#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:39:17 +0300 (Thu, 24 May 2018) $
#$Revision: 769 $
#$URL: svn://172.16.1.111/rod/cif/2/00/00/2000004.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000004
loop_
_publ_author_name
'Yang, Hexiong'
'Sano, Jennifer L.'
'Eichler, Carla'
'Downs, Robert T.'
'Costin, Gelu'
_publ_section_title
;
 Iranite, CuPb~10~(CrO~4~)~6~(SiO~4~)~2~(OH)~2~, isomorphous with
 hemihedrite
;
_journal_coeditor_code           IZ3032
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              122
_journal_page_last               124
_journal_paper_doi               10.1107/S0108270107053449
_journal_volume                  63
_journal_year                    2007
_chemical_compound_source        R060781
_chemical_formula_iupac          'Cu Pb10 (Cr O4)6 (Si O4)2 (O H)2'
_chemical_formula_moiety         'Cr6 Cu H2 O34 Pb10 Si2'
_chemical_formula_sum            'Cr6 Cu H2 O34 Pb10 Si2'
_chemical_formula_weight         3049.64
_chemical_name_common            Iranite
_chemical_name_systematic
;
copper decalead hexachromate bis(orthosilicate) dihydroxide
;
_cell_angle_alpha                120.472(2)
_cell_angle_beta                 92.470(2)
_cell_angle_gamma                55.531(2)
_cell_formula_units_Z            1
_cell_length_a                   9.5416(4)
_cell_length_b                   11.3992(5)
_cell_length_c                   10.7465(4)
_cod_data_source_file            iz3032.cif
_cod_data_source_block           I
_cod_original_cell_volume        780.08(6)
_cod_original_formula_sum        'H2 Cr6 Cu O34 Pb10 Si2'
_cod_database_code               2016341
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R060781.rod
_rod_data_source.block           3500000
_rod_database.code               2000004
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 2016341 COD http://www.crystallography.net/cod/2016341.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
116.6693 0.0000000E+00
117.1515 41.83203
117.6336 48.11890
118.1157 8.852295
118.5978 30.08447
119.0799 10.86353
119.5620 40.13818
120.0442 124.6853
120.5263 257.8218
121.0084 422.4272
121.4905 592.0967
121.9726 746.4541
122.4547 899.7637
122.9369 1070.954
123.4190 1260.246
123.9011 1459.778
124.3832 1667.516
124.8653 1881.091
125.3474 2083.907
125.8296 2252.344
126.3117 2403.791
126.7938 2581.889
127.2759 2804.237
127.7580 3048.555
128.2401 3270.715
128.7223 3471.639
129.2044 3665.219
129.6865 3854.857
130.1686 4043.094
130.6507 4243.693
131.1328 4477.677
131.6149 4732.634
132.0971 4921.605
132.5792 5035.026
133.0613 5123.361
133.5434 5260.503
134.0255 5450.143
134.5076 5634.214
134.9898 5784.120
135.4719 5897.316
135.9540 6017.029
136.4361 6147.465
136.9182 6282.035
137.4003 6402.679
137.8825 6512.479
138.3646 6603.543
138.8467 6664.394
139.3288 6677.916
139.8109 6720.066
140.2930 6812.851
140.7752 6945.323
141.2573 7033.057
141.7394 7054.120
142.2215 7054.884
142.7036 7071.573
143.1857 7099.455
143.6679 7143.015
144.1500 7129.415
144.6321 7123.150
145.1142 7103.849
145.5963 7064.089
146.0784 7015.060
146.5606 6972.804
147.0427 6957.998
147.5248 6928.662
148.0069 6874.884
148.4890 6795.066
148.9711 6697.275
149.4533 6561.528
149.9354 6408.625
150.4175 6285.329
150.8996 6198.651
151.3817 6136.264
151.8638 6094.278
152.3460 6105.042
152.8281 6096.687
153.3102 6064.113
153.7923 6007.993
154.2744 5930.341
154.7565 5819.686
155.2386 5695.002
155.7208 5567.649
156.2029 5400.490
156.6850 5269.409
157.1671 5214.272
157.6492 5235.955
158.1313 5234.302
158.6135 5161.585
159.0956 5055.735
159.5777 4957.685
160.0598 4872.861
160.5419 4804.017
161.0240 4757.856
161.5062 4739.958
161.9883 4715.329
162.4704 4666.233
162.9525 4599.859
163.4346 4528.738
163.9167 4451.538
164.3989 4375.233
164.8810 4307.591
165.3631 4254.546
165.8452 4198.347
166.3273 4129.598
166.8094 4048.831
167.2916 3959.276
167.7737 3844.250
168.2558 3727.354
168.7379 3637.374
169.2200 3597.527
169.7021 3565.814
170.1843 3503.740
170.6664 3415.396
171.1485 3326.739
171.6306 3258.966
172.1127 3202.136
172.5948 3140.728
173.0770 3058.266
173.5591 2974.434
174.0412 2918.782
174.5233 2875.065
175.0054 2829.304
175.4875 2748.251
175.9697 2642.343
176.4518 2540.253
176.9339 2448.322
177.4160 2369.066
177.8981 2316.701
178.3802 2296.277
178.8624 2276.218
179.3445 2208.445
179.8266 2104.581
180.3087 2016.155
180.7908 1991.065
181.2729 2001.859
181.7551 1969.923
182.2372 1878.095
182.7193 1763.655
183.2014 1682.151
183.6835 1631.304
184.1656 1591.432
184.6478 1558.199
185.1299 1526.530
185.6120 1474.003
186.0941 1388.987
186.5762 1293.352
187.0583 1231.713
187.5405 1207.066
188.0226 1191.248
188.5047 1158.159
188.9868 1110.186
189.4689 1063.807
189.9510 1022.873
190.4332 988.3906
190.9153 966.2954
191.3974 958.0186
191.8795 949.4565
192.3616 923.5581
192.8437 880.5874
193.3259 835.4194
193.8080 793.2192
194.2901 753.5376
194.7722 709.5117
195.2543 656.9116
195.7364 611.6348
196.2186 599.8276
196.7007 624.1714
197.1828 650.7456
197.6649 670.0601
198.1470 682.4902
198.6291 674.9004
199.1112 642.8857
199.5934 598.6538
200.0755 559.9287
200.5576 525.3179
201.0397 504.0776
201.5218 508.0684
202.0039 539.4727
202.4861 549.3521
202.9682 529.0996
203.4503 493.0420
203.9324 475.6191
204.4145 480.6177
204.8966 487.4453
205.3788 481.9585
205.8609 463.3198
206.3430 447.6436
206.8251 437.4648
207.3072 431.2456
207.7893 423.3589
208.2715 411.2266
208.7536 402.1240
209.2357 403.6597
209.7178 420.8208
210.1999 428.9199
210.6820 422.2344
211.1642 367.1333
211.6463 411.7729
212.1284 437.7661
212.6105 443.6992
213.0926 368.9619
213.5747 392.5859
214.0569 377.5332
214.5390 362.9160
215.0211 403.5581
215.5032 338.6128
215.9853 372.3384
216.4674 365.3896
216.9496 377.2593
217.4317 349.1733
217.9138 333.7524
218.3959 358.7920
218.8780 361.8071
219.3601 330.0688
219.8423 344.5820
220.3244 277.1250
220.8065 282.0435
221.2886 318.3228
221.7707 289.7891
222.2528 306.2144
222.7349 305.8384
223.2171 228.2803
223.6992 285.5815
224.1813 284.8916
224.6634 224.6494
225.1455 278.0273
225.6276 226.4883
226.1098 212.7104
226.5919 227.4082
227.0740 212.8916
227.5561 245.0303
228.0382 232.6763
228.5203 193.6147
229.0025 211.3462
229.4846 231.9888
229.9667 239.0703
230.4488 225.7925
230.9309 215.1636
231.4130 210.3862
231.8952 207.7148
232.3773 194.0757
232.8594 157.4917
233.3415 126.0728
233.8236 116.3091
234.3057 144.2451
234.7879 158.9780
235.2700 156.8257
235.7521 139.8789
236.2342 114.5850
236.7163 67.81592
237.1984 29.62061
237.6806 21.13916
238.1627 63.72217
238.6448 90.76025
239.1269 92.22217
239.6090 72.10498
240.0911 56.55225
240.5733 48.54199
241.0554 41.52637
241.5375 27.92188
242.0196 8.285156
242.5017 16.20557
242.9838 26.83838
243.4660 113.0757
243.9481 148.3408
244.4302 104.4038
244.9123 41.69189
245.3944 9.503906
245.8765 30.20459
246.3586 36.96875
246.8408 17.21582
247.3229 27.92529
247.8050 72.65088
248.2871 127.3037
248.7692 170.1870
249.2513 177.4385
249.7335 125.4077
250.2156 87.03320
250.6977 78.27490
251.1798 99.54150
251.6619 114.8735
252.1440 120.9897
252.6262 124.8110
253.1083 134.1982
253.5904 154.6040
254.0725 168.8271
254.5546 171.6143
255.0367 162.2485
255.5189 155.6309
256.0010 150.4150
256.4831 149.2109
256.9652 155.5137
257.4473 171.3574
257.9294 190.8076
258.4116 217.9805
258.8937 255.2925
259.3758 259.7295
259.8579 212.9829
260.3400 154.7671
260.8221 138.2100
261.3043 183.6719
261.7864 217.9277
262.2685 214.8579
262.7506 169.9966
263.2327 148.2700
263.7148 157.0659
264.1970 179.1191
264.6791 192.6890
265.1612 196.9565
265.6433 194.7383
266.1254 185.7471
266.6075 169.8730
267.0897 150.8701
267.5718 124.0127
268.0539 100.8315
268.5360 105.2529
269.0181 148.9033
269.5002 177.5239
269.9824 163.3628
270.4645 102.8252
270.9466 76.67090
271.4287 98.34180
271.9108 133.2314
272.3929 125.8193
272.8751 67.83740
273.3572 8.984375
273.8393 32.37012
274.3214 55.88672
274.8035 75.50195
275.2856 90.97510
275.7678 103.4648
276.2499 112.2529
276.7320 116.2427
277.2141 124.8462
277.6962 143.5435
278.1783 172.4443
278.6604 199.9341
279.1425 226.9434
279.6247 251.2666
280.1068 263.1367
280.5889 260.8101
281.0710 273.9795
281.5531 325.9248
282.0352 412.6099
282.5174 474.9980
282.9995 507.7026
283.4816 529.0713
283.9637 568.3687
284.4458 625.3999
284.9279 673.6309
285.4101 694.3008
285.8922 692.8262
286.3743 703.7939
286.8564 728.0713
287.3385 762.4443
287.8206 803.1870
288.3028 850.2773
288.7849 901.3330
289.2670 961.3521
289.7491 1025.499
290.2312 1072.466
290.7133 1098.449
291.1955 1119.336
291.6776 1148.842
292.1597 1188.584
292.6418 1246.450
293.1239 1350.868
293.6060 1475.868
294.0882 1544.190
294.5703 1546.813
295.0524 1533.549
295.5345 1561.313
296.0166 1624.327
296.4987 1694.810
296.9809 1771.876
297.4630 1844.866
297.9451 1887.261
298.4272 1895.125
298.9093 1897.121
299.3914 1930.090
299.8736 1979.567
300.3557 2011.059
300.8378 1984.824
301.3199 1945.037
301.8020 1957.035
302.2841 2028.049
302.7663 2099.517
303.2484 2114.391
303.7305 2096.651
304.2126 2087.312
304.6947 2094.871
305.1768 2121.473
305.6590 2186.444
306.1411 2294.479
306.6232 2378.810
307.1053 2368.556
307.5874 2313.922
308.0695 2285.998
308.5517 2301.386
309.0338 2358.680
309.5159 2481.227
309.9980 2672.799
310.4801 2842.220
310.9622 2906.069
311.4444 2924.642
311.9265 2974.847
312.4086 3095.213
312.8907 3248.062
313.3728 3417.037
313.8549 3601.438
314.3371 3794.275
314.8192 3974.940
315.3013 4166.592
315.7834 4389.611
316.2655 4669.763
316.7477 4963.028
317.2298 5255.287
317.7119 5549.158
318.1940 5858.037
318.6761 6163.800
319.1582 6486.483
319.6404 6845.473
320.1225 7294.830
320.6046 7736.803
321.0867 8131.957
321.5688 8481.665
322.0509 8862.149
322.5330 9291.070
323.0151 9752.704
323.4973 10240.29
323.9794 10794.85
324.4615 11330.67
324.9436 11826.46
325.4257 12286.07
325.9078 12764.52
326.3900 13236.94
326.8721 13736.19
327.3542 14287.60
327.8363 14925.62
328.3184 15578.40
328.8005 16270.65
329.2827 16976.35
329.7648 17590.80
330.2469 18063.99
330.7290 18512.33
331.2111 18991.60
331.6932 19533.41
332.1754 20045.25
332.6575 20532.42
333.1396 20983.98
333.6217 21373.00
334.1038 21683.90
334.5859 21962.77
335.0681 22238.25
335.5502 22525.01
336.0323 22756.08
336.5144 22916.07
336.9965 23028.40
337.4786 23156.90
337.9608 23307.48
338.4429 23445.37
338.9250 23541.60
339.4071 23589.94
339.8892 23673.84
340.3713 23804.54
340.8535 23956.70
341.3356 24084.05
341.8177 24187.10
342.2998 24279.60
342.7819 24380.38
343.2640 24482.86
343.7462 24538.90
344.2283 24548.30
344.7104 24513.01
345.1925 24433.39
345.6746 24310.23
346.1567 24152.59
346.6389 23965.99
347.1210 23747.61
347.6031 23472.26
348.0852 23136.95
348.5673 22784.05
349.0494 22441.79
349.5316 22118.86
350.0137 21833.51
350.4958 21601.84
350.9779 21411.36
351.4600 21255.21
351.9421 21133.13
352.4243 21005.01
352.9064 20833.74
353.3885 20637.68
353.8706 20446.47
354.3527 20302.92
354.8348 20142.43
355.3170 19903.96
355.7991 19593.87
356.2812 19262.45
356.7633 18954.88
357.2454 18633.63
357.7275 18260.64
358.2097 17800.71
358.6918 17313.43
359.1739 16803.25
359.6560 16282.20
360.1381 15810.45
360.6202 15402.64
361.1024 15056.59
361.5845 14775.11
362.0666 14600.44
362.5487 14427.15
363.0308 14219.31
363.5129 13994.10
363.9951 13800.84
364.4772 13667.04
364.9593 13554.20
365.4414 13442.33
365.9235 13295.33
366.4056 13214.19
366.8878 13249.94
367.3698 13346.67
367.8520 13406.92
368.3341 13408.40
368.8162 13399.52
369.2983 13399.76
369.7804 13423.09
370.2625 13402.04
370.7447 13337.63
371.2268 13227.95
371.7089 13061.14
372.1910 12814.30
372.6731 12562.20
373.1552 12328.30
373.6374 12110.21
374.1195 11871.51
374.6016 11594.20
375.0837 11324.53
375.5658 11111.61
376.0479 10958.12
376.5301 10837.49
377.0122 10746.91
377.4943 10681.28
377.9764 10622.48
378.4585 10568.94
378.9406 10539.59
379.4228 10570.19
379.9049 10645.69
380.3870 10676.61
380.8691 10634.04
381.3512 10556.94
381.8333 10500.83
382.3155 10383.81
382.7976 10257.33
383.2797 10122.86
383.7618 9962.055
384.2439 9841.611
384.7260 9707.056
385.2082 9569.921
385.6903 9452.065
386.1724 9295.041
386.6545 9176.254
387.1366 9042.202
387.6187 8915.042
388.1009 8772.611
388.5830 8634.618
389.0651 8511.312
389.5472 8379.635
390.0293 8235.578
390.5114 8109.695
390.9936 7953.396
391.4757 7824.463
391.9578 7706.911
392.4399 7563.537
392.9220 7435.274
393.4041 7300.496
393.8863 7138.333
394.3684 7028.707
394.8505 6898.020
395.3326 6744.628
395.8147 6633.841
396.2968 6485.938
396.7790 6348.778
397.2611 6220.280
397.7432 6080.023
398.2253 5960.949
398.7074 5822.864
399.1895 5683.518
399.6717 5551.074
400.1538 5397.439
400.6359 5281.109
401.1180 5138.649
401.6001 5007.581
402.0822 4878.101
402.5644 4728.826
403.0465 4491.578
403.5286 4268.641
404.0107 4052.766
404.4928 3832.490
404.9749 3607.140
405.4571 3377.568
405.9392 3127.863
406.4213 2866.737
406.9034 2660.857
407.3855 2519.462
407.8676 2395.265
408.3498 2235.975
408.8319 2046.145
409.3140 1867.257
409.7961 1712.963
410.2782 1575.086
410.7603 1435.444
411.2425 1293.621
411.7246 1168.595
412.2067 1084.575
412.6888 1023.170
413.1709 954.7705
413.6530 868.7583
414.1351 779.2651
414.6172 695.2524
415.0994 617.5215
415.5815 543.4971
416.0636 464.4565
416.5457 393.9966
417.0278 343.5996
417.5099 320.5610
417.9921 300.5342
418.4742 269.7866
418.9563 236.5854
419.4384 213.2871
419.9205 224.1953
420.4026 226.2476
420.8848 200.0737
421.3669 140.2803
421.8490 87.02539
422.3311 40.09717
422.8132 4.262207
423.2953 16.24756
423.7775 7.719727
424.2596 2.779297
424.7417 5.412109
425.2238 14.74268
425.7059 26.21289
426.1880 41.77246
426.6702 56.20459
427.1523 65.93848
427.6344 69.55908
428.1165 73.78418
428.5986 78.54150
429.0807 84.39746
429.5629 95.51221
430.0450 113.3853
430.5271 124.9243
431.0092 123.4277
431.4913 109.7905
431.9734 84.63232
432.4556 44.30273
432.9377 9.882324
433.4198 13.04590
433.9019 45.86377
434.3840 74.61035
434.8661 79.44043
435.3483 77.74512
435.8304 102.0220
436.3125 149.6611
436.7946 189.1919
437.2767 190.4458
437.7589 172.4233
438.2410 160.4839
438.7231 167.0381
439.2052 170.9795
439.6873 148.2700
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