#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:42:22 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1244 $
#$URL: svn://172.16.1.111/rod/cif/1/00/06/1000654.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1000654
loop_
_publ_author_name
'Zubkova, N. V.'
'Pushcharovsky, D. Y.'
'Giester, G.'
'Tillmanns, E.'
'Pekov, I. V.'
'Kleimenov, D. A.'
_publ_section_title
;
 The crystal structure of arsentsumebite, Pb2Cu[(As,S)O4]2(OH) Locality:
 oxidation zone of the Berezovskoye gold deposit, Middle Urals, Russia
;
_journal_name_full               'Mineralogy and Petrology'
_journal_page_first              79
_journal_page_last               88
_journal_paper_doi               10.1007/s007100200016
_journal_volume                  75
_journal_year                    2002
_chemical_compound_source        R110041
_chemical_formula_sum            'As Cu H O9 Pb2 S'
_chemical_name_mineral           Arsentsumebite
_space_group_IT_number           11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.29
_cell_angle_gamma                90
_cell_length_a                   7.804
_cell_length_b                   5.890
_cell_length_c                   8.964
_cell_volume                     381.246
_exptl_crystal_density_diffrn    6.359
_cod_original_formula_sum        'Pb2 Cu (As S) (O9 H)'
_cod_database_code               9009849
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110041.rod
_rod_data_source.block           3500000
_rod_database.code               1000654
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009849 COD http://www.crystallography.net/cod/9009849.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
199.5977 0.0000000E+00
200.0798 0.5738980
200.5619 0.2239380
201.0440 5.7647999E-02
201.5261 0.3557590
202.0082 0.8317870
202.4904 1.358231
202.9725 1.923721
203.4546 2.600357
203.9367 2.970779
204.4188 3.317200
204.9009 3.954666
205.3831 4.997818
205.8652 5.236237
206.3473 4.134003
206.8294 3.122940
207.3115 3.217941
207.7936 4.485977
208.2758 6.339462
208.7579 7.374588
209.2400 6.181732
209.7221 5.657104
210.2042 6.129044
210.6863 7.609772
211.1685 9.662292
211.6506 11.73869
212.1327 13.55544
212.6148 14.72992
213.0969 15.89648
213.5790 15.02551
214.0612 13.28329
214.5433 11.40499
215.0254 9.714417
215.5075 8.099129
215.9896 6.517403
216.4717 4.858711
216.9539 2.609123
217.4360 1.640251
217.9181 3.277176
218.4002 5.534950
218.8823 6.458595
219.3644 5.682350
219.8466 4.026260
220.3287 2.524994
220.8108 1.155968
221.2929 0.1940460
221.7750 0.2104640
222.2571 0.2194820
222.7393 7.6812997E-02
223.2214 0.7207870
223.7035 1.447273
224.1856 1.927956
224.6677 2.037521
225.1498 1.663727
225.6320 8.1878997E-02
226.1141 1.936211
226.5962 1.970795
227.0783 1.251442
227.5604 4.896332
228.0425 6.489189
228.5247 6.873230
229.0068 6.300407
229.4889 5.295280
229.9710 4.667763
230.4531 4.981865
230.9352 5.650864
231.4174 6.680435
231.8995 7.131477
232.3816 6.864868
232.8637 6.666084
233.3458 6.880806
233.8279 7.393272
234.3101 7.813812
234.7922 8.052139
235.2743 8.344078
235.7564 8.698471
236.2385 9.186821
236.7206 10.01733
237.2028 11.73390
237.6849 13.91046
238.1670 14.54958
238.6491 12.26976
239.1312 10.50330
239.6133 11.17047
240.0955 13.16720
240.5776 14.58874
241.0597 14.13082
241.5418 12.25182
242.0239 11.19441
242.5060 11.50492
242.9882 11.96107
243.4703 12.41417
243.9524 12.72296
244.4345 12.68697
244.9166 12.16168
245.3987 11.23823
245.8809 10.38458
246.3630 10.05018
246.8451 9.151421
247.3272 6.728714
247.8093 3.847717
248.2914 1.975990
248.7736 1.961037
249.2557 3.308479
249.7378 4.018303
250.2199 3.817940
250.7020 3.225327
251.1841 1.729477
251.6663 8.2099997E-02
252.1484 0.6786500
252.6305 3.6750998E-02
253.1126 1.438072
253.5947 1.944740
254.0768 4.7867000E-02
254.5590 1.128387
255.0411 0.7822420
255.5232 0.1351010
256.0053 0.4756770
256.4874 0.2423020
256.9695 1.501595
257.4517 1.720734
257.9338 0.1183780
258.4159 1.005440
258.8980 0.3089290
259.3801 1.073128
259.8622 2.416290
260.3444 3.446594
260.8265 3.976349
261.3086 3.599953
261.7907 1.062561
262.2728 0.3729250
262.7549 0.5044630
263.2371 1.925629
263.7192 2.042503
264.2013 0.3841860
264.6834 2.101768
265.1655 4.094795
265.6476 5.573524
266.1298 6.435089
266.6119 6.067665
267.0940 5.412193
267.5761 5.317604
268.0582 5.954620
268.5403 7.043221
269.0225 8.376518
269.5046 10.10129
269.9867 11.27632
270.4688 11.36047
270.9509 11.19090
271.4330 11.43860
271.9152 12.18690
272.3973 13.26589
272.8794 14.63195
273.3615 16.30828
273.8436 17.56992
274.3257 18.29016
274.8079 18.66167
275.2900 18.19204
275.7721 17.08728
276.2542 17.40619
276.7363 21.40086
277.2184 28.48301
277.7006 33.20486
278.1827 33.89912
278.6648 33.49360
279.1469 33.69894
279.6290 34.54134
280.1111 35.82985
280.5933 37.55026
281.0754 39.66180
281.5575 41.86285
282.0396 44.10925
282.5217 46.45895
283.0038 48.97218
283.4860 51.57642
283.9681 54.16481
284.4502 56.92336
284.9323 59.86208
285.4144 62.45193
285.8965 64.29842
286.3787 66.60784
286.8608 70.47816
287.3429 75.45034
287.8250 79.78331
288.3071 82.47308
288.7892 84.93126
289.2714 89.43372
289.7535 96.21385
290.2356 102.6656
290.7177 107.1904
291.1998 110.4604
291.6819 114.2591
292.1641 118.9444
292.6462 124.3384
293.1283 130.4981
293.6104 137.3082
294.0925 143.9862
294.5746 149.8779
295.0568 155.4684
295.5389 161.7758
296.0210 169.0380
296.5031 176.6094
296.9852 183.8837
297.4673 191.0294
297.9495 198.6345
298.4316 207.2120
298.9137 216.1920
299.3958 224.5500
299.8779 232.0804
300.3600 239.8910
300.8422 248.8664
301.3243 258.5990
301.8064 268.3482
302.2885 278.1883
302.7706 287.8800
303.2527 297.0020
303.7349 305.5304
304.2170 314.4439
304.6991 325.6073
305.1812 336.6502
305.6633 344.0142
306.1454 346.1405
306.6276 347.2875
307.1097 351.6726
307.5918 359.0338
308.0739 365.0418
308.5560 367.9638
309.0381 368.9936
309.5203 370.0450
310.0024 371.3195
310.4845 370.9368
310.9666 366.5045
311.4487 358.8645
311.9308 352.4688
312.4130 348.8990
312.8951 345.7679
313.3772 340.8567
313.8593 334.3184
314.3414 327.4464
314.8235 320.3741
315.3057 313.5347
315.7878 308.2843
316.2699 305.2859
316.7520 302.1079
317.2341 296.8393
317.7162 290.1690
318.1984 283.2773
318.6805 275.5255
319.1626 267.8585
319.6447 262.5898
320.1268 260.0915
320.6089 258.2443
321.0911 256.1360
321.5732 253.9316
322.0553 251.8393
322.5374 249.7474
323.0195 247.6265
323.5016 245.4744
323.9838 243.3490
324.4659 241.7502
324.9480 241.0261
325.4301 240.6873
325.9122 240.0150
326.3943 238.8298
326.8765 238.3447
327.3586 239.8808
327.8407 243.0664
328.3228 245.7572
328.8049 247.2249
329.2870 248.3830
329.7692 250.0854
330.2513 252.2952
330.7334 254.8237
331.2155 257.9641
331.6976 261.3169
332.1797 264.0040
332.6619 265.9678
333.1440 267.1638
333.6261 267.1216
334.1082 266.2572
334.5903 265.4832
335.0724 264.8702
335.5546 264.5965
336.0367 265.2196
336.5188 266.8686
337.0009 268.0055
337.4830 267.3829
337.9651 265.7487
338.4473 264.6496
338.9294 264.9109
339.4115 264.6881
339.8936 262.4360
340.3757 258.3069
340.8578 253.4386
341.3400 247.9511
341.8221 242.1630
342.3042 236.6455
342.7863 231.4810
343.2684 226.0230
343.7505 219.7383
344.2327 212.9295
344.7148 206.3699
345.1969 200.3053
345.6790 194.2963
346.1611 187.7186
346.6432 180.6730
347.1254 173.7579
347.6075 167.1705
348.0896 160.7857
348.5717 154.5988
349.0538 148.5874
349.5359 142.6452
350.0181 136.7383
350.5002 130.8068
350.9823 124.6444
351.4644 117.9759
351.9465 111.3343
352.4286 104.7748
352.9108 98.44273
353.3929 92.95521
353.8750 88.79339
354.3571 85.54544
354.8392 82.17477
355.3214 78.68880
355.8035 75.10700
356.2856 71.28167
356.7677 67.40480
357.2498 63.84561
357.7319 60.72142
358.2141 57.84690
358.6962 54.98175
359.1783 52.15250
359.6604 49.16532
360.1425 45.93234
360.6246 42.55606
361.1068 38.71529
361.5889 34.49471
362.0710 31.29561
362.5531 30.58748
363.0352 32.32397
363.5173 32.72603
363.9995 31.49635
364.4816 29.38367
364.9637 25.99991
365.4458 21.96836
365.9279 18.94604
366.4100 17.95654
366.8922 18.18102
367.3743 16.93876
367.8564 13.01373
368.3385 9.452049
368.8206 6.240662
369.3027 3.755424
369.7849 2.926704
370.2670 3.914886
370.7491 5.182495
371.2312 4.496956
371.7133 0.8677140
372.1954 1.740593
372.6776 2.945877
373.1597 3.538643
373.6418 3.550407
374.1239 3.294167
374.6060 3.740883
375.0881 5.928490
375.5703 9.728165
376.0524 10.95208
376.5345 6.906418
377.0166 3.440521
377.4987 1.977478
377.9808 1.872429
378.4630 2.237694
378.9451 2.670151
379.4272 3.004959
379.9093 2.784050
380.3914 1.216026
380.8735 0.4444430
381.3557 1.468857
381.8378 2.582809
382.3199 2.487328
382.8020 1.036789
383.2841 1.028923
383.7662 2.941734
384.2484 4.703545
384.7305 6.340416
385.2126 7.935661
385.6947 9.317284
386.1768 10.47808
386.6589 11.37256
387.1411 11.86212
387.6232 11.77627
388.1053 11.36440
388.5874 11.55713
389.0695 12.67414
389.5516 13.81275
390.0338 15.03175
390.5159 16.03904
390.9980 16.65903
391.4801 16.83521
391.9622 16.36037
392.4443 14.51684
392.9265 11.03580
393.4086 8.845055
393.8907 9.217705
394.3728 10.18465
394.8549 11.07298
395.3370 11.66440
395.8192 11.40630
396.3013 9.196693
396.7834 5.881172
397.2655 4.458809
397.7476 5.564377
398.2297 6.924309
398.7119 7.449524
399.1940 7.482689
399.6761 7.414818
400.1582 7.359840
400.6403 7.191658
401.1224 6.488358
401.6046 5.316238
402.0867 4.980179
402.5688 6.171181
403.0509 8.061867
403.5330 9.711540
404.0151 11.12441
404.4973 12.33486
404.9794 13.57942
405.4615 14.56966
405.9436 14.46864
406.4257 13.01304
406.9078 11.87605
407.3900 12.81368
407.8721 15.35491
408.3542 16.91993
408.8363 16.60300
409.3184 15.91879
409.8005 15.59805
410.2827 15.67443
410.7648 16.42435
411.2469 18.20002
411.7290 20.25841
412.2111 20.73979
412.6932 19.02271
413.1754 17.56783
413.6575 16.53995
414.1396 16.10822
414.6217 16.77669
415.1038 18.51400
415.5859 20.23448
416.0681 20.74189
416.5502 19.83695
417.0323 20.00483
417.5144 22.10548
417.9965 24.19437
418.4786 25.68884
418.9608 26.57012
419.4429 26.79460
419.9250 26.30180
420.4071 25.45785
420.8892 25.33730
421.3713 27.22956
421.8535 27.84103
422.3356 25.50453
422.8177 23.03482
423.2998 22.55042
423.7819 24.32661
424.2640 27.38892
424.7462 30.86390
425.2283 34.79417
425.7104 38.67581
426.1925 41.85255
426.6746 45.73936
427.1567 51.19009
427.6389 57.50836
428.1210 63.53609
428.6031 68.67812
429.0852 73.46097
429.5673 78.73243
430.0494 84.21371
430.5316 90.80477
431.0137 99.40044
431.4958 108.8090
431.9779 118.6438
432.4600 128.7226
432.9421 138.2224
433.4243 145.5370
433.9064 151.6523
434.3885 160.9110
434.8706 174.4779
435.3527 188.7325
435.8348 201.2233
436.3170 212.8397
436.7991 225.3711
437.2812 240.0138
437.7633 254.5916
438.2454 266.9832
438.7275 277.4176
439.2097 287.5367
439.6918 298.3066
440.1739 308.3878
440.6560 315.9037
441.1381 321.1263
441.6202 323.7421
442.1024 323.7591
442.5845 321.0787
443.0666 315.2331
443.5487 306.2874
444.0308 295.4092
444.5129 283.2578
444.9951 269.9152
445.4772 255.8117
445.9593 239.7275
446.4414 224.5038
446.9235 211.5576
447.4056 199.8525
447.8878 187.4963
448.3699 173.8778
448.8520 160.4318
449.3341 149.3587
449.8162 141.6153
450.2983 133.7658
450.7805 125.4106
451.2626 117.3490
451.7447 109.7995
452.2268 102.8713
452.7089 96.60201
453.1910 91.02171
453.6732 86.19007
454.1553 82.53889
454.6374 81.08026
455.1195 79.08226
455.6016 75.61163
456.0837 71.83755
456.5659 68.92066
457.0480 66.91467
457.5301 64.94417
458.0122 61.65755
458.4943 57.10838
458.9764 54.77229
459.4586 56.43942
459.9407 57.82273
460.4228 56.50976
460.9049 53.45476
461.3870 50.28236
461.8691 47.46096
462.3513 44.91888
462.8334 42.70418
463.3155 40.91679
463.7976 39.11985
464.2797 37.05782
464.7618 34.92435
465.2440 32.86550
465.7261 30.84853
466.2082 29.33844
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467.1724 28.66381
467.6545 28.14144
468.1367 27.19906
468.6188 26.30547
469.1009 25.83830
469.5830 25.69642
470.0651 24.95806
470.5472 23.06767
471.0294 21.25395
471.5115 19.59504
471.9936 18.24169
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473.4399 16.99868
473.9221 17.23686
474.4042 17.90507
474.8863 17.80912
475.3684 15.97739
475.8505 14.40819
476.3326 13.92437
476.8148 14.24416
477.2969 14.74776
477.7790 15.19818
478.2611 15.73430
478.7432 16.88831
479.2253 19.54385
479.7075 20.36211
480.1896 16.18054
480.6717 12.33685
481.1538 12.39052
481.6359 15.76601
482.1180 18.79620
482.6002 18.65710
483.0823 16.49368
483.5644 15.69986
484.0465 16.77583
484.5286 17.33152
485.0107 15.38593
485.4929 12.84520
485.9750 12.15046
486.4571 13.87507
486.9392 15.76641
487.4213 16.71786
487.9034 16.82499
488.3856 16.08820
488.8677 14.39917
489.3498 12.62111
489.8319 11.47950
490.3140 10.97709
490.7961 10.58688
491.2783 10.74167
491.7604 10.78347
492.2425 9.898705
492.7246 8.561836
493.2067 7.890602
493.6888 8.284466
494.1710 8.915905
494.6531 8.407177
495.1352 6.050900
495.6173 4.829472
496.0994 5.769356
496.5815 6.676914
497.0637 5.980610
497.5458 4.444286
498.0279 4.028587
498.5100 5.971390
498.9921 9.076756
499.4742 10.22452
499.9564 8.637814
500.4385 7.052864
500.9206 5.317749
501.4027 4.123093
501.8848 4.326851
502.3669 5.659962
502.8491 6.725643
503.3312 6.166958
503.8133 4.769794
504.2954 4.968239
504.7775 7.210972
505.2596 8.873764
505.7418 8.275631
506.2239 6.636673
506.7060 5.658237
507.1881 5.470184
507.6702 5.778091
508.1523 7.160568
508.6345 8.712234
509.1166 8.682957
509.5987 6.810501
510.0808 4.543430
510.5629 2.911800
511.0450 1.917294
511.5272 1.440739
512.0093 2.259308
512.4914 2.609085
512.9735 1.420933
513.4556 0.2974130
513.9377 1.220005
514.4199 0.9982490
514.9020 0.1950450
515.3841 0.5767290
515.8662 1.382217
516.3483 1.715206
516.8304 0.9513240
517.3126 0.3700100
517.7947 0.5124050
518.2768 1.007858
518.7589 1.381351
519.2410 1.460037
519.7231 1.135311
520.2053 5.6800002E-04
520.6874 2.036957
521.1695 3.449879
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1262.665 8.022209
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1264.111 6.426523
1264.594 6.025879
1265.076 6.860651
1265.558 6.874275
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1267.004 3.143443
1267.486 3.200281
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1268.450 7.960223
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1269.415 7.833484
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1270.379 0.3430220
1270.861 2.870205
1271.343 10.24087
1271.825 11.18994
1272.307 7.296285
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1273.271 2.028766
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1274.236 5.054028
1274.718 7.452117
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1277.128 0.9324140
1277.611 3.8426999E-02
1278.093 0.1351890
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1279.057 3.037515
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1281.468 5.285182
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1282.914 1.182543
1283.396 4.7439998E-03
1283.878 1.0349000E-02
1284.360 1.442317
1284.842 1.580745
1285.324 0.0000000E+00
