#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:41:58 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1238 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000649.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000649
loop_
_publ_author_name
'Zubkova, N. V.'
'Pushcharovsky, D. Y.'
'Giester, G.'
'Tillmanns, E.'
'Pekov, I. V.'
'Kleimenov, D. A.'
_publ_section_title
;
 The crystal structure of arsentsumebite, Pb2Cu[(As,S)O4]2(OH) Locality:
 oxidation zone of the Berezovskoye gold deposit, Middle Urals, Russia
;
_journal_name_full               'Mineralogy and Petrology'
_journal_page_first              79
_journal_page_last               88
_journal_paper_doi               10.1007/s007100200016
_journal_volume                  75
_journal_year                    2002
_chemical_compound_source        R070629
_chemical_formula_sum            'As Cu H O9 Pb2 S'
_chemical_name_mineral           Arsentsumebite
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.29
_cell_angle_gamma                90
_cell_length_a                   7.804
_cell_length_b                   5.890
_cell_length_c                   8.964
_cell_volume                     381.246
_exptl_crystal_density_diffrn    6.359
_cod_original_formula_sum        'Pb2 Cu (As S) (O9 H)'
_cod_database_code               9009849
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R070629.rod
_rod_data_source.block           3500000
_rod_database.code               1000649
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009849 COD http://www.crystallography.net/cod/9009849.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
113.2559 0.0000000E+00
113.7380 51.58789
114.2202 2.847656
114.7023 35.37598
115.1844 133.9912
115.6665 220.6064
116.1486 245.8174
116.6307 214.0781
117.1129 195.6895
117.5950 192.0527
118.0771 198.8271
118.5592 222.1387
119.0413 263.7256
119.5234 294.0518
120.0056 272.5049
120.4877 215.9170
120.9698 171.6953
121.4519 155.4004
121.9340 161.0742
122.4161 175.1895
122.8982 195.0596
123.3804 227.2471
123.8625 282.1494
124.3446 354.9414
124.8267 421.4590
125.3088 472.0410
125.7909 508.8369
126.2731 506.4365
126.7552 398.4199
127.2373 291.5215
127.7194 240.4775
128.2015 253.3838
128.6837 300.0850
129.1658 337.0137
129.6479 356.0596
130.1300 375.9648
130.6121 417.3779
131.0942 453.0654
131.5764 448.6748
132.0585 390.7070
132.5406 300.0605
133.0227 248.5674
133.5048 283.1113
133.9869 308.1123
134.4691 319.2871
134.9512 311.9258
135.4333 281.0264
135.9154 218.5557
136.3975 127.7705
136.8796 67.48242
137.3618 44.64258
137.8439 38.86035
138.3260 40.47949
138.8081 49.45508
139.2902 72.82910
139.7723 128.1035
140.2545 211.8662
140.7366 250.8525
141.2187 201.7461
141.7008 123.0938
142.1829 80.78516
142.6650 84.99414
143.1472 105.4385
143.6293 104.4141
144.1114 84.06738
144.5935 76.91699
145.0756 100.9814
145.5577 144.2168
146.0399 176.5859
146.5220 194.0869
147.0041 196.4697
147.4862 178.4814
147.9683 140.4229
148.4504 106.4941
148.9326 101.9385
149.4147 129.9209
149.8968 153.5303
150.3789 165.8506
150.8610 173.0020
151.3431 169.2490
151.8252 157.2051
152.3074 151.9746
152.7895 191.0996
153.2716 329.7129
153.7537 396.1748
154.2358 338.9961
154.7179 246.2998
155.2001 185.0518
155.6822 200.9736
156.1643 266.6787
156.6464 319.1143
157.1285 375.6211
157.6106 409.6895
158.0928 408.8164
158.5749 387.8242
159.0570 360.7578
159.5391 331.7998
160.0212 311.4639
160.5033 324.5801
160.9855 375.3730
161.4676 435.6406
161.9497 455.3047
162.4318 434.4941
162.9139 434.9268
163.3960 490.4912
163.8782 609.8330
164.3603 662.2695
164.8424 578.0049
165.3245 463.6973
165.8066 403.6240
166.2887 403.9053
166.7709 425.3447
167.2530 423.2422
167.7351 400.8818
168.2172 393.2539
168.6993 426.7422
169.1814 466.6631
169.6636 460.3496
170.1457 389.6543
170.6278 315.0811
171.1099 328.3105
171.5920 405.7100
172.0741 447.9932
172.5563 377.9648
173.0384 239.9131
173.5205 173.0107
174.0026 240.4248
174.4847 325.9248
174.9668 315.1572
175.4490 215.7441
175.9311 122.5156
176.4132 110.1367
176.8953 176.0674
177.3774 231.8789
177.8595 254.6152
178.3417 269.0010
178.8238 295.9980
179.3059 336.5381
179.7880 367.9092
180.2701 357.1182
180.7522 289.6191
181.2344 240.6152
181.7165 231.6953
182.1986 237.6367
182.6807 247.5781
183.1628 258.0400
183.6449 265.8076
184.1271 264.2676
184.6092 247.4414
185.0913 233.0596
185.5734 231.0723
186.0555 227.9883
186.5376 206.8477
187.0198 160.8799
187.5019 105.6973
187.9840 82.15332
188.4661 132.3770
188.9482 163.0049
189.4303 153.8086
189.9125 125.5439
190.3946 105.2305
190.8767 107.1074
191.3588 123.1045
191.8409 113.4883
192.3230 32.21387
192.8052 23.51172
193.2873 16.35840
193.7694 27.09961
194.2515 57.67188
194.7336 43.26855
195.2157 8.918945
195.6979 27.33984
196.1800 23.37500
196.6621 63.59375
197.1442 51.94727
197.6263 2.458008
198.1084 38.51367
198.5906 36.88770
199.0727 3.839844
199.5548 24.93262
200.0369 9.643555
200.5190 8.959961
201.0011 14.38379
201.4833 6.095703
201.9654 13.16016
202.4475 49.44727
202.9296 98.10059
203.4117 122.2314
203.8938 101.2383
204.3760 67.20508
204.8581 53.31738
205.3402 62.60938
205.8223 63.66895
206.3044 13.51855
206.7865 68.86816
207.2687 112.9512
207.7508 62.06836
208.2329 17.98926
208.7150 26.29297
209.1971 60.97852
209.6792 148.9150
210.1614 145.0605
210.6435 81.87207
211.1256 30.66895
211.6077 28.70117
212.0898 55.14258
212.5719 61.58984
213.0541 35.08691
213.5362 11.38574
214.0183 22.25879
214.5004 55.72070
214.9825 81.79199
215.4646 87.04492
215.9468 72.46191
216.4289 37.67969
216.9110 37.97266
217.3931 104.4297
217.8752 137.7363
218.3573 141.5811
218.8395 126.9766
219.3216 81.63281
219.8037 11.32812
220.2858 6.395508
220.7679 86.82227
221.2500 172.7832
221.7322 190.6807
222.2143 152.9326
222.6964 105.4600
223.1785 84.54004
223.6606 91.26465
224.1427 97.65918
224.6249 103.9580
225.1070 109.6514
225.5891 112.7344
226.0712 114.4424
226.5533 118.6719
227.0354 130.0361
227.5176 150.0938
227.9997 165.7861
228.4818 169.8457
228.9639 175.4219
229.4460 191.0605
229.9281 214.3975
230.4103 235.5869
230.8924 243.4902
231.3745 234.9492
231.8566 229.2900
232.3387 223.8770
232.8208 222.8936
233.3030 233.2920
233.7851 252.0811
234.2672 267.7617
234.7493 266.5498
235.2314 241.6738
235.7135 223.0791
236.1957 205.4014
236.6778 196.8799
237.1599 209.5254
237.6420 239.8652
238.1241 268.9961
238.6062 272.0977
239.0884 232.5605
239.5705 223.7676
240.0526 280.7373
240.5347 335.6709
241.0168 343.3086
241.4989 302.0430
241.9811 244.2324
242.4632 206.9531
242.9453 198.7139
243.4274 186.2256
243.9095 162.8887
244.3916 140.7139
244.8738 128.6895
245.3559 126.9922
245.8380 127.2627
246.3201 118.3164
246.8022 90.06348
247.2843 87.81934
247.7665 135.2451
248.2486 189.2637
248.7307 217.6465
249.2128 217.3730
249.6949 208.1865
250.1770 212.1992
250.6592 234.7432
251.1413 247.3428
251.6234 254.4775
252.1055 250.8594
252.5876 225.9365
253.0697 179.2109
253.5519 130.1182
254.0340 102.4404
254.5161 97.87891
254.9982 105.3945
255.4803 131.8516
255.9624 162.1377
256.4445 194.8926
256.9267 230.0439
257.4088 250.9004
257.8909 233.4473
258.3730 163.1270
258.8551 134.2705
259.3372 184.8516
259.8194 254.4199
260.3015 298.1328
260.7836 309.6230
261.2657 298.4346
261.7478 266.5488
262.2299 208.8193
262.7121 179.6787
263.1942 219.3623
263.6763 262.5859
264.1584 243.0264
264.6405 153.3223
265.1227 58.95801
265.6048 24.26855
266.0869 56.70020
266.5690 87.06738
267.0511 101.8828
267.5332 113.3330
268.0154 148.6240
268.4975 210.5723
268.9796 257.2998
269.4617 239.9678
269.9438 158.1650
270.4259 120.0869
270.9081 164.6855
271.3902 231.6895
271.8723 277.7119
272.3544 298.8193
272.8365 300.3555
273.3186 280.4248
273.8008 243.2344
274.2829 224.9326
274.7650 245.9346
275.2471 270.5020
275.7292 265.7480
276.2113 233.8857
276.6935 213.6621
277.1756 236.7139
277.6577 296.1328
278.1398 335.4531
278.6219 329.5332
279.1040 327.1885
279.5862 376.3496
280.0683 469.4961
280.5504 544.5146
281.0325 558.4102
281.5146 522.7002
281.9967 499.0098
282.4789 484.2305
282.9610 483.5127
283.4431 512.9990
283.9252 565.8232
284.4073 601.9580
284.8894 597.1299
285.3716 561.0674
285.8537 528.1436
286.3358 481.9844
286.8179 458.6719
287.3000 486.9512
287.7821 558.1279
288.2643 640.3652
288.7464 729.3525
289.2285 811.5537
289.7106 854.5830
290.1927 836.0342
290.6748 822.3486
291.1570 849.9521
291.6391 908.4395
292.1212 966.0088
292.6033 1010.662
293.0854 1047.265
293.5675 1086.655
294.0497 1132.012
294.5318 1172.750
295.0139 1202.456
295.4960 1224.697
295.9781 1246.276
296.4602 1267.915
296.9424 1292.340
297.4245 1325.378
297.9066 1367.729
298.3887 1412.814
298.8708 1454.450
299.3529 1497.771
299.8351 1557.738
300.3172 1643.445
300.7993 1728.464
301.2814 1763.775
301.7635 1742.126
302.2456 1748.492
302.7278 1821.665
303.2099 1926.764
303.6920 2020.608
304.1741 2095.451
304.6562 2153.205
305.1383 2192.112
305.6205 2211.291
306.1026 2231.229
306.5847 2254.783
307.0668 2279.979
307.5489 2304.554
308.0310 2328.428
308.5132 2354.086
308.9953 2387.779
309.4774 2429.248
309.9595 2450.725
310.4416 2429.252
310.9237 2402.633
311.4059 2399.802
311.8880 2421.823
312.3701 2456.459
312.8522 2498.729
313.3343 2547.160
313.8164 2584.674
314.2986 2594.545
314.7807 2608.431
315.2628 2656.957
315.7449 2730.372
316.2270 2785.172
316.7091 2791.584
317.1913 2757.380
317.6734 2730.299
318.1555 2705.302
318.6376 2691.053
319.1197 2699.322
319.6018 2721.090
320.0840 2734.648
320.5661 2729.150
321.0482 2710.210
321.5303 2699.647
322.0124 2725.790
322.4945 2723.150
322.9767 2643.776
323.4588 2535.141
323.9409 2472.594
324.4230 2486.149
324.9051 2542.185
325.3872 2574.400
325.8694 2570.455
326.3515 2563.906
326.8336 2562.881
327.3157 2557.285
327.7978 2530.846
328.2799 2480.653
328.7621 2427.222
329.2442 2399.815
329.7263 2415.955
330.2084 2415.420
330.6905 2381.088
331.1726 2343.159
331.6548 2331.272
332.1369 2344.216
332.6190 2348.645
333.1011 2304.776
333.5832 2196.056
334.0653 2141.431
334.5475 2198.337
335.0296 2245.947
335.5117 2205.547
335.9938 2098.404
336.4759 2005.130
336.9580 1994.276
337.4402 2064.235
337.9223 2086.113
338.4044 2020.781
338.8865 1953.805
339.3686 1909.703
339.8507 1878.399
340.3329 1837.617
340.8150 1771.269
341.2971 1686.592
341.7792 1628.724
342.2613 1631.214
342.7434 1619.492
343.2256 1579.087
343.7077 1523.597
344.1898 1465.228
344.6719 1411.208
345.1540 1365.688
345.6361 1333.289
346.1183 1320.906
346.6004 1294.413
347.0825 1243.184
347.5646 1189.839
348.0467 1153.513
348.5288 1136.233
349.0110 1118.771
349.4931 1068.479
349.9752 966.4604
350.4573 906.6025
350.9394 952.8623
351.4215 989.6831
351.9037 953.1538
352.3858 852.7886
352.8679 744.1685
353.3500 672.7656
353.8321 635.3506
354.3142 615.5718
354.7964 639.7036
355.2785 650.0410
355.7606 610.1367
356.2427 541.7832
356.7248 488.1104
357.2069 475.7451
357.6891 491.6372
358.1712 506.5039
358.6533 532.8066
359.1354 529.2017
359.6175 451.6084
360.0996 347.4775
360.5818 268.6655
361.0639 231.5479
361.5460 226.1782
362.0281 254.9092
362.5102 325.9731
362.9923 360.3955
363.4745 302.1953
363.9566 214.5234
364.4387 159.1973
364.9208 144.7354
365.4029 143.0752
365.8850 134.5596
366.3672 121.0308
366.8493 111.4741
367.3314 106.0996
367.8135 108.4233
368.2956 128.0312
368.7777 163.2437
369.2599 186.7300
369.7420 185.0229
370.2241 165.1216
370.7062 135.7354
371.1883 96.15527
371.6704 56.12744
372.1526 19.96729
372.6347 10.90771
373.1168 28.08789
373.5989 29.10791
374.0810 17.22070
374.5631 14.97607
375.0453 63.46338
375.5274 98.33691
376.0095 100.6182
376.4916 75.24023
376.9737 47.34668
377.4558 1.388184
377.9380 29.66406
378.4201 26.11475
378.9022 0.1416020
379.3843 26.64355
379.8664 46.32178
380.3485 59.73486
380.8307 68.44727
381.3128 74.61035
381.7949 71.69189
382.2770 49.91650
382.7591 23.96484
383.2412 5.032715
383.7234 3.746582
384.2055 0.4824220
384.6876 17.67432
385.1697 53.24805
385.6518 94.49072
386.1339 168.8120
386.6161 223.0405
387.0982 211.6904
387.5803 154.9248
388.0624 115.0771
388.5445 143.5264
389.0266 229.1836
389.5088 250.9121
389.9909 134.6133
390.4730 35.59082
390.9551 15.69775
391.4372 36.27344
391.9193 48.51709
392.4015 62.09375
392.8836 72.43848
393.3657 68.34619
393.8478 41.80566
394.3299 20.49707
394.8120 4.985840
395.2942 2.225586
395.7763 4.944824
396.2584 25.86035
396.7405 47.70947
397.2226 63.97998
397.7047 74.75781
398.1869 56.89111
398.6690 14.41943
399.1511 87.80176
399.6332 147.3081
400.1153 187.1147
400.5974 192.0474
401.0796 136.0034
401.5617 44.82959
402.0438 30.57715
402.5259 94.09277
403.0080 126.1602
403.4901 93.41260
403.9723 27.68262
404.4544 24.51465
404.9365 53.56543
405.4186 70.77197
405.9007 80.64648
406.3828 84.87695
406.8650 93.39502
407.3471 111.3071
407.8292 132.9307
408.3113 154.2617
408.7934 181.7759
409.2755 182.6523
409.7577 115.6392
410.2398 27.99512
410.7219 9.539551
411.2040 15.67188
411.6861 57.88379
412.1682 73.00146
412.6504 56.94189
413.1325 41.58838
413.6146 19.43311
414.0967 4.857422
414.5788 6.168945
415.0609 21.99121
415.5431 50.89990
416.0252 95.54248
416.5073 146.9756
416.9894 162.9629
417.4715 101.6572
417.9536 54.58350
418.4358 25.96924
418.9179 18.04541
419.4000 36.85840
419.8821 82.89111
420.3642 143.3115
420.8463 199.9644
421.3285 252.8286
421.8106 301.2573
422.2927 358.2505
422.7748 399.6748
423.2569 394.5386
423.7390 358.5327
424.2212 344.3325
424.7033 404.7422
425.1854 522.7290
425.6675 588.2295
426.1496 567.1431
426.6317 550.0786
427.1139 565.9756
427.5960 607.4683
428.0781 668.3604
428.5602 750.3076
429.0423 841.2588
429.5244 934.8984
430.0066 1032.462
430.4887 1107.782
430.9708 1144.762
431.4529 1163.537
431.9350 1179.843
432.4171 1193.823
432.8993 1233.330
433.3814 1340.092
433.8635 1476.009
434.3456 1561.309
434.8277 1576.894
435.3098 1585.388
435.7920 1645.293
436.2741 1753.313
436.7562 1839.311
437.2383 1877.181
437.7204 1913.188
438.2025 1989.532
438.6847 2088.022
439.1668 2153.753
439.6489 2157.614
440.1310 2118.168
440.6131 2085.025
441.0952 2060.569
441.5774 2038.857
442.0595 2028.237
442.5416 2015.299
443.0237 1986.284
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