#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-04-26 14:10:14 +0300 (Thu, 26 Apr 2018) $ #$Revision: 651 $ #$URL: svn://172.16.1.111/rod/cif/2/00/00/2000002.rod $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2000002 loop_ _publ_author_name 'Cadoni, Marcella' 'Ferraris, Giovanni' _publ_section_title ; Penkvilksite-2O: Na~2~TiSi~4~O~11~·2H~2~O ; _journal_coeditor_code FA3162 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 87 _journal_page_last 90 _journal_paper_doi 10.1107/S0108270108031806 _journal_volume 64 _journal_year 2008 _chemical_compound_source R130027 _chemical_formula_iupac 'Na2 Ti Si4 O11, 2H2 O' _chemical_formula_moiety 'Na2 Ti Si4 O11, 2(H2 O)' _chemical_formula_sum 'H4 Na2 O13 Si4 Ti' _chemical_formula_weight 418.10 _chemical_name_common 'sodium titanosilicate hydrate' _chemical_name_systematic ; disodium titanium tetrasilicate dihydrate ; _space_group_IT_number 60 _symmetry_cell_setting orthorhombic _symmetry_space_group_name_Hall '-P 2a 2n' _symmetry_space_group_name_H-M 'P n c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 16.320(2) _cell_length_b 8.7378(9) _cell_length_c 7.3854(8) _cell_measurement_reflns_used 1306 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 28.3 _cell_measurement_theta_min 2.5 _cell_volume 1053.2(2) _computing_cell_refinement 'SMART (Bruker, 2004)' _computing_data_collection 'SMART (Bruker, 2004)' _computing_data_reduction 'SAINT-Plus (Bruker, 2004) and SADABS (Sheldrick, 2002)' _computing_molecular_graphics 'ATOMS 6.2 (Dowty, 2002)' _computing_publication_material 'SHELXL97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_structure_solution 'SHELXS97 (Sheldrick, 2008)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker SMART APEX' _diffrn_measurement_method '\f and \w' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0820 _diffrn_reflns_av_sigmaI/netI 0.0379 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 13075 _diffrn_reflns_theta_full 28.28 _diffrn_reflns_theta_max 28.28 _diffrn_reflns_theta_min 2.50 _exptl_absorpt_coefficient_mu 1.427 _exptl_absorpt_correction_T_max 0.9720 _exptl_absorpt_correction_T_min 0.8705 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details '(SADABS; Sheldrick, 2002)' _exptl_crystal_density_diffrn 2.638 _exptl_crystal_density_method 'not measured' _exptl_crystal_description tabular _exptl_crystal_F_000 832 _exptl_crystal_size_max 0.10 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.02 _refine_diff_density_max 1.133 _refine_diff_density_min -1.131 _refine_ls_extinction_coef 0.0028(13) _refine_ls_extinction_method 'SHELXL97 (Sheldrick, 2008)' _refine_ls_goodness_of_fit_ref 1.230 _refine_ls_hydrogen_treatment noref _refine_ls_matrix_type full _refine_ls_number_parameters 94 _refine_ls_number_reflns 1306 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.230 _refine_ls_R_factor_all 0.0868 _refine_ls_R_factor_gt 0.0756 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+14.7729P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1568 _refine_ls_wR_factor_ref 0.1610 _reflns_number_gt 1109 _reflns_number_total 1306 _reflns_threshold_expression I>2\s(I) _cod_data_source_file fa3162.cif _cod_data_source_block I _cod_database_code 2016825 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R130027.rod _rod_data_source.block 3500000 _rod_database.code 2000002 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 2016825 COD http://www.crystallography.net/cod/2016825.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 90.23535 0.0000000E+00 90.71747 2.818146 91.19958 4.644989 91.68170 11.50775 92.16382 15.63669 92.64594 16.64075 93.12805 16.54318 93.61017 16.05200 94.09229 14.20306 94.57440 9.233429 95.05651 5.854523 95.53863 4.808136 96.02074 5.282654 96.50286 6.593658 96.98498 8.266968 97.46709 9.595306 97.94921 11.21652 98.43133 12.08893 98.91344 13.78653 99.39556 16.70880 99.87768 20.56992 100.3598 24.90738 100.8419 29.49579 101.3240 34.27795 101.8061 38.75281 102.2883 42.92029 102.7704 46.98227 103.2525 51.23978 103.7346 55.84766 104.2167 60.91891 104.6988 65.92368 105.1810 69.57483 105.6631 70.93539 106.1452 69.78265 106.6273 67.24866 107.1094 65.31134 107.5915 63.36343 108.0737 61.02798 108.5558 58.19223 109.0379 54.91519 109.5200 51.85538 110.0021 49.72549 110.4842 48.88794 110.9664 47.38400 111.4485 45.32031 111.9306 42.77808 112.4127 39.54068 112.8948 35.72586 113.3769 31.65735 113.8591 27.72675 114.3412 24.06924 114.8233 20.20419 115.3054 15.65952 115.7875 11.11179 116.2696 7.208679 116.7517 4.169067 117.2339 1.810852 117.7160 0.2116390 118.1981 2.111328 118.6802 3.480652 119.1623 4.084991 119.6444 3.944061 120.1266 3.318726 120.6087 2.126587 121.0908 0.6908570 121.5729 0.3799130 122.0550 1.074738 122.5371 1.438080 123.0193 1.235291 123.5014 0.3490600 123.9835 0.1405030 124.4656 0.7527470 124.9477 2.157440 125.4298 3.300262 125.9120 3.821503 126.3941 4.050232 126.8762 4.747101 127.3583 6.163879 127.8404 7.670197 128.3225 9.028931 128.8047 10.35159 129.2868 11.78220 129.7689 13.41196 130.2510 15.23444 130.7331 17.14993 131.2152 19.41199 131.6974 21.53500 132.1795 22.91650 132.6616 23.97989 133.1437 25.72284 133.6258 29.12582 134.1079 34.61560 134.5901 39.42993 135.0722 42.95688 135.5543 46.43068 136.0364 50.52899 136.5185 55.31793 137.0006 60.44606 137.4828 65.45981 137.9649 70.32512 138.4470 75.43460 138.9291 81.07617 139.4112 86.88327 139.8933 92.67233 140.3755 98.56624 140.8576 103.9899 141.3397 108.2838 141.8218 111.6251 142.3039 113.1581 142.7860 111.9799 143.2681 108.3348 143.7503 103.0984 144.2324 95.36388 144.7145 86.65945 145.1966 78.13795 145.6787 69.92621 146.1608 62.47662 146.6430 56.14735 147.1251 51.06161 147.6072 46.54233 148.0893 43.13068 148.5714 40.39780 149.0535 38.72655 149.5357 38.18723 150.0178 38.40292 150.4999 38.88269 150.9820 39.67012 151.4641 40.64775 151.9462 41.66634 152.4284 42.88412 152.9105 44.45496 153.3926 46.42097 153.8747 48.69592 154.3568 51.05696 154.8389 53.44560 155.3211 56.01524 155.8032 58.70224 156.2853 61.58441 156.7674 64.79718 157.2495 68.42996 157.7316 72.38037 158.2138 76.20084 158.6959 79.55066 159.1780 83.15775 159.6601 87.21484 160.1422 91.65759 160.6243 96.41983 161.1065 101.5692 161.5886 106.9098 162.0707 111.5544 162.5528 115.3730 163.0349 118.6926 163.5170 121.6129 163.9991 124.1560 164.4813 126.4491 164.9634 128.7102 165.4455 130.6889 165.9276 131.9111 166.4097 132.2244 166.8918 131.8457 167.3740 131.0702 167.8561 129.9746 168.3382 128.1259 168.8203 125.0432 169.3024 121.1250 169.7845 116.7018 170.2667 111.9127 170.7488 106.6993 171.2309 100.8378 171.7130 93.95450 172.1951 87.09460 172.6772 80.41159 173.1594 73.97464 173.6415 67.84253 174.1236 62.06062 174.6057 56.62717 175.0878 51.63246 175.5699 47.29706 176.0521 43.12537 176.5342 39.01434 177.0163 35.05116 177.4984 31.41942 177.9805 28.25864 178.4626 25.60263 178.9448 23.05737 179.4269 20.19427 179.9090 17.76903 180.3911 16.15724 180.8732 15.18237 181.3553 14.41815 181.8375 13.55008 182.3196 12.64548 182.8017 11.82417 183.2838 11.00851 183.7659 10.27383 184.2480 9.671692 184.7301 9.204544 185.2123 8.826813 185.6944 8.481705 186.1765 8.158371 186.6586 7.961365 187.1407 8.137802 187.6228 8.265503 188.1050 8.081696 188.5871 7.553650 189.0692 6.698914 189.5513 5.392838 190.0334 3.643814 190.5155 2.075333 190.9977 0.7797700 191.4798 0.2957310 191.9619 1.158203 192.4440 1.780518 192.9261 2.371719 193.4082 3.303604 193.8904 4.437241 194.3725 5.200119 194.8546 5.108612 195.3367 4.579529 195.8188 4.496689 196.3009 5.119141 196.7831 5.769974 197.2652 6.018051 197.7473 5.924103 198.2294 5.577789 198.7115 4.916946 199.1936 4.013748 199.6758 3.169632 200.1579 2.345642 200.6400 1.659973 201.1221 1.268402 201.6042 1.061600 202.0863 0.7745360 202.5685 0.1784210 203.0506 0.7060090 203.5327 1.491974 204.0148 2.090088 204.4969 2.671509 204.9790 3.378662 205.4612 4.128372 205.9433 4.719772 206.4254 5.003845 206.9075 4.978683 207.3896 4.771927 207.8717 4.038895 208.3539 3.439240 208.8360 3.198517 209.3181 3.283859 209.8002 3.566925 210.2823 3.983536 210.7644 4.584869 211.2466 4.849518 211.7287 4.511795 212.2108 4.111130 212.6929 3.923721 213.1750 3.888596 213.6571 3.709625 214.1393 3.052292 214.6214 1.756027 215.1035 1.178101 215.5856 1.863663 216.0677 2.611191 216.5498 2.762650 217.0320 2.369629 217.5141 1.927826 217.9962 1.877243 218.4783 2.268646 218.9604 2.758301 219.4425 3.534470 219.9247 4.248184 220.4068 4.505966 220.8889 4.379150 221.3710 4.477707 221.8531 5.405991 222.3352 7.232681 222.8174 8.706726 223.2995 9.657196 223.7816 10.38995 224.2637 11.10837 224.7458 11.82784 225.2279 12.48543 225.7100 13.05127 226.1922 13.50188 226.6743 13.78708 227.1564 13.67540 227.6385 13.53786 228.1206 13.72734 228.6027 14.26505 229.0849 14.93427 229.5670 15.60150 230.0491 16.28168 230.5312 17.02122 231.0133 17.83755 231.4954 18.70975 231.9776 19.60799 232.4597 20.52771 232.9418 21.50278 233.4239 22.40633 233.9060 23.41927 234.3881 24.88031 234.8703 27.02560 235.3524 29.51237 235.8345 31.90596 236.3166 34.19138 236.7987 36.51401 237.2808 38.86563 237.7630 41.33266 238.2451 44.12970 238.7272 47.49951 239.2093 50.97766 239.6914 53.60583 240.1735 54.97777 240.6557 56.85637 241.1378 60.34427 241.6199 64.47195 242.1020 68.31900 242.5841 71.49873 243.0662 74.47583 243.5484 78.05762 244.0305 82.38785 244.5126 86.94229 244.9947 91.85764 245.4768 96.76343 245.9589 101.2318 246.4410 105.0996 246.9232 108.7873 247.4053 113.1207 247.8874 118.3331 248.3695 123.6190 248.8516 128.3315 249.3337 133.2472 249.8159 139.1248 250.2980 146.1979 250.7801 153.8435 251.2622 161.0350 251.7443 167.3685 252.2264 174.0729 252.7086 181.3197 253.1907 188.9683 253.6728 196.9541 254.1549 205.1921 254.6370 213.6492 255.1191 222.4406 255.6013 231.9174 256.0834 240.9730 256.5655 249.7520 257.0476 258.1345 257.5297 266.3020 258.0118 274.1505 258.4940 281.2262 258.9761 287.1151 259.4582 292.6189 259.9403 294.4355 260.4224 292.2196 260.9045 287.5222 261.3867 280.9773 261.8688 272.8032 262.3509 263.1858 262.8330 252.2286 263.3151 239.7616 263.7972 226.3472 264.2794 211.1096 264.7615 195.8898 265.2436 181.6231 265.7257 168.4252 266.2078 155.9607 266.6899 143.9157 267.1721 132.2931 267.6542 121.4442 268.1363 110.8790 268.6184 101.3305 269.1005 93.28064 269.5826 86.63989 270.0648 81.01927 270.5469 76.12769 271.0290 72.00208 271.5111 68.58591 271.9932 66.01648 272.4753 63.84563 272.9575 61.94009 273.4396 60.29527 273.9217 58.96582 274.4038 58.01195 274.8859 57.40291 275.3680 56.81380 275.8501 55.79037 276.3322 55.25769 276.8144 55.77277 277.2965 57.02069 277.7786 58.26819 278.2607 59.09013 278.7428 59.64163 279.2249 60.62413 279.7071 62.17854 280.1892 63.89899 280.6713 65.73227 281.1534 67.66019 281.6355 69.50792 282.1176 71.10292 282.5998 72.88435 283.0819 76.14795 283.5640 82.01544 284.0461 87.04797 284.5282 89.98547 285.0103 91.81958 285.4925 93.87798 285.9746 96.56390 286.4567 99.81670 286.9388 103.7144 287.4209 108.4833 287.9030 113.0129 288.3852 117.4091 288.8673 121.3407 289.3494 124.3220 289.8315 126.2341 290.3136 127.4117 290.7957 128.2095 291.2779 128.6172 291.7600 128.5927 292.2421 128.2195 292.7242 127.3572 293.2063 125.8186 293.6884 123.5777 294.1706 120.8514 294.6527 117.7014 295.1348 114.1197 295.6169 110.7633 296.0990 107.6611 296.5811 104.7877 297.0633 102.1009 297.5454 99.61728 298.0275 97.40002 298.5096 95.51874 298.9917 93.98080 299.4738 92.59319 299.9560 91.20534 300.4381 90.10837 300.9202 89.47345 301.4023 89.27675 301.8844 89.41086 302.3665 89.89529 302.8487 90.62921 303.3308 91.31526 303.8129 92.09894 304.2950 92.62399 304.7771 92.55484 305.2592 92.09283 305.7414 91.87491 306.2235 92.31415 306.7056 92.78123 307.1877 91.97792 307.6698 89.81148 308.1519 87.25584 308.6341 84.65735 309.1162 81.87111 309.5983 78.64444 310.0804 74.90442 310.5625 70.81841 311.0446 66.63965 311.5268 62.38576 312.0089 57.79526 312.4910 52.63345 312.9731 47.19562 313.4552 41.64317 313.9373 35.99527 314.4195 30.64906 314.9016 26.03552 315.3837 22.11797 315.8658 18.24615 316.3479 14.10063 316.8300 10.17206 317.3121 6.837753 317.7943 4.095398 318.2764 1.846573 318.7585 3.1677000E-02 319.2406 1.286407 319.7227 2.151794 320.2048 2.352341 320.6870 2.335159 321.1691 2.361923 321.6512 2.378723 322.1333 2.220032 322.6154 1.842819 323.0975 1.190369 323.5797 0.1331180 324.0618 1.351822 324.5439 3.086349 325.0260 5.187042 325.5081 7.471893 325.9902 9.576050 326.4724 11.35399 326.9545 13.04170 327.4366 14.95605 327.9187 17.03284 328.4008 19.54152 328.8829 22.82773 329.3651 26.42978 329.8472 29.87291 330.3293 33.07458 330.8114 36.02327 331.2935 38.55501 331.7756 40.65645 332.2578 43.55615 332.7399 47.72202 333.2220 52.34225 333.7041 56.82530 334.1862 61.19640 334.6683 65.93294 335.1505 71.38745 335.6326 77.38593 336.1147 82.88669 336.5968 87.81467 337.0789 92.52899 337.5610 97.00307 338.0432 101.3705 338.5253 106.0055 339.0074 111.1700 339.4895 116.5081 339.9716 121.0054 340.4537 124.7160 340.9359 127.6369 341.4180 129.8552 341.9001 131.2359 342.3822 131.4995 342.8643 130.5972 343.3464 128.9405 343.8286 126.9760 344.3107 124.4931 344.7928 122.0134 345.2749 119.7574 345.7570 117.4730 346.2391 114.9020 346.7213 112.0289 347.2034 108.9839 347.6855 105.9412 348.1676 102.9093 348.6497 99.95135 349.1318 96.89130 349.6140 94.08186 350.0961 91.83162 350.5782 89.97049 351.0603 88.02722 351.5424 85.69617 352.0245 83.20819 352.5067 81.50423 352.9888 80.79501 353.4709 80.60449 353.9530 80.90036 354.4351 81.67831 354.9172 82.97171 355.3994 84.78883 355.8815 87.03696 356.3636 89.58482 356.8457 92.52835 357.3278 95.61752 357.8099 98.68484 358.2920 102.0047 358.7741 105.8819 359.2563 110.2678 359.7384 114.7153 360.2205 118.7649 360.7026 122.3253 361.1847 126.3952 361.6668 131.3443 362.1490 136.3710 362.6311 141.3741 363.1132 146.2625 363.5953 150.8896 364.0774 155.1982 364.5595 159.1254 365.0417 162.4029 365.5238 164.9166 366.0059 166.8332 366.4880 168.2468 366.9701 169.0759 367.4522 169.2785 367.9344 168.8314 368.4165 167.6678 368.8986 165.5469 369.3807 162.0657 369.8628 158.7186 370.3449 155.6374 370.8271 152.6190 371.3092 149.4603 371.7913 146.2248 372.2734 143.1177 372.7555 140.3851 373.2376 138.0188 373.7198 135.5378 374.2019 133.0486 374.6840 130.2757 375.1661 127.2132 375.6482 123.8116 376.1303 120.0499 376.6125 115.9090 377.0946 111.3433 377.5767 106.1738 378.0588 100.2171 378.5409 94.19839 379.0230 88.47278 379.5052 82.66078 379.9873 76.38423 380.4694 69.57565 380.9515 62.62984 381.4336 55.76982 381.9157 48.98769 382.3979 42.98543 382.8800 38.13506 383.3621 33.81410 383.8442 29.43349 384.3263 25.13118 384.8084 21.29271 385.2906 18.35542 385.7727 16.02792 386.2548 13.57002 386.7369 10.87234 387.2190 8.472519 387.7011 6.875443 388.1833 5.716904 388.6654 4.496048 389.1475 3.052612 389.6296 1.651733 390.1117 0.5876770 390.5938 0.1887050 391.0760 1.070953 391.5581 2.360977 392.0402 3.581879 392.5223 3.987335 393.0044 3.524918 393.4865 3.144669 393.9687 3.284439 394.4508 3.713531 394.9329 4.082520 395.4150 4.346390 395.8971 4.560211 396.3792 4.797760 396.8614 5.039322 397.3435 5.134888 397.8256 5.033981 398.3077 4.827911 398.7898 4.461777 399.2719 4.015656 399.7540 3.827164 400.2361 4.153702 400.7183 4.705643 401.2004 4.578201 401.6825 3.312988 402.1646 2.288544 402.6467 2.018173 403.1288 1.984177 403.6110 1.546967 404.0931 0.5768890 404.5752 0.5510560 405.0573 1.409271 405.5394 1.948639 406.0215 2.408920 406.5037 2.601929 406.9858 2.902695 407.4679 3.492264 407.9500 4.345001 408.4321 5.374664 408.9142 6.549698 409.3964 7.833496 409.8785 9.079041 410.3606 10.34708 410.8427 11.48068 411.3248 12.44406 411.8069 13.28294 412.2891 13.96832 412.7712 14.52328 413.2533 15.12686 413.7354 16.03404 414.2175 17.32224 414.6996 18.62206 415.1818 20.12100 415.6639 21.44817 416.1460 22.25488 416.6281 22.76501 417.1102 23.47333 417.5923 24.68887 418.0745 26.34598 418.5566 28.37787 419.0387 31.20981 419.5208 33.43869 420.0029 34.06427 420.4850 34.21315 420.9672 34.89734 421.4493 36.36554 421.9314 38.19789 422.4135 40.06206 422.8956 41.94907 423.3777 43.74121 423.8599 45.39862 424.3420 46.98012 424.8241 48.80046 425.3062 50.66898 425.7883 51.86662 426.2704 51.92096 426.7526 51.21101 427.2347 50.22881 427.7168 48.96754 428.1989 47.54491 428.6810 46.14099 429.1631 44.52773 429.6453 42.26216 430.1274 39.02928 430.6095 35.85072 431.0916 33.26093 431.5737 31.08835 432.0558 28.94823 432.5380 26.73859 433.0201 24.65834 433.5022 22.88539 433.9843 21.42854 434.4664 20.53764 434.9485 20.60976 435.4307 20.91895 435.9128 21.06143 436.3949 21.03133 436.8770 20.88206 437.3591 20.60252 437.8412 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464.8398 14.89818 465.3219 14.37944 465.8040 14.25789 466.2861 14.06613 466.7682 13.24510 467.2503 11.68065 467.7325 10.37157 468.2146 9.482544 468.6967 8.676819 469.1788 7.964630 469.6609 7.255142 470.1430 6.391006 470.6252 5.293610 471.1073 4.158478 471.5894 3.343231 472.0715 2.905121 472.5536 2.543610 473.0357 2.302643 473.5179 2.060638 474.0000 1.768066 474.4821 1.419006 474.9642 1.000504 475.4463 0.4551850 475.9284 0.1448970 476.4106 0.7288670 476.8927 1.348434 477.3748 1.602661 477.8569 1.151001 478.3390 0.2813260 478.8211 0.5487980 479.3033 1.329086 479.7854 2.036072 480.2675 2.458374 480.7496 2.848206 481.2317 3.774368 481.7138 5.357346 482.1959 6.993958 482.6780 8.144440 483.1602 8.804550 483.6423 9.556503 484.1244 10.46155 484.6065 11.38290 485.0886 12.12555 485.5707 12.88101 486.0529 14.04758 486.5350 15.77264 487.0171 17.71518 487.4992 19.25389 487.9813 20.03085 488.4634 21.44179 488.9456 24.02821 489.4277 26.61829 489.9098 28.52934 490.3919 29.97882 490.8740 31.56537 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544.8710 186.6239 545.3531 186.2943 545.8353 186.3222 546.3174 186.6342 546.7995 186.1698 547.2816 184.7178 547.7637 182.8169 548.2458 180.5263 548.7280 178.0204 549.2101 175.6542 549.6922 173.7994 550.1743 171.4858 550.6564 167.7148 551.1385 163.0932 551.6207 159.0005 552.1028 155.7343 552.5849 152.3667 553.0670 147.9824 553.5491 142.5690 554.0313 137.5050 554.5134 133.1082 554.9955 128.5963 555.4776 123.5317 555.9597 118.3203 556.4418 113.5333 556.9240 109.2789 557.4061 105.3079 557.8882 101.3414 558.3703 97.40831 558.8524 93.28151 559.3345 88.80302 559.8167 84.40054 560.2988 80.08766 560.7809 75.96793 561.2630 72.20612 561.7451 68.88643 562.2272 65.58302 562.7094 61.71742 563.1915 57.55472 563.6736 54.02599 564.1557 51.27711 564.6378 48.90588 565.1199 46.78494 565.6021 44.80699 566.0842 42.49937 566.5663 39.39503 567.0484 36.63144 567.5305 34.95616 568.0126 33.66895 568.4948 31.75520 568.9769 29.12114 569.4590 26.49286 569.9411 24.59222 570.4232 23.37268 570.9053 22.09908 571.3875 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