#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:41:19 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1228 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000640.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000640
loop_
_publ_author_name
'Hazen, R. M.'
'Burnham, C. W.'
_publ_section_title
;
 The crystal structures of one-layer phlogopite and annite
;
_journal_name_full               'American Mineralogist'
_journal_page_first              889
_journal_page_last               900
_journal_volume                  58
_journal_year                    1973
_chemical_compound_source        R060204
_chemical_formula_sum
'Al1.282 Ca0.03 Cl0.05 F0.22 Fe2.43 H1.38 K0.88 Mg0.12 Mn0.03 Na0.07 O11.73 Si2.808 Ti0.21'
_chemical_name_mineral           Annite
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.63
_cell_angle_gamma                90
_cell_length_a                   5.3860
_cell_length_b                   9.3241
_cell_length_c                   10.2683
_cell_volume                     506.820
_exptl_crystal_density_diffrn    3.250
_cod_original_formula_sum
;Al1.282 Ca0.03 Cl0.05 F0.22 Fe2.43 H1.38 K0.88 Mg0.12 Mn0.03 Na0.07 O11.73
 Si2.808 Ti0.21
;
_cod_database_code               9000377
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060204.rod
_rod_data_source.block           3500000
_rod_database.code               1000640
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000377 COD http://www.crystallography.net/cod/9000377.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
145.3421 0.0000000E+00
145.8242 0.2505490
146.3063 0.4784240
146.7884 0.1232450
147.2706 0.1681670
147.7527 0.1430050
148.2348 0.2596740
148.7169 0.8653560
149.1990 1.288483
149.6811 1.381836
150.1633 1.755020
150.6454 2.758972
151.1275 4.240952
151.6096 5.715118
152.0917 6.997482
152.5738 8.181641
153.0560 9.482773
153.5381 10.96347
154.0202 12.33237
154.5023 13.17772
154.9844 13.45793
155.4665 14.06393
155.9487 15.55583
156.4308 17.41435
156.9129 19.31224
157.3950 21.19991
157.8771 22.98276
158.3592 24.41077
158.8414 25.15196
159.3235 26.39668
159.8056 28.67355
160.2877 31.38808
160.7698 34.10699
161.2519 36.64706
161.7341 39.01080
162.2162 41.17088
162.6983 42.92825
163.1804 44.75923
163.6625 46.58371
164.1446 48.55070
164.6268 50.83754
165.1089 53.56651
165.5910 56.67427
166.0731 59.79993
166.5552 63.12671
167.0373 66.26598
167.5195 68.94536
168.0016 71.38469
168.4837 74.04887
168.9658 77.26983
169.4479 81.01219
169.9300 84.37968
170.4122 87.30460
170.8943 90.01127
171.3764 92.59585
171.8585 95.04858
172.3406 97.33376
172.8227 99.44238
173.3049 101.3134
173.7870 102.8819
174.2691 104.0350
174.7512 104.9771
175.2333 105.8495
175.7154 106.6596
176.1976 107.4061
176.6797 108.2370
177.1618 109.0097
177.6439 109.2876
178.1260 108.8447
178.6081 107.9400
179.0903 106.9673
179.5724 105.7334
180.0545 104.4141
180.5366 102.8076
181.0187 100.7229
181.5008 98.51695
181.9830 96.38389
182.4651 94.16135
182.9472 91.61364
183.4293 89.01635
183.9114 86.33628
184.3935 83.48955
184.8757 80.68890
185.3578 78.08059
185.8399 75.67745
186.3220 73.40484
186.8041 70.73902
187.2862 66.90917
187.7684 63.24660
188.2505 60.45256
188.7326 58.31802
189.2147 56.14735
189.6968 53.46776
190.1789 50.24270
190.6611 47.35980
191.1432 45.02361
191.6253 42.82556
192.1074 40.68820
192.5895 38.60370
193.0716 36.56310
193.5538 34.58792
194.0359 32.67026
194.5180 30.77815
195.0001 28.82336
195.4822 26.96973
195.9643 25.32033
196.4465 23.85849
196.9286 22.48167
197.4107 21.12688
197.8928 19.80637
198.3749 18.33738
198.8570 16.47998
199.3392 14.67064
199.8213 13.15571
200.3034 11.96175
200.7855 11.06149
201.2676 10.51567
201.7497 10.34505
202.2319 9.946701
202.7140 9.099617
203.1961 8.151787
203.6782 7.386818
204.1603 6.837570
204.6424 6.372047
205.1246 5.885780
205.6067 5.389595
206.0888 4.906517
206.5709 4.494743
207.0530 4.074219
207.5351 3.490013
208.0173 2.672340
208.4994 1.902321
208.9815 1.427254
209.4636 1.160690
209.9457 0.9602970
210.4278 0.8501510
210.9100 0.7600560
211.3921 0.4849170
211.8742 0.1081850
212.3563 0.5986180
212.8384 0.6172100
213.3205 0.3760220
213.8027 0.2741240
214.2848 0.6831050
214.7669 1.381363
215.2490 1.492935
215.7311 0.5740360
216.2132 0.2570270
216.6953 0.5564420
217.1775 0.4558030
217.6596 0.1543120
218.1417 0.3283390
218.6238 0.9118420
219.1059 1.070511
219.5880 0.2774960
220.0702 0.2999570
220.5523 0.1519240
221.0344 0.4127810
221.5165 0.8789980
221.9986 0.8831180
222.4807 0.4873350
222.9629 0.2789230
223.4450 0.4051280
223.9271 0.5839770
224.4092 0.8759990
224.8913 1.170509
225.3734 1.274742
225.8556 1.037956
226.3377 0.5044100
226.8198 0.1810610
227.3019 0.3161930
227.7840 0.4099120
228.2661 0.4294200
228.7483 0.3282930
229.2304 2.2774000E-02
229.7125 0.7523500
230.1946 1.778725
230.6767 2.177193
231.1588 1.235336
231.6410 0.4976270
232.1231 0.4473720
232.6052 0.8739320
233.0873 1.329422
233.5694 1.539246
234.0515 1.552887
234.5337 1.734634
235.0158 2.295349
235.4979 2.760712
235.9800 2.932693
236.4621 2.902962
236.9442 2.887741
237.4264 3.020294
237.9085 3.244003
238.3906 3.293297
238.8727 2.971497
239.3548 2.732796
239.8369 2.799347
240.3191 3.072380
240.8012 3.292854
241.2833 3.300629
241.7654 3.208931
242.2475 3.356842
242.7296 3.847977
243.2118 4.362427
243.6939 4.806213
244.1760 5.172905
244.6581 5.436310
245.1402 5.573257
245.6223 5.604980
246.1045 5.572258
246.5866 5.445396
247.0687 5.355927
247.5508 5.392662
248.0329 5.524147
248.5150 5.630875
248.9972 5.643997
249.4793 5.657402
249.9614 5.834328
250.4435 6.209343
250.9256 6.516075
251.4077 6.530724
251.8899 6.326370
252.3720 6.243057
252.8541 6.447960
253.3362 6.699692
253.8183 6.685242
254.3004 6.407913
254.7826 6.218643
255.2647 6.459389
255.7468 7.019386
256.2289 7.284828
256.7110 6.896744
257.1931 6.535126
257.6753 6.389320
258.1574 7.329247
258.6395 7.965454
259.1216 8.304359
259.6037 7.484329
260.0858 8.157417
260.5680 8.230911
261.0501 8.279442
261.5322 9.161873
262.0143 8.509399
262.4964 9.459854
262.9785 9.624207
263.4607 9.614212
263.9428 9.778145
264.4249 10.32611
264.9070 10.73785
265.3891 10.64835
265.8712 10.26110
266.3534 9.989830
266.8355 10.12171
267.3176 10.56172
267.7997 10.92204
268.2818 11.26373
268.7639 11.40395
269.2461 11.14884
269.7282 10.69429
270.2103 10.33233
270.6924 10.25134
271.1745 10.42970
271.6566 10.71004
272.1388 10.47064
272.6209 11.11861
273.1030 11.44424
273.5851 11.53444
274.0672 10.51323
274.5493 10.99163
275.0315 10.86848
275.5136 10.71175
275.9957 11.35750
276.4778 10.23136
276.9599 10.20053
277.4420 10.58016
277.9242 11.02338
278.4063 11.37516
278.8884 11.56695
279.3705 11.52810
279.8526 11.25812
280.3347 10.85608
280.8169 10.15289
281.2990 9.423409
281.7811 8.901787
282.2632 8.631561
282.7453 8.473717
283.2274 8.263817
283.7096 8.075493
284.1917 7.730026
284.6738 7.007042
285.1559 6.267273
285.6380 5.710899
286.1201 5.380936
286.6023 5.232750
287.0844 5.264206
287.5665 5.568001
288.0486 5.696602
288.5307 5.521263
289.0128 5.272545
289.4950 5.084534
289.9771 4.940041
290.4592 4.702766
290.9413 4.197784
291.4234 3.383415
291.9055 2.806839
292.3877 2.599007
292.8698 2.497643
293.3519 2.480438
293.8340 2.501480
294.3161 2.492134
294.7982 2.401352
295.2804 2.236938
295.7625 2.099197
296.2446 2.086632
296.7267 1.990372
297.2088 1.676842
297.6909 1.275063
298.1731 0.9867250
298.6552 0.9270940
299.1373 1.031151
299.6194 1.057045
300.1015 0.9667890
300.5836 0.8372420
301.0658 0.5050960
301.5479 0.2071990
302.0300 0.2947850
302.5121 0.8902890
302.9942 1.667900
303.4763 1.928764
303.9585 1.060631
304.4406 0.5869830
304.9227 0.8593600
305.4048 1.293320
305.8869 1.406815
306.3690 1.097076
306.8512 0.6043780
307.3333 0.2503740
307.8154 5.7472002E-02
308.2975 3.3821002E-02
308.7796 2.1354999E-02
309.2617 6.9678999E-02
309.7439 0.2967070
310.2260 0.6158750
310.7081 0.8611530
311.1902 0.8426360
311.6723 0.4955370
312.1544 0.3628390
312.6366 0.6890790
313.1187 0.9569020
313.6008 0.9364320
314.0829 0.6849210
314.5650 0.3637620
315.0471 7.4913003E-02
315.5293 0.1729510
316.0114 0.2579500
316.4935 9.8040001E-03
316.9756 0.2107010
317.4577 0.3588560
317.9398 0.4264140
318.4220 0.3804630
318.9041 0.1969910
319.3862 5.0583001E-02
319.8683 0.1281360
320.3504 0.1149520
320.8326 0.3544460
321.3147 0.5967100
321.7968 0.8172070
322.2789 1.024078
322.7610 1.209633
323.2431 1.306206
323.7253 1.182121
324.2074 0.6443250
324.6895 0.2637250
325.1716 2.4277000E-02
325.6537 0.1423190
326.1358 0.1173100
326.6180 0.6874240
327.1001 1.162498
327.5822 1.055489
328.0643 0.1899030
328.5464 0.3678510
329.0285 0.5167850
329.5107 0.5030520
329.9928 0.3304290
330.4749 7.0450000E-02
330.9570 0.1392440
331.4391 0.1873780
331.9212 8.6898997E-02
332.4034 3.8688999E-02
332.8855 2.7930999E-02
333.3676 3.8582001E-02
333.8497 0.4483950
334.3318 0.9683760
334.8139 1.241020
335.2961 1.080505
335.7782 0.6581500
336.2603 0.4882510
336.7424 0.8255460
337.2245 1.044090
337.7066 1.011154
338.1888 0.8972470
338.6708 0.8634800
339.1530 0.9515300
339.6351 1.093033
340.1172 1.187225
340.5993 1.247704
341.0814 1.229042
341.5635 1.093697
342.0457 0.9223790
342.5278 0.6614690
343.0099 0.3746490
343.4920 0.2516330
343.9741 0.5052110
344.4562 1.161125
344.9384 1.710510
345.4205 2.307114
345.9026 2.622627
346.3847 2.322166
346.8668 1.698059
347.3489 1.277489
347.8311 1.408775
348.3132 1.930748
348.7953 2.186279
349.2774 1.990570
349.7595 1.798569
350.2416 1.633270
350.7238 1.541039
351.2059 1.597893
351.6880 1.827736
352.1701 2.124474
352.6522 2.311562
353.1343 2.356827
353.6165 2.384293
354.0986 2.526146
354.5807 2.565521
355.0628 2.264381
355.5449 1.667831
356.0270 1.116974
356.5092 0.9721070
356.9913 1.251183
357.4734 1.507103
357.9555 1.810738
358.4376 1.999504
358.9197 1.923943
359.4019 1.688492
359.8840 1.499603
360.3661 1.491547
360.8482 1.609100
361.3303 1.665955
361.8124 1.598244
362.2946 1.607376
362.7767 2.019066
363.2588 2.422485
363.7409 1.756699
364.2230 2.425209
364.7051 2.784134
365.1873 2.850990
365.6694 1.759453
366.1515 2.160896
366.6336 1.964081
367.1157 1.744431
367.5978 2.253296
368.0800 2.371170
368.5621 2.404083
369.0442 2.302170
369.5263 2.095161
370.0084 1.962540
370.4905 1.899780
370.9727 1.912651
371.4548 2.167053
371.9369 2.518875
372.4190 2.623688
372.9011 2.194328
373.3832 1.547798
373.8654 1.183884
374.3475 1.148178
374.8296 1.107483
375.3117 0.8660130
375.7938 0.5372920
376.2759 0.2796100
376.7581 0.1052020
377.2402 4.9510002E-03
377.7223 4.8679998E-03
378.2044 9.7015001E-02
378.6865 0.1907580
379.1686 0.2313770
379.6508 0.2861790
380.1329 0.5542140
380.6150 1.038513
381.0971 1.302818
381.5792 0.9825290
382.0613 0.4526900
382.5435 0.3195190
383.0256 0.6578830
383.5077 0.9876560
383.9898 0.8906480
384.4719 0.4660640
384.9540 0.3472600
385.4362 0.8822020
385.9183 1.429878
386.4004 1.577805
386.8825 1.399696
387.3646 1.112892
387.8467 0.7994920
388.3289 0.4915620
388.8110 0.2869110
389.2931 0.1316830
389.7752 0.1500930
390.2573 0.5321880
390.7394 1.029259
391.2216 1.346207
391.7037 1.430206
392.1858 1.379677
392.6679 1.335991
393.1500 1.311783
393.6321 1.247658
394.1143 1.129471
394.5964 0.9911500
395.0785 0.3697280
395.5606 1.107307
396.0427 1.539146
396.5248 1.682793
397.0070 0.6707000
397.4891 1.153877
397.9712 1.038147
398.4533 0.8957600
398.9354 1.585114
399.4175 0.7375260
399.8997 1.413582
400.3818 1.338631
400.8639 1.386856
401.3460 1.435822
401.8281 1.464096
402.3102 1.557480
402.7924 1.828201
403.2745 2.055092
403.7566 2.149086
404.2387 2.101410
404.7208 1.896973
405.2029 1.467194
405.6851 0.8837360
406.1672 0.7587890
406.6493 1.600906
407.1314 2.172607
407.6135 2.060463
408.0956 1.616241
408.5778 1.183807
409.0599 0.8840330
409.5420 0.7197570
410.0241 0.7251280
410.5062 0.9342190
410.9883 1.130814
411.4705 1.267906
411.9526 1.398239
412.4347 1.641495
412.9168 1.938278
413.3989 2.032753
413.8810 1.604607
414.3632 0.8196640
414.8453 0.2780840
415.3274 1.7890999E-02
415.8095 7.0679002E-02
416.2916 0.2535170
416.7737 0.7780760
417.2559 1.341606
417.7380 2.038292
418.2201 2.480934
418.7022 2.085625
419.1843 0.9569930
419.6664 9.9463999E-02
420.1486 0.1645360
420.6307 5.9241999E-02
421.1128 0.1919020
421.5949 0.5898280
422.0770 0.9248350
422.5591 1.132858
423.0413 1.229782
423.5234 1.237373
424.0055 1.158028
424.4876 0.9752810
424.9697 0.6433490
425.4518 0.1881410
425.9340 0.1980210
426.4161 0.6319500
426.8982 0.8788530
427.3803 0.7521290
427.8624 0.3669130
428.3445 7.8171000E-02
428.8267 0.5246050
429.3088 0.8962780
429.7909 1.057106
430.2730 0.9213100
430.7551 0.7393340
431.2372 0.4043660
431.7194 0.1067350
432.2015 1.8340999E-02
432.6836 0.1181110
433.1657 0.2521360
433.6478 0.3038790
434.1299 0.2759320
434.6121 0.1943360
435.0942 5.2551001E-02
435.5763 0.2228780
436.0584 0.3211290
436.5405 0.3045730
437.0226 3.9565999E-02
437.5048 0.4974900
437.9869 1.039833
438.4690 1.129196
438.9511 0.5895540
439.4332 0.1599200
439.9153 0.2445300
440.3975 0.4497600
440.8796 0.1973570
441.3617 0.3437190
441.8438 0.7261510
442.3259 0.6026310
442.8080 0.1427990
443.2902 5.6030001E-02
443.7723 0.1440810
444.2544 0.2493060
444.7365 0.1032870
445.2186 0.5266420
445.7007 0.6337740
446.1829 0.3360060
446.6650 4.8668001E-02
447.1471 0.2857360
447.6292 0.3822100
448.1113 0.3340230
448.5934 3.7094001E-02
449.0756 0.2006450
449.5577 1.0399000E-02
450.0398 0.4657290
450.5219 0.8092190
451.0040 0.7893220
451.4861 0.6757510
451.9683 0.7829900
452.4504 1.065254
452.9325 1.187988
453.4146 0.9647450
453.8967 0.5520860
454.3788 0.2763670
454.8610 0.1093060
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