#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:42:14 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1242 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000652.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000652
loop_
_publ_author_name
'Moore, P. B.'
'Araki, T.'
_publ_section_title
;
 Armangite, Mn26[As6(OH)4O14][As6O18]2[CO3], a fluorite derivative
 structure
;
_journal_name_full               'American Mineralogist'
_journal_page_first              748
_journal_page_last               757
_journal_volume                  64
_journal_year                    1979
_chemical_compound_source        R100054
_chemical_formula_sum            'C As18 Mn26 O57'
_chemical_name_mineral           Armangite
_space_group_IT_number           147
_symmetry_space_group_name_Hall  '-P 3'
_symmetry_space_group_name_H-M   'P -3'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_length_a                   13.491
_cell_length_b                   13.491
_cell_length_c                   8.855
_cell_volume                     1395.750
_exptl_crystal_density_diffrn    4.403
_cod_original_cell_volume        1395.749
_cod_original_formula_sum        'C Mn26 As18 O57'
_cod_database_code               9000725
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R100054.rod
_rod_data_source.block           3500000
_rod_database.code               1000652
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9000725 COD http://www.crystallography.net/cod/9000725.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
91.53320 0.0000000E+00
92.01532 5.868530
92.49744 0.5834960
92.97955 5.326477
93.46167 14.43872
93.94379 17.79059
94.42590 17.98181
94.90802 17.20435
95.39014 16.35101
95.87225 15.23254
96.35437 14.69171
96.83649 15.29553
97.31860 16.91650
97.80072 19.52899
98.28284 22.58588
98.76495 25.50085
99.24707 28.24860
99.72919 31.27527
100.2113 33.86908
100.6934 34.98737
101.1755 35.34338
101.6577 36.39978
102.1398 39.51477
102.6219 45.03131
103.1040 50.53058
103.5861 56.58020
104.0682 62.10492
104.5504 65.97443
105.0325 68.31305
105.5146 70.73914
105.9967 75.43317
106.4788 83.34674
106.9609 90.53442
107.4431 96.22705
107.9252 101.0446
108.4073 105.7602
108.8894 110.5287
109.3715 115.5200
109.8536 121.2058
110.3358 127.8907
110.8179 134.0284
111.3000 138.2177
111.7821 140.7149
112.2642 144.0858
112.7463 150.5159
113.2285 157.5653
113.7106 162.6852
114.1927 165.1376
114.6748 166.4371
115.1569 168.7511
115.6390 172.7015
116.1212 176.2031
116.6033 178.9653
117.0854 180.9078
117.5675 181.9639
118.0496 182.5312
118.5317 183.0971
119.0139 185.0680
119.4960 190.3782
119.9781 195.6339
120.4602 199.6152
120.9423 202.4185
121.4244 203.6328
121.9066 202.9874
122.3887 200.6238
122.8708 197.6849
123.3529 194.2375
123.8350 190.0455
124.3171 184.7119
124.7993 178.3918
125.2814 171.9182
125.7635 166.1981
126.2456 161.4442
126.7277 156.3765
127.2098 150.5292
127.6920 144.5607
128.1741 139.1704
128.6562 134.5806
129.1383 130.2945
129.6204 125.8776
130.1025 121.3488
130.5847 116.3747
131.0668 110.4347
131.5489 103.8539
132.0310 97.71121
132.5131 91.86121
132.9952 86.98474
133.4774 83.90518
133.9595 82.59933
134.4416 81.27826
134.9237 78.25116
135.4058 73.26883
135.8879 68.20190
136.3701 63.08096
136.8522 58.21078
137.3343 53.95041
137.8164 50.33298
138.2985 46.95938
138.7806 43.08017
139.2628 38.41199
139.7449 33.70245
140.2270 28.54462
140.7091 23.58304
141.1912 19.53833
141.6733 16.75381
142.1555 14.77921
142.6376 12.13535
143.1197 7.865021
143.6018 3.943420
144.0839 0.4887390
144.5660 2.477844
145.0482 4.861847
145.5303 6.526917
146.0124 7.622528
146.4945 9.335571
146.9766 12.77631
147.4587 15.63004
147.9409 16.68542
148.4230 16.19171
148.9051 15.36005
149.3872 14.61719
149.8693 14.24243
150.3514 13.42029
150.8336 11.77634
151.3157 9.781036
151.7978 7.645172
152.2799 5.313995
152.7620 3.247955
153.2441 2.300507
153.7263 1.850586
154.2084 0.7998350
154.6905 1.306061
155.1726 4.242584
155.6547 7.602386
156.1368 11.55347
156.6190 15.63181
157.1011 19.31479
157.5832 22.90463
158.0653 27.05853
158.5474 32.36563
159.0295 38.73010
159.5117 44.87204
159.9938 50.63974
160.4759 56.34589
160.9580 61.90128
161.4401 67.44388
161.9222 73.24600
162.4044 79.54672
162.8865 86.42035
163.3686 93.56812
163.8507 100.6575
164.3328 108.2967
164.8149 117.1419
165.2971 127.0333
165.7792 136.9128
166.2613 145.5721
166.7434 152.3594
167.2255 159.6850
167.7076 167.8220
168.1898 176.2535
168.6719 184.6035
169.1540 192.8261
169.6361 201.0305
170.1182 209.3823
170.6003 217.9088
171.0825 226.5581
171.5646 235.5395
172.0467 244.5446
172.5288 253.2049
173.0109 261.4037
173.4930 269.3104
173.9752 277.1550
174.4573 284.8983
174.9394 292.7861
175.4215 301.5190
175.9036 310.4709
176.3857 318.1683
176.8679 324.1535
177.3500 328.7893
177.8321 332.5558
178.3142 335.4265
178.7963 338.1188
179.2784 341.3266
179.7606 344.9236
180.2427 347.6698
180.7248 348.9672
181.2069 349.4337
181.6890 349.8998
182.1711 350.4551
182.6533 350.1611
183.1354 347.7321
183.6175 342.8642
184.0996 338.2881
184.5817 335.1510
185.0638 332.1661
185.5460 328.7566
186.0281 324.7755
186.5102 320.1595
186.9923 314.5796
187.4744 307.3769
187.9565 300.9901
188.4387 296.2194
188.9208 291.9314
189.4029 287.3780
189.8850 282.2980
190.3671 276.9900
190.8492 271.8684
191.3314 266.7820
191.8135 262.2890
192.2956 258.6868
192.7777 255.4987
193.2598 252.5049
193.7419 249.6028
194.2241 246.5061
194.7062 242.5316
195.1883 236.0835
195.6704 230.5513
196.1525 226.8302
196.6346 223.8146
197.1168 220.1502
197.5989 215.2315
198.0810 209.5178
198.5631 204.4023
199.0452 200.4839
199.5273 196.3336
200.0095 191.5299
200.4916 186.3740
200.9737 181.2832
201.4558 176.3795
201.9379 171.6183
202.4200 166.8844
202.9022 162.0694
203.3843 157.5545
203.8664 153.7160
204.3485 150.2946
204.8306 146.5299
205.3127 142.0120
205.7949 137.3453
206.2770 133.7685
206.7591 131.7689
207.2412 129.7352
207.7233 126.2946
208.2054 121.7760
208.6876 118.2629
209.1697 117.1655
209.6518 117.1324
210.1339 116.0117
210.6160 113.3340
211.0981 110.5813
211.5803 108.9115
212.0624 108.3656
212.5445 108.4641
213.0266 109.6830
213.5087 110.9513
213.9908 111.1551
214.4730 109.9982
214.9551 108.4613
215.4372 107.7207
215.9193 107.9373
216.4014 107.9337
216.8836 106.8512
217.3657 105.6886
217.8478 105.2397
218.3299 105.7139
218.8120 106.4026
219.2941 106.3244
219.7763 105.2800
220.2584 104.1023
220.7405 102.7567
221.2226 101.4368
221.7047 100.3038
222.1868 99.39453
222.6690 98.57877
223.1511 97.74579
223.6332 97.17554
224.1153 95.85663
224.5974 93.14200
225.0795 90.13480
225.5617 87.57019
226.0438 85.67242
226.5259 84.25449
227.0080 83.07864
227.4901 82.66061
227.9722 81.50302
228.4544 78.90701
228.9365 76.06744
229.4186 74.04269
229.9007 73.09067
230.3828 72.59518
230.8649 71.45908
231.3471 68.94020
231.8292 66.92361
232.3113 65.69502
232.7934 64.76523
233.2755 63.75250
233.7576 62.54880
234.2398 61.22267
234.7219 59.91916
235.2040 58.59955
235.6861 57.37561
236.1682 56.49338
236.6503 55.57356
237.1325 54.09657
237.6146 51.96945
238.0967 49.80238
238.5788 48.57268
239.0609 48.93265
239.5430 48.80315
240.0252 47.82707
240.5073 46.48157
240.9894 45.13425
241.4715 43.87552
241.9536 42.93195
242.4357 42.68510
242.9179 43.34906
243.4000 43.80415
243.8821 43.68564
244.3642 43.39276
244.8463 43.45230
245.3284 43.98352
245.8106 44.52310
246.2927 44.47772
246.7748 43.86458
247.2569 43.35715
247.7390 42.88490
248.2211 42.58337
248.7033 42.72316
249.1854 43.38321
249.6675 44.04590
250.1496 44.10085
250.6317 43.67874
251.1138 43.49216
251.5960 43.85982
252.0781 44.46562
252.5602 44.91089
253.0423 45.14848
253.5244 45.20299
254.0065 44.92415
254.4887 44.45610
254.9708 44.25127
255.4529 44.76474
255.9350 45.49310
256.4171 45.62474
256.8992 44.99684
257.3813 44.37119
257.8635 44.59801
258.3456 45.23392
258.8277 45.42102
259.3098 44.50208
259.7919 43.21478
260.2740 42.67697
260.7562 43.04092
261.2383 43.51793
261.7204 43.85776
262.2025 43.98721
262.6846 43.71733
263.1667 42.82373
263.6489 41.72038
264.1310 41.00667
264.6131 40.76375
265.0952 40.54396
265.5773 40.11714
266.0594 39.63235
266.5416 39.18941
267.0237 38.77605
267.5058 38.51654
267.9879 38.71472
268.4700 39.54630
268.9521 40.03101
269.4343 39.41490
269.9164 38.52974
270.3985 38.03342
270.8806 38.10530
271.3627 38.35594
271.8448 38.17795
272.3270 37.38625
272.8091 37.10007
273.2912 38.10132
273.7733 39.38306
274.2554 40.36589
274.7375 40.94907
275.2197 41.36324
275.7018 41.86476
276.1839 42.47981
276.6660 43.01437
277.1481 43.03751
277.6302 43.27986
278.1124 44.43019
278.5945 46.38246
279.0766 48.16609
279.5587 48.82745
280.0408 48.29346
280.5229 47.33459
281.0051 45.67998
281.4872 43.82169
281.9693 41.78482
282.4514 39.68422
282.9335 37.78308
283.4156 36.50723
283.8978 35.88548
284.3799 34.50397
284.8620 31.38138
285.3441 28.44920
285.8262 26.61896
286.3083 25.50867
286.7905 24.17224
287.2726 21.79938
287.7547 18.56375
288.2368 16.27771
288.7189 15.92746
289.2010 15.40460
289.6832 13.89598
290.1653 11.90939
290.6474 10.23880
291.1295 9.380157
291.6116 9.128937
292.0938 8.681870
292.5759 7.954269
293.0580 7.138428
293.5401 6.189423
294.0222 5.213669
294.5043 4.371368
294.9865 3.740280
295.4686 3.193207
295.9507 2.375183
296.4328 0.9423070
296.9149 0.1386570
297.3970 0.5710750
297.8792 0.7575530
298.3613 1.015640
298.8434 1.451721
299.3255 1.989403
299.8076 2.531296
300.2897 3.179993
300.7719 3.577698
301.2540 3.608070
301.7361 3.505753
302.2182 3.322853
302.7003 3.118713
303.1824 3.063759
303.6646 3.442978
304.1467 4.468117
304.6288 5.140724
305.1109 5.405922
305.5930 5.371964
306.0751 4.884521
306.5573 4.112534
307.0394 3.491005
307.5215 3.401352
308.0036 3.843094
308.4857 4.196968
308.9678 4.677681
309.4500 5.010490
309.9321 5.015038
310.4142 4.729103
310.8963 4.280762
311.3784 3.726112
311.8605 3.107758
312.3427 2.628395
312.8248 2.587715
313.3069 2.340813
313.7890 1.490982
314.2711 0.4338530
314.7532 0.2734070
315.2354 0.3392720
315.7175 2.4673000E-02
316.1996 0.1039200
316.6817 0.9642640
317.1638 1.613464
317.6459 1.770638
318.1281 1.785545
318.6102 2.014610
319.0923 2.557884
319.5744 3.184410
320.0565 3.490021
320.5386 3.295486
321.0208 3.187111
321.5029 3.050995
321.9850 3.091087
322.4671 3.463570
322.9492 4.168877
323.4313 5.075066
323.9135 6.104645
324.3956 7.335426
324.8777 8.275558
325.3598 8.656952
325.8419 8.996132
326.3240 9.534187
326.8062 10.20805
327.2883 10.78875
327.7704 11.06320
328.2525 11.05962
328.7346 11.27699
329.2167 11.72034
329.6989 12.41982
330.1810 13.74701
330.6631 15.25091
331.1452 16.23244
331.6273 16.27820
332.1094 15.69255
332.5916 15.42672
333.0737 15.69718
333.5558 15.93257
334.0379 15.89880
334.5200 15.85598
335.0021 16.12572
335.4843 16.79976
335.9664 17.56331
336.4485 17.91592
336.9306 17.78653
337.4127 17.44362
337.8948 16.48811
338.3770 15.65508
338.8591 15.50299
339.3412 16.00739
339.8233 16.63016
340.3055 16.82399
340.7876 16.54626
341.2697 16.26582
341.7518 15.92761
342.2339 15.64849
342.7160 15.64044
343.1982 15.73719
343.6803 15.51325
344.1624 14.50313
344.6445 12.96962
345.1266 12.30786
345.6087 13.11039
346.0909 13.81807
346.5730 14.08165
347.0551 13.92562
347.5372 13.26289
348.0193 11.95055
348.5014 10.46700
348.9836 9.735611
349.4657 9.989845
349.9478 10.23629
350.4299 10.23312
350.9120 10.11229
351.3941 10.00948
351.8763 9.944366
352.3584 9.713760
352.8405 8.919060
353.3226 7.528511
353.8047 6.675903
354.2868 6.955009
354.7690 7.337517
355.2511 7.118576
355.7332 6.413422
356.2153 5.724670
356.6974 5.484924
357.1795 5.527679
357.6617 5.176102
358.1438 4.232140
358.6259 3.288467
359.1080 2.700264
359.5901 2.354149
360.0722 2.084915
360.5544 1.871132
361.0365 1.656342
361.5186 1.347862
362.0007 0.9001460
362.4828 0.3615490
362.9649 0.4237210
363.4471 1.130775
363.9292 1.269951
364.4113 0.6324160
364.8934 6.8145998E-02
365.3755 0.6276780
365.8576 2.044189
366.3398 2.500114
366.8219 1.049210
367.3040 0.6859360
367.7861 0.8422780
368.2682 0.3998340
368.7503 1.474648
369.2325 1.808609
369.7146 1.556999
370.1967 0.8865890
370.6788 0.2286530
371.1609 1.354538
371.6430 2.234207
372.1252 2.892509
372.6073 3.323967
373.0894 3.169159
373.5715 2.975395
374.0536 3.171745
374.5357 3.779594
375.0179 4.725693
375.5000 6.090775
375.9821 7.617241
376.4642 8.718628
376.9463 9.263565
377.4284 9.772774
377.9106 10.39754
378.3927 11.10426
378.8748 11.77405
379.3569 12.34759
379.8390 13.11418
380.3211 14.64400
380.8033 17.19917
381.2854 18.87955
381.7675 18.96024
382.2496 18.53455
382.7317 18.33168
383.2138 18.43393
383.6960 18.73714
384.1781 19.16298
384.6602 19.71906
385.1423 20.54163
385.6244 21.78101
386.1065 23.05928
386.5887 24.35852
387.0708 25.58998
387.5529 26.63216
388.0350 27.43533
388.5171 28.00827
388.9992 28.36262
389.4814 28.24898
389.9635 28.27892
390.4456 28.22326
390.9277 28.46223
391.4098 29.64826
391.8919 31.66391
392.3741 33.45410
392.8562 33.79153
393.3383 32.37237
393.8204 31.87990
394.3025 33.23152
394.7846 34.48627
395.2668 34.95267
395.7489 34.84120
396.2310 34.59557
396.7131 34.45411
397.1952 34.44926
397.6773 34.71295
398.1595 35.52914
398.6416 36.13598
399.1237 36.30479
399.6058 36.33012
400.0879 36.49841
400.5700 36.86300
401.0522 37.21353
401.5343 37.25119
402.0164 36.89808
402.4985 36.66544
402.9806 36.69475
403.4627 36.74785
403.9449 36.75906
404.4270 36.70801
404.9091 36.57834
405.3912 36.39328
405.8733 36.09998
406.3554 35.50595
406.8376 34.49614
407.3197 33.47612
407.8018 32.38272
408.2839 31.45953
408.7660 31.05015
409.2481 31.29018
409.7303 31.73390
410.2124 32.08035
410.6945 32.30688
411.1766 32.04553
411.6587 30.90193
412.1408 29.66239
412.6230 29.10197
413.1051 29.13684
413.5872 29.18739
414.0693 28.99361
414.5514 28.67551
415.0335 28.47368
415.5157 28.42352
415.9978 28.20236
416.4799 27.43779
416.9620 26.37112
417.4441 25.72971
417.9262 25.60071
418.4084 25.81981
418.8905 26.44191
419.3726 27.34479
419.8547 28.27350
420.3368 29.18709
420.8189 29.88744
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