#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:41:04 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1224 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000636.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000636
loop_
_publ_author_name
'Groat, L. A.'
'Jambor, J. L.'
'Pemberton, B. C.'
_publ_section_title
;
 The crystal structure of argentojarosite, AgFe3(SO4)2(OH)6 Locality:
 Tintic Standard mine at Dividend, central Utah
;
_journal_name_full               'The Canadian Mineralogist'
_journal_page_first              921
_journal_page_last               928
_journal_paper_doi               10.2113/gscanmin.41.4.921
_journal_volume                  41
_journal_year                    2003
_chemical_compound_source        R060097
_chemical_formula_sum            'Ag Al0.12 Fe2.88 H6 O14 S2'
_chemical_name_mineral           Argentojarosite
_space_group_IT_number           166
_symmetry_space_group_name_Hall  '-R 3 2"'
_symmetry_space_group_name_H-M   'R -3 m :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   7.3398
_cell_length_b                   7.3398
_cell_length_c                   16.538
_cell_volume                     771.582
_exptl_crystal_density_diffrn    3.655
_cod_original_sg_symbol_H-M      'R -3 m'
_cod_original_formula_sum        'Ag (Fe2.88 Al.12) S2 O14 H6'
_cod_database_code               9004771
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060097.rod
_rod_data_source.block           3500000
_rod_database.code               1000636
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9004771 COD http://www.crystallography.net/cod/9004771.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
108.8945 0.0000000E+00
109.3766 9.5656998E-02
109.8588 0.3060460
110.3409 0.2752510
110.8230 4.0004998E-02
111.3051 8.1528001E-02
111.7872 0.3134350
112.2693 0.9751720
112.7515 1.625668
113.2336 2.134319
113.7157 2.723883
114.1978 3.674044
114.6799 4.970362
115.1620 6.394777
115.6442 7.869921
116.1263 9.388214
116.6084 10.77044
117.0905 11.96006
117.5726 12.98466
118.0547 13.88026
118.5369 14.65148
119.0190 15.27662
119.5011 15.67428
119.9832 15.66833
120.4653 15.86997
120.9474 16.44449
121.4296 17.16810
121.9117 17.85128
122.3938 18.41450
122.8759 18.91237
123.3580 19.52834
123.8401 20.31953
124.3223 21.19444
124.8044 22.18161
125.2865 23.24671
125.7686 24.33868
126.2507 25.43831
126.7328 26.54441
127.2150 27.65780
127.6971 28.86942
128.1792 30.03984
128.6613 31.05022
129.1434 31.99983
129.6255 33.04412
130.1077 34.29390
130.5898 35.75108
131.0719 37.20613
131.5540 38.53728
132.0361 39.81903
132.5182 41.14486
133.0004 42.52681
133.4825 43.98051
133.9646 45.67434
134.4467 47.60209
134.9288 49.67900
135.4109 52.33481
135.8931 55.18070
136.3752 56.95578
136.8573 57.81134
137.3394 57.05228
137.8215 54.28094
138.3036 49.77433
138.7858 44.39286
139.2679 38.46818
139.7500 31.84061
140.2321 25.97079
140.7142 20.92792
141.1963 16.62218
141.6785 13.12047
142.1606 10.39401
142.6427 8.271008
143.1248 6.587702
143.6069 5.509768
144.0890 4.545235
144.5712 3.668833
145.0533 2.899073
145.5354 2.240246
146.0175 1.698643
146.4996 1.271322
146.9817 0.9617520
147.4639 0.8803390
147.9460 0.7456170
148.4281 0.4908940
148.9102 0.1927240
149.3923 4.9300998E-02
149.8744 0.1936040
150.3566 0.2778760
150.8387 0.3943810
151.3208 0.5694730
151.8029 0.7112240
152.2850 0.7896920
152.7671 0.8087410
153.2493 0.7714900
153.7314 0.6524930
154.2135 0.4982600
154.6956 0.3911150
155.1777 0.3395000
155.6598 0.3160670
156.1420 0.3340090
156.6241 0.3999560
157.1062 0.3834670
157.5883 0.1796590
158.0704 0.1152630
158.5525 0.4421920
159.0347 0.8027590
159.5168 1.144783
159.9989 1.359301
160.4810 1.353394
160.9631 1.453876
161.4452 1.877115
161.9274 2.384653
162.4095 2.737040
162.8916 2.811020
163.3737 2.703581
163.8558 2.737267
164.3379 3.092737
164.8201 3.355326
165.3022 3.368820
165.7843 3.273392
166.2664 3.254478
166.7485 3.464319
167.2306 3.841599
167.7128 4.183565
168.1949 4.502439
168.6770 4.773218
169.1591 4.932215
169.6412 5.040466
170.1233 5.225409
170.6055 5.592016
171.0876 6.134224
171.5697 6.514692
172.0518 6.654362
172.5339 6.743752
173.0160 6.831871
173.4982 6.934799
173.9803 7.100397
174.4624 7.389973
174.9445 7.793562
175.4266 8.108952
175.9087 8.266796
176.3909 8.385363
176.8730 8.546888
177.3551 8.756216
177.8372 9.019009
178.3193 9.428446
178.8014 9.904924
179.2836 10.19127
179.7657 10.13434
180.2478 9.890779
180.7299 9.699099
181.2120 9.596468
181.6941 9.456999
182.1763 9.202414
182.6584 8.855164
183.1405 8.440886
183.6226 7.933569
184.1047 7.367512
184.5868 6.848871
185.0690 6.383175
185.5511 5.967716
186.0332 5.599295
186.5153 5.271281
186.9974 4.965441
187.4795 4.655733
187.9617 4.348383
188.4438 4.145416
188.9259 4.102307
189.4080 4.121059
189.8901 4.189726
190.3722 4.295898
190.8544 4.418655
191.3365 4.534466
191.8186 4.638953
192.3007 4.819103
192.7828 5.054945
193.2649 5.384554
193.7471 5.809940
194.2292 6.339634
194.7113 6.997008
195.1934 7.806162
195.6755 8.789150
196.1576 9.820394
196.6398 10.81961
197.1219 11.92153
197.6040 13.18259
198.0861 14.60573
198.5682 16.17946
199.0503 17.88672
199.5325 19.73718
200.0146 21.75384
200.4967 23.93991
200.9788 26.26784
201.4609 28.72031
201.9430 31.30407
202.4252 34.03357
202.9073 36.98318
203.3894 40.17855
203.8715 43.17854
204.3536 45.98795
204.8357 48.58865
205.3179 50.94466
205.8000 53.05463
206.2821 54.97920
206.7642 56.71427
207.2463 58.29108
207.7284 59.90186
208.2106 61.60336
208.6927 63.35608
209.1748 65.10275
209.6569 66.84705
210.1390 68.60053
210.6211 70.33692
211.1033 72.08860
211.5854 73.96021
212.0675 76.07168
212.5496 78.32485
213.0317 80.53030
213.5138 82.68752
213.9960 84.74364
214.4781 86.56979
214.9602 88.27974
215.4423 90.12455
215.9244 92.34055
216.4065 94.79697
216.8886 96.97279
217.3708 98.79849
217.8529 100.4142
218.3350 101.8825
218.8171 103.2249
219.2992 104.5024
219.7813 105.8305
220.2635 107.1428
220.7456 107.9610
221.2277 108.1300
221.7098 107.9065
222.1919 107.6128
222.6740 107.0093
223.1562 105.6929
223.6383 103.3937
224.1204 100.1339
224.6025 96.15996
225.0846 91.01138
225.5667 85.57151
226.0489 79.80382
226.5310 73.88352
227.0131 68.05403
227.4952 62.41758
227.9773 57.01859
228.4594 52.05304
228.9416 47.66053
229.4237 43.61498
229.9058 39.92207
230.3879 36.54940
230.8700 33.50003
231.3521 30.76784
231.8343 28.34035
232.3164 26.11851
232.7985 24.11821
233.2806 22.28463
233.7627 20.61631
234.2448 19.10181
234.7270 17.72685
235.2091 16.49177
235.6912 15.38374
236.1733 14.28959
236.6554 13.10621
237.1375 12.03307
237.6197 11.17747
238.1018 10.48371
238.5839 9.813682
239.0660 9.085667
239.5481 8.321082
240.0302 7.637784
240.5124 7.018343
240.9945 6.479832
241.4766 6.075609
241.9587 5.763872
242.4408 5.445300
242.9229 5.071456
243.4051 4.650072
243.8872 4.202631
244.3693 3.668011
244.8514 3.195364
245.3335 2.864365
245.8156 2.651869
246.2978 2.494809
246.7799 2.381058
247.2620 2.292000
247.7441 2.186865
248.2262 2.069616
248.7083 1.932281
249.1905 1.771400
249.6726 1.587717
250.1547 1.373091
250.6368 1.098623
251.1189 0.8212030
251.6010 0.6273430
252.0832 0.5248790
252.5653 0.4524140
253.0474 0.3688960
253.5295 0.2838060
254.0116 0.2480410
254.4937 0.3207520
254.9759 0.3913780
255.4580 0.3188350
255.9401 9.8325998E-02
256.4222 0.1145820
256.9043 0.2128180
257.3864 0.2163480
257.8686 0.2238720
258.3507 0.2391350
258.8328 0.2848300
259.3149 0.4008720
259.7970 0.5760270
260.2791 0.7140840
260.7613 0.7374400
261.2434 0.6642580
261.7255 0.5988640
262.2076 0.5672530
262.6897 0.5231930
263.1718 0.4423860
263.6540 0.3273360
264.1361 0.1874470
264.6182 9.8839998E-03
265.1003 0.2424130
265.5824 0.3665740
266.0645 0.2964100
266.5467 0.2319930
267.0288 0.2530120
267.5109 0.3541260
267.9930 0.5320530
268.4751 0.8099970
268.9572 1.154928
269.4394 1.409666
269.9215 1.498277
270.4036 1.611394
270.8857 1.844233
271.3678 2.143362
271.8499 2.422671
272.3321 2.629359
272.8142 2.788999
273.2963 2.970865
273.7784 3.150609
274.2605 3.399351
274.7426 3.720025
275.2248 4.113111
275.7069 4.592947
276.1890 5.179610
276.6711 5.818970
277.1532 6.357448
277.6353 6.720058
278.1175 7.122513
278.5996 7.566410
279.0817 8.081139
279.5638 8.704923
280.0459 9.454768
280.5280 10.28755
281.0102 11.13069
281.4923 11.97492
281.9744 12.84501
282.4565 13.66086
282.9386 14.54639
283.4207 15.64118
283.9029 16.96511
284.3850 18.35793
284.8671 19.56525
285.3492 20.49011
285.8313 21.46516
286.3134 22.55529
286.7956 23.65327
287.2777 24.70574
287.7598 25.69700
288.2419 26.63939
288.7240 27.54370
289.2061 28.38644
289.6883 29.25616
290.1704 30.22909
290.6525 31.15727
291.1346 31.91705
291.6167 32.54906
292.0988 33.20991
292.5810 34.06083
293.0631 35.12523
293.5452 36.10923
294.0273 36.91290
294.5094 37.73852
294.9915 38.68678
295.4737 39.71353
295.9558 40.71419
296.4379 41.61164
296.9200 42.41364
297.4021 43.18847
297.8842 43.92694
298.3664 44.64837
298.8485 45.38054
299.3306 46.09260
299.8127 46.74000
300.2948 47.29760
300.7769 47.76244
301.2591 48.12033
301.7412 48.50456
302.2233 48.58429
302.7054 48.29997
303.1875 47.71235
303.6696 46.88814
304.1518 45.85591
304.6339 44.59739
305.1160 43.05041
305.5981 41.19792
306.0802 39.03804
306.5623 36.44017
307.0445 33.65018
307.5266 30.79717
308.0087 27.94313
308.4908 25.13154
308.9729 22.39474
309.4550 19.58747
309.9372 17.28561
310.4193 15.68846
310.9014 14.32970
311.3835 12.93860
311.8656 11.49304
312.3477 10.12980
312.8299 9.000220
313.3120 8.120943
313.7941 7.318539
314.2762 6.565207
314.7583 5.890608
315.2404 5.313192
315.7226 4.826681
316.2047 4.421320
316.6868 4.098636
317.1689 3.847904
317.6510 3.563756
318.1331 3.209476
318.6153 2.869707
319.0974 2.598851
319.5795 2.360403
320.0616 2.068609
320.5437 1.667141
321.0258 1.211653
321.5080 0.9141240
321.9901 0.9496580
322.4722 0.9671360
322.9543 0.9692080
323.4364 0.9136910
323.9185 0.7293030
324.4007 0.4059030
324.8828 4.3189999E-02
325.3649 0.1811120
325.8470 0.1852500
326.3291 0.1725150
326.8112 0.1381550
327.2934 0.1075160
327.7755 0.1060700
328.2576 0.1291160
328.7397 0.1429290
329.2218 0.1075440
329.7039 5.2129999E-03
330.1861 5.9978001E-02
330.6682 5.2643999E-02
331.1503 3.7199002E-02
331.6324 4.3414999E-02
332.1145 7.1519002E-02
332.5966 0.1223730
333.0788 0.1902090
333.5609 0.2611530
334.0430 0.2892510
334.5251 0.1804100
335.0072 0.1326070
335.4893 0.2088610
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336.4536 0.5308800
336.9357 0.6826660
337.4178 0.8235110
337.8999 0.9601120
338.3820 1.039768
338.8642 1.200322
339.3463 1.546977
339.8284 1.920435
340.3105 2.156786
340.7926 2.219827
341.2747 2.222420
341.7568 2.337993
342.2390 2.611725
342.7211 2.889057
343.2032 3.201978
343.6853 3.490826
344.1674 3.696342
344.6495 3.835418
345.1317 3.987960
345.6138 4.239336
346.0959 4.598789
346.5780 4.900689
347.0601 5.091763
347.5422 5.273061
348.0244 5.476622
348.5065 5.688867
348.9886 5.876234
349.4707 6.011534
349.9528 6.117164
350.4349 6.280594
350.9171 6.516815
351.3992 6.797737
351.8813 7.176460
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352.8455 7.870776
353.3276 8.068491
353.8098 8.182596
354.2919 8.227855
354.7740 8.145620
355.2561 8.176725
355.7382 8.472343
356.2203 8.789895
356.7025 8.993858
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357.6667 9.092505
358.1488 9.116886
358.6309 9.147902
359.1130 9.134685
359.5952 9.107299
360.0773 8.991154
360.5594 8.732948
361.0415 8.369900
361.5236 7.975492
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362.4879 7.199709
362.9700 6.804243
363.4521 6.399180
363.9342 5.990087
364.4163 5.567817
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365.3806 4.741289
365.8627 4.350931
366.3448 3.981436
366.8269 3.637933
367.3090 3.318691
367.7911 3.029392
368.2733 2.803918
368.7554 2.582883
369.2375 2.306758
369.7196 1.978334
370.2017 1.677023
370.6838 1.470391
371.1660 1.342722
371.6481 1.231440
372.1302 1.158030
372.6123 1.051128
373.0944 0.8167050
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374.5408 0.1950770
375.0229 0.1862660
375.5050 0.1678090
375.9871 0.1415100
376.4692 8.8064000E-02
376.9514 4.8028000E-02
377.4335 0.1930710
377.9156 0.2275010
378.3977 0.1001800
378.8798 2.9172000E-02
379.3619 2.0445000E-02
379.8441 9.1748998E-02
380.3262 0.1521170
380.8083 0.1036260
381.2904 1.4165000E-02
381.7725 4.7632001E-02
382.2546 8.4912002E-02
382.7368 6.8735003E-02
383.2189 7.3400997E-02
383.7010 0.2517240
384.1831 0.3407060
384.6652 0.3235370
385.1473 0.2736700
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386.5937 0.2139580
387.0758 0.1999370
387.5579 0.1559610
388.0400 1.9760000E-02
388.5222 0.1686000
389.0043 0.2616000
389.4864 0.1647720
389.9685 2.5464000E-02
390.4506 5.1208001E-02
390.9327 0.1755890
391.4149 0.3359840
391.8970 0.2834870
392.3791 0.1661860
392.8612 0.1838000
393.3433 0.3755430
393.8254 0.5976530
394.3076 0.6785150
394.7897 0.5783480
395.2718 0.5476920
395.7539 0.6241980
396.2360 0.7288760
396.7181 0.8349250
397.2003 0.9336810
397.6824 1.005727
398.1645 1.032939
398.6466 1.033785
399.1287 1.104790
399.6108 1.310727
400.0930 1.509939
400.5751 1.693369
401.0572 1.861116
401.5393 2.021674
402.0214 2.175075
402.5035 2.302677
402.9857 2.362494
403.4678 2.289584
403.9499 2.341558
404.4320 2.616652
404.9141 2.909732
405.3962 3.099832
405.8784 3.215315
406.3605 3.366099
406.8426 3.638616
407.3247 4.015513
407.8068 4.361290
408.2889 4.644498
408.7711 4.938739
409.2532 5.275567
409.7353 5.623516
410.2174 5.926123
410.6995 6.162674
411.1816 6.422409
411.6638 6.835956
412.1459 7.413821
412.6280 8.082116
413.1101 8.930157
413.5922 9.783218
414.0743 10.48109
414.5565 11.07028
415.0386 11.76958
415.5207 12.76406
416.0028 13.98504
416.4849 15.15326
416.9670 16.18108
417.4492 17.37766
417.9313 18.97785
418.4134 20.81890
418.8955 22.71321
419.3776 24.60312
419.8597 26.57240
420.3419 28.75094
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