#------------------------------------------------------------------------------ #$Date: 2019-10-15 09:51:56 +0300 (Tue, 15 Oct 2019) $ #$Revision: 1378 $ #$URL: svn://172.16.1.111/rod/cif/1/00/06/1000679.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_1000679 loop_ _publ_author_name 'Kanzaki, M.' 'Xue, X.' 'Amalberti, J.' 'Zhang, Q.' _publ_section_title ; Raman and NMR spectroscopic characterization of high-pressure K-cymrite (KAlSi3O8 H2O) and its anhydrous form (kokchetavite) : K-cymrite ; _journal_name_full 'Journal of Mineralogical and Petrological Sciences' _journal_page_first 114 _journal_page_last 119 _journal_paper_doi 10.2465/jmps.111020i _journal_volume 114 _journal_year 2012 _chemical_compound_source 'synthesized at 5 GPa and 800 C' _chemical_formula_structural 'NaAlSi3O8 H2O' _chemical_formula_sum 'Al H2 K O9 Si3' _chemical_name_mineral K-cymrite _chemical_name_systematic 'hydrous sodium alumino-silicate' _cod_original_formula_sum 'O9 Si3 Al K H2' _raman_determination.method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state powder _raman_measurement_device.location 'Institute for Planetary Materials, Okayama University' _raman_measurement_device.company 'home made' _raman_measurement_device.model 'Semrock filter system' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.55 _raman_measurement_device.excitation_laser_type argon _raman_measurement_device.excitation_laser_wavelength 488 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 1 _raman_measurement_device.power_on_sample 60 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.0 _raman_measurement_device.diffraction_grating 1200 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement_device_calibration.standard other _raman_measurement_device_calibration.standard_details ; Plasma lines are used. ; _raman_measurement.integration_time 300 _raman_measurement.datetime_initiated 2011-09-07 _raman_measurement.range_min 50.000 _raman_measurement.range_max 1400.643 _rod_data_source.file k-cymrite.rod _rod_data_source.block /var/www/html/rod/tmp/uploads/1571122279.3252-A619ABAF81C5BA8B.rod _rod_database.code 1000679 loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 50.000 429 51.262 438 52.523 441 53.785 439 55.046 437 56.307 433 57.567 434 58.828 438 60.088 435 61.349 431 62.609 430 63.869 432 65.128 440 66.388 435 67.647 440 68.906 433 70.165 440 71.424 447 72.683 442 73.941 453 75.200 461 76.458 459 77.716 470 78.974 481 80.231 495 81.489 515 82.746 531 84.003 564 85.260 575 86.517 588 87.773 597 89.030 615 90.286 621 91.542 641 92.798 646 94.054 657 95.309 642 96.565 661 97.820 655 99.075 685 100.330 697 101.585 712 102.839 747 104.093 798 105.348 844 106.602 916 107.855 993 109.109 1106 110.363 1283 111.616 1471 112.869 1616 114.122 1651 115.375 1579 116.627 1408 117.880 1243 119.132 1111 120.384 992 121.636 928 122.888 849 124.139 806 125.391 750 126.642 749 127.893 724 129.144 696 130.395 687 131.645 680 132.896 664 134.146 661 135.396 646 136.646 640 137.896 631 139.145 645 140.394 640 141.644 623 142.893 635 144.141 613 145.390 617 146.639 614 147.887 614 149.135 617 150.383 612 151.631 612 152.878 602 154.126 611 155.373 616 156.620 612 157.867 605 159.114 607 160.361 608 161.607 593 162.853 589 164.099 584 165.345 586 166.591 585 167.837 574 169.082 575 170.327 574 171.572 561 172.817 555 174.062 560 175.306 559 176.551 555 177.795 544 179.039 556 180.283 542 181.527 541 182.770 539 184.013 529 185.257 538 186.500 543 187.742 540 188.985 537 190.228 538 191.470 545 192.712 537 193.954 540 195.196 538 196.437 534 197.679 538 198.920 534 200.161 522 201.402 542 202.643 530 203.884 536 205.124 532 206.364 524 207.604 529 208.844 526 210.084 528 211.324 529 212.563 523 213.802 529 215.041 526 216.280 524 217.519 524 218.758 524 219.996 520 221.234 519 222.472 517 223.710 521 224.948 519 226.185 521 227.423 521 228.660 517 229.897 523 231.134 514 232.371 514 233.607 516 234.843 527 236.080 517 237.316 522 238.551 518 239.787 516 241.023 514 242.258 520 243.493 504 244.728 513 245.963 517 247.197 512 248.432 515 249.666 526 250.900 522 252.134 519 253.368 530 254.602 517 255.835 521 257.068 513 258.302 516 259.535 510 260.767 528 262.000 522 263.232 515 264.465 520 265.697 517 266.929 521 268.160 515 269.392 518 270.623 523 271.855 519 273.086 525 274.317 534 275.547 525 276.778 531 278.008 528 279.239 529 280.469 531 281.699 528 282.928 534 284.158 527 285.387 527 286.616 522 287.846 528 289.074 532 290.303 525 291.532 531 292.760 518 293.988 516 295.216 520 296.444 522 297.672 524 298.899 521 300.127 515 301.354 527 302.581 523 303.808 533 305.035 530 306.261 522 307.487 534 308.714 534 309.940 526 311.165 522 312.391 529 313.617 529 314.842 528 316.067 529 317.292 527 318.517 536 319.742 532 320.966 538 322.190 540 323.415 539 324.639 544 325.862 540 327.086 527 328.309 546 329.533 533 330.756 540 331.979 543 333.202 553 334.424 545 335.647 550 336.869 554 338.091 552 339.313 562 340.535 562 341.757 572 342.978 566 344.199 567 345.421 583 346.642 580 347.862 595 349.083 596 350.303 601 351.524 621 352.744 619 353.964 628 355.184 643 356.403 658 357.623 675 358.842 698 360.061 713 361.280 735 362.499 768 363.717 784 364.936 838 366.154 905 367.372 916 368.590 1001 369.808 1087 371.025 1177 372.243 1269 373.460 1394 374.677 1546 375.894 1659 377.111 1790 378.328 1869 379.544 1920 380.760 1921 381.976 1871 383.192 1800 384.408 1697 385.624 1610 386.839 1476 388.054 1366 389.269 1276 390.484 1190 391.699 1119 392.914 1058 394.128 989 395.342 948 396.556 920 397.770 877 398.984 859 400.198 826 401.411 798 402.624 778 403.838 762 405.050 738 406.263 722 407.476 723 408.688 705 409.900 686 411.113 680 412.324 675 413.536 663 414.748 636 415.959 627 417.171 619 418.382 617 419.593 606 420.803 604 422.014 589 423.224 589 424.435 580 425.645 569 426.855 580 428.064 571 429.274 560 430.483 568 431.693 561 432.902 562 434.111 565 435.319 559 436.528 545 437.736 552 438.945 550 440.153 556 441.361 562 442.568 553 443.776 548 444.983 548 446.191 550 447.398 547 448.605 541 449.812 550 451.018 552 452.225 544 453.431 552 454.637 548 455.843 543 457.049 548 458.254 549 459.460 549 460.665 553 461.870 544 463.075 545 464.280 542 465.484 534 466.689 543 467.893 541 469.097 543 470.301 541 471.505 541 472.709 540 473.912 550 475.115 552 476.318 543 477.521 541 478.724 531 479.927 536 481.129 533 482.332 532 483.534 530 484.736 521 485.937 525 487.139 529 488.341 526 489.542 529 490.743 523 491.944 524 493.145 526 494.345 523 495.546 515 496.746 530 497.946 524 499.146 517 500.346 527 501.546 533 502.745 529 503.945 531 505.144 530 506.343 533 507.542 542 508.740 539 509.939 559 511.137 560 512.335 564 513.533 574 514.731 570 515.929 569 517.126 560 518.324 553 519.521 553 520.718 550 521.915 542 523.111 528 524.308 526 525.504 525 526.700 516 527.896 512 529.092 508 530.288 512 531.483 503 532.679 519 533.874 512 535.069 510 536.264 498 537.459 502 538.653 503 539.848 496 541.042 515 542.236 502 543.430 506 544.623 505 545.817 504 547.010 502 548.204 500 549.397 499 550.590 508 551.782 501 552.975 500 554.167 501 555.360 505 556.552 505 557.744 496 558.935 503 560.127 510 561.318 501 562.510 498 563.701 505 564.892 495 566.082 508 567.273 498 568.464 501 569.654 509 570.844 497 572.034 501 573.224 506 574.413 504 575.603 500 576.792 503 577.981 500 579.170 495 580.359 497 581.548 498 582.736 513 583.924 498 585.113 502 586.301 507 587.488 508 588.676 499 589.864 497 591.051 499 592.238 500 593.425 497 594.612 494 595.799 497 596.985 497 598.172 499 599.358 497 600.544 497 601.730 499 602.915 499 604.101 498 605.286 496 606.472 500 607.657 497 608.842 494 610.026 505 611.211 495 612.395 500 613.579 498 614.764 504 615.947 498 617.131 501 618.315 504 619.498 504 620.682 499 621.865 500 623.048 497 624.230 494 625.413 493 626.595 495 627.778 499 628.960 498 630.142 496 631.324 501 632.505 501 633.687 497 634.868 493 636.049 493 637.230 500 638.411 495 639.592 497 640.772 499 641.953 497 643.133 491 644.313 506 645.493 494 646.672 492 647.852 500 649.031 492 650.210 503 651.389 503 652.568 501 653.747 495 654.926 499 656.104 500 657.282 491 658.460 496 659.638 495 660.816 493 661.994 497 663.171 495 664.348 492 665.525 496 666.702 492 667.879 496 669.056 487 670.232 494 671.408 499 672.585 499 673.761 495 674.936 492 676.112 496 677.287 493 678.463 493 679.638 489 680.813 498 681.988 493 683.162 491 684.337 489 685.511 489 686.686 487 687.860 491 689.033 503 690.207 496 691.381 495 692.554 494 693.727 491 694.900 492 696.073 493 697.246 489 698.419 499 699.591 495 700.763 498 701.935 492 703.107 497 704.279 493 705.451 489 706.622 492 707.793 490 708.965 492 710.136 500 711.306 504 712.477 494 713.648 500 714.818 497 715.988 503 717.158 503 718.328 494 719.498 504 720.667 501 721.836 501 723.006 504 724.175 501 725.344 497 726.512 493 727.681 501 728.849 500 730.017 496 731.186 496 732.353 497 733.521 500 734.689 495 735.856 502 737.023 506 738.191 504 739.358 506 740.524 497 741.691 508 742.857 502 744.024 500 745.190 506 746.356 502 747.522 506 748.687 507 749.853 500 751.018 510 752.183 511 753.348 508 754.513 502 755.678 508 756.843 504 758.007 508 759.171 511 760.335 500 761.499 507 762.663 509 763.827 503 764.990 509 766.153 510 767.316 503 768.479 515 769.642 511 770.805 517 771.967 508 773.129 508 774.292 503 775.454 510 776.615 508 777.777 510 778.939 516 780.100 510 781.261 510 782.422 511 783.583 502 784.744 508 785.904 521 787.065 507 788.225 509 789.385 511 790.545 509 791.705 503 792.864 506 794.024 512 795.183 518 796.342 508 797.501 511 798.660 524 799.819 510 800.977 522 802.135 519 803.294 517 804.452 513 805.609 517 806.767 512 807.925 510 809.082 526 810.239 523 811.396 526 812.553 530 813.710 524 814.866 529 816.023 536 817.179 534 818.335 541 819.491 543 820.647 546 821.803 553 822.958 559 824.113 570 825.268 569 826.423 585 827.578 601 828.733 610 829.887 620 831.042 616 832.196 637 833.350 621 834.504 619 835.658 615 836.811 610 837.965 595 839.118 581 840.271 560 841.424 566 842.577 561 843.729 554 844.882 538 846.034 540 847.186 534 848.338 527 849.490 530 850.642 521 851.793 522 852.944 525 854.096 519 855.247 525 856.397 513 857.548 513 858.699 511 859.849 510 860.999 508 862.149 508 863.299 505 864.449 504 865.599 510 866.748 510 867.897 511 869.047 514 870.195 508 871.344 506 872.493 508 873.641 509 874.790 510 875.938 510 877.086 513 878.234 506 879.382 504 880.529 513 881.676 511 882.824 503 883.971 507 885.118 506 886.264 505 887.411 506 888.558 508 889.704 501 890.850 514 891.996 502 893.142 502 894.287 507 895.433 507 896.578 505 897.723 506 898.868 508 900.013 507 901.158 502 902.303 490 903.447 500 904.591 507 905.735 501 906.879 500 908.023 501 909.167 501 910.310 513 911.453 504 912.597 515 913.740 502 914.882 503 916.025 509 917.168 503 918.310 505 919.452 503 920.594 511 921.736 505 922.878 511 924.019 500 925.161 503 926.302 502 927.443 502 928.584 507 929.725 504 930.865 507 932.006 506 933.146 508 934.286 506 935.426 501 936.566 511 937.706 505 938.846 503 939.985 502 941.124 509 942.263 513 943.402 506 944.541 512 945.679 509 946.818 506 947.956 510 949.094 500 950.232 519 951.370 514 952.508 517 953.645 511 954.783 509 955.920 512 957.057 514 958.194 510 959.330 507 960.467 505 961.603 505 962.740 510 963.876 501 965.012 518 966.147 513 967.283 513 968.419 512 969.554 509 970.689 519 971.824 511 972.959 515 974.094 517 975.228 515 976.362 518 977.497 522 978.631 526 979.765 514 980.898 534 982.032 528 983.165 531 984.299 531 985.432 528 986.565 533 987.698 540 988.830 526 989.963 542 991.095 536 992.227 533 993.359 548 994.491 532 995.623 544 996.755 538 997.886 540 999.017 544 1000.148 542 1001.279 546 1002.410 547 1003.541 553 1004.671 543 1005.802 546 1006.932 547 1008.062 542 1009.192 546 1010.321 543 1011.451 538 1012.580 543 1013.710 542 1014.839 540 1015.968 545 1017.096 531 1018.225 538 1019.354 531 1020.482 532 1021.610 526 1022.738 531 1023.866 528 1024.994 531 1026.121 530 1027.249 527 1028.376 533 1029.503 533 1030.630 528 1031.757 527 1032.883 529 1034.010 524 1035.136 525 1036.262 525 1037.388 526 1038.514 525 1039.640 533 1040.765 528 1041.891 531 1043.016 531 1044.141 533 1045.266 535 1046.390 537 1047.515 532 1048.640 527 1049.764 538 1050.888 541 1052.012 540 1053.136 533 1054.259 544 1055.383 547 1056.506 542 1057.630 545 1058.753 542 1059.876 539 1060.998 550 1062.121 541 1063.243 547 1064.366 544 1065.488 549 1066.610 543 1067.732 545 1068.853 560 1069.975 559 1071.096 552 1072.217 548 1073.338 547 1074.459 541 1075.580 545 1076.701 546 1077.821 538 1078.941 551 1080.061 547 1081.181 554 1082.301 554 1083.421 551 1084.540 549 1085.660 545 1086.779 545 1087.898 552 1089.017 551 1090.136 558 1091.254 555 1092.373 550 1093.491 567 1094.609 564 1095.727 569 1096.845 571 1097.963 571 1099.080 571 1100.197 573 1101.315 570 1102.432 572 1103.549 589 1104.665 572 1105.782 577 1106.898 569 1108.015 579 1109.131 569 1110.247 572 1111.363 572 1112.478 567 1113.594 571 1114.709 572 1115.824 564 1116.940 567 1118.054 566 1119.169 571 1120.284 563 1121.398 558 1122.513 559 1123.627 560 1124.741 560 1125.855 547 1126.968 544 1128.082 566 1129.195 550 1130.308 551 1131.421 552 1132.534 543 1133.647 548 1134.760 544 1135.872 530 1136.985 549 1138.097 544 1139.209 545 1140.321 533 1141.432 548 1142.544 540 1143.655 542 1144.766 533 1145.877 535 1146.988 531 1148.099 526 1149.210 536 1150.320 529 1151.431 539 1152.541 535 1153.651 529 1154.761 529 1155.870 523 1156.980 527 1158.089 526 1159.199 531 1160.308 531 1161.417 530 1162.525 538 1163.634 527 1164.743 530 1165.851 531 1166.959 516 1168.067 529 1169.175 523 1170.283 526 1171.390 530 1172.498 530 1173.605 522 1174.712 527 1175.819 531 1176.926 522 1178.033 531 1179.139 535 1180.246 525 1181.352 528 1182.458 520 1183.564 518 1184.670 527 1185.775 524 1186.881 529 1187.986 519 1189.091 534 1190.196 533 1191.301 520 1192.406 527 1193.510 516 1194.614 520 1195.719 516 1196.823 524 1197.927 517 1199.031 519 1200.134 505 1201.238 520 1202.341 512 1203.444 514 1204.547 514 1205.650 519 1206.753 522 1207.855 520 1208.958 519 1210.060 517 1211.162 522 1212.264 518 1213.366 512 1214.468 514 1215.569 517 1216.670 517 1217.772 518 1218.873 518 1219.974 518 1221.074 523 1222.175 526 1223.275 523 1224.376 526 1225.476 515 1226.576 514 1227.676 521 1228.775 514 1229.875 519 1230.974 522 1232.074 517 1233.173 511 1234.272 523 1235.370 522 1236.469 511 1237.568 519 1238.666 519 1239.764 517 1240.862 512 1241.960 507 1243.058 515 1244.155 523 1245.253 515 1246.350 517 1247.447 515 1248.544 516 1249.641 523 1250.738 516 1251.834 513 1252.931 519 1254.027 530 1255.123 517 1256.219 524 1257.315 518 1258.410 521 1259.506 508 1260.601 524 1261.696 515 1262.791 515 1263.886 506 1264.981 513 1266.075 518 1267.170 516 1268.264 516 1269.358 514 1270.452 524 1271.546 513 1272.640 516 1273.733 514 1274.827 516 1275.920 517 1277.013 516 1278.106 519 1279.199 518 1280.291 520 1281.384 524 1282.476 515 1283.568 514 1284.660 516 1285.752 523 1286.844 521 1287.935 524 1289.027 515 1290.118 528 1291.209 527 1292.300 528 1293.391 520 1294.482 524 1295.572 529 1296.662 523 1297.753 522 1298.843 526 1299.933 515 1301.022 524 1302.112 527 1303.202 522 1304.291 528 1305.380 533 1306.469 521 1307.558 526 1308.647 529 1309.735 534 1310.824 530 1311.912 531 1313.000 529 1314.088 530 1315.176 524 1316.263 522 1317.351 540 1318.438 527 1319.526 527 1320.613 531 1321.700 526 1322.786 531 1323.873 532 1324.960 520 1326.046 535 1327.132 525 1328.218 532 1329.304 530 1330.390 544 1331.475 539 1332.561 536 1333.646 535 1334.731 535 1335.816 535 1336.901 536 1337.986 540 1339.070 543 1340.155 532 1341.239 544 1342.323 534 1343.407 538 1344.491 536 1345.574 541 1346.658 543 1347.741 547 1348.824 540 1349.907 542 1350.990 540 1352.073 545 1353.156 544 1354.238 548 1355.320 548 1356.403 544 1357.485 543 1358.566 552 1359.648 538 1360.730 549 1361.811 528 1362.892 537 1363.974 545 1365.055 540 1366.135 541 1367.216 543 1368.297 549 1369.377 540 1370.457 548 1371.537 547 1372.617 535 1373.697 539 1374.777 540 1375.856 542 1376.935 541 1378.015 547 1379.094 530 1380.173 535 1381.251 532 1382.330 542 1383.408 534 1384.487 532 1385.565 537 1386.643 536 1387.721 530 1388.798 543 1389.876 537 1390.953 531 1392.031 526 1393.108 536 1394.185 534 1395.261 544 1396.338 539 1397.415 532 1398.491 528 1399.567 534 1400.643 529