 14.71759
360.1221 12.50122
360.6042 12.92380
361.0863 15.03668
361.5685 16.15063
362.0506 14.53589
362.5327 11.18195
363.0148 10.24908
363.4969 13.79694
363.9790 16.99661
364.4612 18.74295
364.9433 19.96530
365.4254 21.66229
365.9075 24.17795
366.3896 27.41843
366.8717 31.31848
367.3539 36.37769
367.8360 40.94077
368.3181 44.13864
368.8002 47.52194
369.2823 52.15073
369.7644 58.04138
370.2466 64.64282
370.7287 71.56305
371.2108 78.83664
371.6929 85.76456
372.1750 92.31253
372.6571 98.59811
373.1393 104.7218
373.6214 110.6880
374.1035 116.6926
374.5856 122.8642
375.0677 128.7120
375.5498 132.5877
376.0320 132.5730
376.5141 133.3248
376.9962 135.8257
377.4783 138.8315
377.9604 141.2293
378.4425 142.7354
378.9247 143.7982
379.4068 144.8099
379.8889 145.4480
380.3710 147.4252
380.8531 151.7759
381.3352 156.5350
381.8174 160.5103
382.2995 163.9844
382.7816 168.2248
383.2637 174.4983
383.7458 182.3879
384.2279 189.1699
384.7101 194.3049
385.1922 198.2709
385.6743 201.5896
386.1564 204.0453
386.6385 205.2326
387.1206 204.8452
387.6028 203.5399
388.0849 202.5455
388.5670 202.1434
389.0491 201.2477
389.5312 198.8126
390.0133 196.2544
390.4955 194.4515
390.9776 193.6241
391.4597 193.7010
391.9418 194.2685
392.4239 195.3774
392.9060 198.0468
393.3882 202.8575
393.8703 208.3640
394.3524 213.7075
394.8345 218.9916
395.3166 224.4529
395.7987 230.0295
396.2809 235.9240
396.7630 242.4824
397.2451 249.7999
397.7272 257.0758
398.2093 263.7138
398.6914 270.3297
399.1736 277.8572
399.6557 286.5752
400.1378 295.6119
400.6199 304.2620
401.1020 312.8413
401.5841 322.3123
402.0662 333.0219
402.5483 344.2365
403.0305 354.9624
403.5126 365.2437
403.9947 375.9842
404.4768 387.4212
404.9589 399.3383
405.4410 411.5942
405.9232 424.1012
406.4053 436.7821
406.8874 449.8053
407.3695 462.8281
407.8516 474.6225
408.3337 485.0451
408.8159 494.5625
409.2980 504.7577
409.7801 513.8458
410.2622 519.2014
410.7443 519.9783
411.2264 516.4250
411.7086 508.9944
412.1907 497.5229
412.6728 481.5060
413.1549 459.5461
413.6370 434.3311
414.1191 406.8702
414.6013 377.6887
415.0834 347.3135
415.5655 315.8628
416.0476 283.4645
416.5297 254.4963
417.0118 230.9922
417.4940 208.9027
417.9761 187.7288
418.4582 167.5044
418.9403 148.3434
419.4224 130.2101
419.9045 113.7978
420.3867 100.3733
420.8688 90.97467
421.3509 82.05447
421.8330 73.48331
422.3151 65.36636
422.7972 57.60745
423.2794 50.36581
423.7615 44.07132
424.2436 39.24008
424.7257 35.68539
425.2078 32.10413
425.6899 28.49927
426.1721 24.86688
426.6542 20.73605
427.1363 16.74084
427.6184 13.77954
428.1005 12.25696
428.5826 11.18140
429.0648 9.310730
429.5469 6.620605
430.0290 4.123199
430.5111 2.011169
430.9932 0.2261660
431.4753 1.306091
431.9575 2.594971
432.4396 3.719116
432.9217 4.727325
433.4038 5.583618
433.8859 6.302002
434.3680 6.908722
434.8502 7.072845
435.3323 6.317566
435.8144 5.005310
436.2965 4.144653
436.7786 3.672729
437.2607 3.797211
437.7429 5.348053
438.2250 7.548676
438.7071 8.303772
439.1892 6.771576
439.6713 4.705475
440.1534 4.685699
440.6356 7.313751
441.1177 9.310547
441.5998 10.87338
442.0819 11.46378
442.5640 10.08685
443.0461 7.188080
443.5282 4.457123
444.0103 3.039459
444.4925 2.730621
444.9746 2.425873
445.4567 2.659271
445.9388 2.219360
446.4209 0.3808900
446.9030 1.877930
447.3852 3.523895
447.8673 4.315399
448.3494 4.848846
448.8315 5.839996
449.3136 7.301544
449.7957 9.146332
450.2779 11.81683
450.7600 14.44998
451.2421 16.67850
451.7242 18.66019
452.2063 20.70990
452.6884 22.96475
453.1706 25.43604
453.6527 27.90387
454.1348 29.90121
454.6169 33.34332
455.0990 40.53748
455.5811 48.16599
456.0633 53.46536
456.5454 56.34052
457.0275 59.78708
457.5096 66.19006
457.9917 74.95367
458.4738 84.25150
458.9560 94.27713
459.4381 104.0293
459.9202 112.3689
460.4023 120.0241
460.8844 128.4458
461.3665 138.2598
461.8487 148.3010
462.3308 157.8156
462.8129 166.8506
463.2950 175.6819
463.7771 184.5994
464.2592 192.9131
464.7414 199.3383
465.2235 203.5262
465.7056 208.5372
466.1877 214.4229
466.6698 221.5296
467.1519 230.2422
467.6341 240.4863
468.1162 251.7993
468.5983 263.9211
469.0804 276.8339
469.5625 289.9868
470.0446 302.3829
470.5268 316.3575
471.0089 332.0209
471.4910 349.3602
471.9731 368.7602
472.4552 390.0337
472.9373 411.9484
473.4195 433.2152
473.9016 453.7610
474.3837 474.2341
474.8658 497.9750
475.3479 517.5398
475.8300 532.1225
476.3122 540.8684
476.7943 543.3342
477.2764 539.4224
477.7585 528.0044
478.2406 506.4364
478.7227 474.2004
479.2049 436.9321
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