#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-04-26 13:27:53 +0300 (Thu, 26 Apr 2018) $
#$Revision: 465 $
#$URL: svn://172.16.1.111/rod/cif/2/10/00/2100002.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2100002
loop_
_publ_author_name
'Toman, K.'
_publ_section_title
;
 Ordering in olivenite-adamite solid solutions Locality: Tsumeb, Southwest
 Africa
;
_journal_name_full               'Acta Crystallographica, Section B'
_journal_page_first              715
_journal_page_last               721
_journal_paper_doi               10.1107/S0567740878003933
_journal_volume                  34
_journal_year                    1978
_chemical_compound_source        R050583
_chemical_formula_sum            'As Cu0.86 H O5 Zn1.14'
_chemical_name_mineral           Zincolivenite
_space_group_IT_number           58
_symmetry_space_group_name_Hall  '-P 2 2n'
_symmetry_space_group_name_H-M   'P n n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   8.50
_cell_length_b                   8.52
_cell_length_c                   5.99
_cell_volume                     433.796
_exptl_crystal_density_diffrn    4.366
_cod_original_formula_sum        'As Zn1.14 Cu.86 O5 H'
_cod_database_code               9011188
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050583.rod
_rod_data_source.block           3500000
_rod_database.code               2100002
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011188 COD http://www.crystallography.net/cod/9011188.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
142.6650 0.0000000E+00
143.1472 8.8623002E-02
143.6293 4.577148
144.1114 22.18811
144.5935 36.30481
145.0756 34.72803
145.5577 22.00293
146.0399 17.28516
146.5220 26.63220
147.0041 32.59668
147.4862 32.28296
147.9683 25.80432
148.4504 17.38843
148.9326 8.332520
149.4147 2.183594
149.8968 5.425903
150.3789 9.497070
150.8610 26.70068
151.3431 38.79822
151.8252 43.97168
152.3074 43.24438
152.7895 35.96960
153.2716 13.99646
153.7537 3.760254
154.2358 15.89575
154.7179 35.02673
155.2001 48.30188
155.6822 50.33081
156.1643 44.00537
156.6464 38.39282
157.1285 31.07910
157.6106 27.66577
158.0928 30.78809
158.5749 37.63159
159.0570 44.37085
159.5391 48.63379
160.0212 50.81226
160.5033 55.24432
160.9855 58.69299
161.4676 67.13928
161.9497 85.94427
162.4318 112.1252
162.9139 137.2571
163.3960 154.4248
163.8782 163.3109
164.3603 176.7980
164.8424 198.2694
165.3245 221.2670
165.8066 242.5109
166.2887 261.6390
166.7709 277.6345
167.2530 287.5393
167.7351 291.6482
168.2172 302.7487
168.6993 324.6655
169.1814 350.0074
169.6636 369.9556
170.1457 382.5110
170.6278 391.5449
171.1099 400.4324
171.5920 407.1083
172.0741 419.0204
172.5563 445.8484
173.0384 478.4857
173.5205 499.0959
174.0026 497.8882
174.4847 493.4249
174.9668 506.0020
175.4490 533.9810
175.9311 556.2497
176.4132 547.0085
176.8953 507.7544
177.3774 497.8798
177.8595 574.3235
178.3417 645.4760
178.8238 646.3859
179.3059 572.3957
179.7880 474.5682
180.2701 409.8905
180.7522 386.9586
181.2344 360.2906
181.7165 315.3006
182.1986 269.4156
182.6807 234.3120
183.1628 213.0896
183.6449 198.8175
184.1271 179.3137
184.6092 149.1042
185.0913 124.8536
185.5734 108.9273
186.0555 98.20203
186.5376 90.86957
187.0198 86.14594
187.5019 83.05804
187.9840 78.83313
188.4661 70.43103
188.9482 64.92590
189.4303 65.37451
189.9125 68.12781
190.3946 69.67126
190.8767 68.33368
191.3588 63.69604
191.8409 53.39801
192.3230 27.90637
192.8052 7.453552
193.2873 4.684082
193.7694 8.524109
194.2515 4.682251
194.7336 7.374756
195.2157 26.25641
195.6979 31.97913
196.1800 14.18347
196.6621 1.072571
197.1442 1.791626
197.6263 11.32477
198.1084 20.12952
198.5906 16.70886
199.0727 1.359070
199.5548 5.479858
200.0369 4.710571
200.5190 15.48822
201.0011 13.65833
201.4833 0.7336430
201.9654 7.879211
202.4475 1.053833
202.9296 26.20996
203.4117 46.77887
203.8938 61.19330
204.3760 71.43445
204.8581 77.76752
205.3402 80.03186
205.8223 82.47180
206.3044 87.41504
206.7865 95.17120
207.2687 107.1347
207.7508 126.4295
208.2329 149.5009
208.7150 170.2226
209.1971 187.5585
209.6792 205.2462
210.1614 227.0826
210.6435 251.5734
211.1256 275.4625
211.6077 296.4280
212.0898 316.1016
212.5719 338.1780
213.0541 363.4554
213.5362 389.9833
214.0183 415.3407
214.5004 440.4644
214.9825 468.2167
215.4646 502.6699
215.9468 541.5897
216.4289 573.5154
216.9110 590.0651
217.3931 611.6095
217.8752 656.7767
218.3573 717.2245
218.8395 768.6617
219.3216 786.9149
219.8037 775.4992
220.2858 780.8714
220.7679 822.3386
221.2500 860.8722
221.7322 877.9600
222.2143 876.5965
222.6964 868.7963
223.1785 865.5010
223.6606 867.3607
224.1427 858.9470
224.6249 830.3732
225.1070 799.3044
225.5891 773.6995
226.0712 752.2001
226.5533 728.1826
227.0354 693.9778
227.5176 647.6786
227.9997 605.4715
228.4818 569.9207
228.9639 536.5231
229.4460 504.5027
229.9281 473.5595
230.4103 443.3009
230.8924 413.9659
231.3745 386.0856
231.8566 356.0983
232.3387 319.7887
232.8208 284.8544
233.3030 253.6787
233.7851 226.9603
234.2672 205.6383
234.7493 192.1117
235.2314 190.9340
235.7135 180.6735
236.1957 152.2722
236.6778 123.7029
237.1599 103.7677
237.6420 93.50720
238.1241 89.95428
238.6062 90.79865
239.0884 99.54730
239.5705 100.6328
240.0526 92.79059
240.5347 79.95575
241.0168 59.56769
241.4989 33.92200
241.9811 13.36328
242.4632 11.55469
242.9453 39.84979
243.4274 51.10553
243.9095 32.38324
244.3916 8.898560
244.8738 4.146545
245.3559 4.517883
245.8380 1.102661
246.3201 5.298035
246.8022 7.583984
247.2843 9.762695
247.7665 15.09961
248.2486 18.13232
248.7307 13.03705
249.2128 8.5387997E-02
249.6949 14.68842
250.1770 23.84912
250.6592 27.00641
251.1413 24.26428
251.6234 6.632141
252.1055 10.90863
252.5876 13.78931
253.0697 1.067261
253.5519 13.35883
254.0340 13.37512
254.5161 6.377930
254.9982 19.59576
255.4803 23.15076
255.9624 22.51038
256.4445 18.87109
256.9267 13.13666
257.4088 11.35767
257.8909 22.19653
258.3730 48.87256
258.8551 70.51086
259.3372 84.99817
259.8194 95.13580
260.3015 103.7094
260.7836 110.7209
261.2657 116.9259
261.7478 121.8566
262.2299 124.9430
262.7121 136.8845
263.1942 162.5654
263.6763 193.9804
264.1584 227.8068
264.6405 263.0676
265.1227 292.8300
265.6048 306.1855
266.0869 302.0654
266.5690 318.7775
267.0511 377.1720
267.5332 443.3636
268.0154 487.5877
268.4975 508.3230
268.9796 525.4184
269.4617 554.0191
269.9438 595.1021
270.4259 638.9183
270.9081 689.5237
271.3902 739.7964
271.8723 781.2811
272.3544 814.5212
272.8365 851.0109
273.3186 900.7485
273.8008 963.1387
274.2829 1022.782
274.7650 1079.775
275.2471 1133.716
275.7292 1186.263
276.2113 1236.867
276.6935 1279.634
277.1756 1305.750
277.6577 1318.955
278.1398 1342.497
278.6219 1396.336
279.1040 1445.301
279.5862 1462.030
280.0683 1448.519
280.5504 1426.740
281.0325 1409.358
281.5146 1393.594
281.9967 1369.726
282.4789 1339.133
282.9610 1299.375
283.4431 1248.055
283.9252 1185.678
284.4073 1114.629
284.8894 1031.611
285.3716 943.4302
285.8537 868.9719
286.3358 815.4984
286.8179 767.6759
287.3000 717.4357
287.7821 665.7554
288.2643 617.4826
288.7464 574.3857
289.2285 536.2867
289.7106 502.0583
290.1927 474.6287
290.6748 446.3907
291.1570 409.4304
291.6391 368.0244
292.1212 336.4376
292.6033 322.3400
293.0854 318.3668
293.5675 310.1473
294.0497 297.3529
294.5318 282.6830
295.0139 264.8394
295.4960 245.8956
295.9781 231.2362
296.4602 223.5647
296.9424 218.8510
297.4245 209.1415
297.9066 192.5284
298.3887 180.2681
298.8708 179.5472
299.3529 184.7969
299.8351 185.8954
300.3172 179.7520
300.7993 170.9285
301.2814 166.2964
301.7635 166.5806
302.2456 163.6906
302.7278 153.3915
303.2099 139.6898
303.6920 126.2415
304.1741 112.9659
304.6562 103.9106
305.1383 106.4717
305.6205 121.5520
306.1026 130.9920
306.5847 130.8822
307.0668 124.5727
307.5489 112.4770
308.0310 95.11810
308.5132 79.77356
308.9953 73.46771
309.4774 77.79382
309.9595 84.40601
310.4416 92.56335
310.9237 102.0210
311.4059 114.7986
311.8880 130.8853
312.3701 142.6971
312.8522 141.0114
313.3343 126.5575
313.8164 118.3518
314.2986 121.0704
314.7807 125.5630
315.2628 126.6880
315.7449 124.9923
316.2270 123.2066
316.7091 122.6735
317.1913 123.5708
317.6734 126.5948
318.1555 133.1837
318.6376 139.9846
319.1197 146.7222
319.6018 152.7688
320.0840 157.0283
320.5661 159.1701
321.0482 158.7991
321.5303 154.0933
322.0124 142.8558
322.4945 131.1210
322.9767 117.0038
323.4588 103.8771
323.9409 98.20959
324.4230 102.8922
324.9051 112.2801
325.3872 114.9100
325.8694 105.8361
326.3515 98.67603
326.8336 98.88495
327.3157 99.34222
327.7978 91.31281
328.2799 72.87103
328.7621 50.77472
329.2442 33.94080
329.7263 24.45734
330.2084 16.24695
330.6905 7.868469
331.1726 1.692688
331.6548 1.126831
332.1369 5.629089
332.6190 9.856262
333.1011 7.768127
333.5832 2.690796
334.0653 7.581604
334.5475 1.159424
335.0296 4.979858
335.5117 2.871033
335.9938 5.381958
336.4759 11.94702
336.9580 10.47461
337.4402 1.126282
337.9223 5.332947
338.4044 7.994995
338.8865 8.915527
339.3686 7.349182
339.8507 4.475586
340.3329 2.610474
340.8150 3.239746
341.2971 5.429138
341.7792 4.653442
342.2613 8.282776
342.7434 12.34540
343.2256 4.546997
343.7077 27.23389
344.1898 38.58411
344.6719 32.29517
345.1540 15.34674
345.6361 3.326599
346.1183 3.356201
346.6004 5.028809
347.0825 2.947266
347.5646 11.81714
348.0467 14.79144
348.5288 10.75018
349.0110 4.102234
349.4931 0.3231200
349.9752 3.463867
350.4573 2.338623
350.9394 9.142456
351.4215 20.25647
351.9037 25.33630
352.3858 24.50732
352.8679 22.51349
353.3500 22.17090
353.8321 23.56506
354.3142 29.88251
354.7964 49.34369
355.2785 63.38306
355.7606 60.61957
356.2427 47.78223
356.7248 38.25281
357.2069 40.39850
357.6891 50.42706
358.1712 57.29047
358.6533 58.68378
359.1354 62.25568
359.6175 74.09027
360.0996 88.50586
360.5818 98.15619
361.0639 99.08716
361.5460 98.58032
362.0281 107.3702
362.5102 126.5888
362.9923 145.3644
363.4745 162.4440
363.9566 175.7939
364.4387 182.9534
364.9208 183.3043
365.4029 180.2583
365.8850 173.2569
366.3672 163.8714
366.8493 160.9105
367.3314 167.7282
367.8135 179.6038
368.2956 193.3713
368.7777 208.7717
369.2599 220.7787
369.7420 226.5470
370.2241 227.7581
370.7062 226.2170
371.1883 221.5577
371.6704 217.4459
372.1526 218.0924
372.6347 222.3823
373.1168 224.0593
373.5989 224.3349
374.0810 220.4371
374.5631 206.2678
375.0453 183.1730
375.5274 164.3456
376.0095 158.6663
376.4916 163.2538
376.9737 164.2094
377.4558 159.7263
377.9380 154.9460
378.4201 153.6254
378.9022 153.5372
379.3843 148.7520
379.8664 134.2355
380.3485 115.8667
380.8307 106.1131
381.3128 111.9724
381.7949 113.5333
382.2770 106.7512
382.7591 96.57047
383.2412 87.35522
383.7234 80.05295
384.2055 73.62784
384.6876 66.54529
385.1697 57.48364
385.6518 53.87006
386.1339 61.71420
386.6161 68.50635
387.0982 67.54825
387.5803 60.04395
388.0624 50.39795
388.5445 41.30310
389.0266 33.32629
389.5088 30.73492
389.9909 45.20651
390.4730 51.16833
390.9551 37.06543
391.4372 14.42471
391.9193 2.405701
392.4015 6.424164
392.8836 2.252045
393.3657 1.860016
393.8478 5.982483
394.3299 8.579895
394.8120 10.38629
395.2942 11.40805
395.7763 9.509369
396.2584 4.867340
396.7405 1.275940
397.2226 4.312378
397.7047 14.04614
398.1869 18.02121
398.6690 9.220276
399.1511 2.082397
399.6332 8.662872
400.1153 23.42780
400.5974 31.81122
401.0796 21.70114
401.5617 1.816284
402.0438 5.866028
402.5259 1.395447
403.0080 10.04507
403.4901 13.22531
403.9723 13.20953
404.4544 12.22305
404.9365 11.75314
405.4186 10.57004
405.9007 6.631439
406.3828 0.7032780
406.8650 2.394714
407.3471 0.2231140
407.8292 4.748047
408.3113 4.556641
408.7934 1.674835
409.2755 4.901276
409.7577 0.8538820
410.2398 9.981384
410.7219 14.35663
411.2040 12.51953
411.6861 9.151886
412.1682 9.171509
412.6504 13.24548
413.1325 14.34772
413.6146 6.540039
414.0967 1.254089
414.5788 7.975250
415.0609 23.15515
415.5431 35.63077
416.0252 38.39905
416.5073 33.37872
416.9894 29.60358
417.4715 26.66647
417.9536 25.55734
418.4358 26.72974
418.9179 29.62698
419.4000 35.27710
419.8821 43.50516
420.3642 50.22461
420.8463 47.61172
421.3285 29.10147
421.8106 19.52002
422.2927 26.42752
422.7748 35.11841
423.2569 38.57343
423.7390 37.23431
424.2212 35.41077
424.7033 36.55118
425.1854 40.03943
425.6675 41.89417
426.1496 40.74561
426.6317 40.27740
427.1139 45.28497
427.5960 50.59464
428.0781 48.36606
428.5602 34.00598
429.0423 16.78336
429.5244 9.348938
430.0066 11.95584
430.4887 12.63947
430.9708 6.447205
431.4529 1.535980
431.9350 5.564819
432.4171 5.494324
432.8993 4.434113
433.3814 5.565796
433.8635 6.273468
434.3456 1.411041
434.8277 20.07193
435.3098 33.75137
435.7920 24.48441
436.2741 5.290771
436.7562 20.40366
437.2383 6.545135
437.7204 10.15839
438.2025 12.85721
438.6847 5.576996
439.1668 1.312347
439.6489 6.614471
440.1310 18.40155
440.6131 28.45898
441.0952 39.31061
441.5774 44.76331
442.0595 42.00296
442.5416 35.23019
443.0237 27.02448
443.5058 18.44730
443.9879 11.07144
444.4701 6.986023
444.9522 6.891449
445.4343 5.207367
445.9164 1.863678
446.3985 6.669464
446.8806 6.186920
447.3628 1.680084
447.8449 4.554443
448.3270 11.58740
448.8091 18.85135
449.2912 25.67352
449.7733 33.25580
450.2555 35.80344
450.7376 24.50259
451.2197 12.93796
451.7018 13.94766
452.1839 29.38239
452.6660 43.40793
453.1482 39.92657
453.6303 23.23502
454.1124 13.96356
454.5945 16.33002
455.0766 22.06714
455.5587 25.85892
456.0409 27.69519
456.5230 26.64087
457.0051 17.64636
457.4872 9.424255
457.9693 10.67978
458.4514 20.12100
458.9336 31.71964
459.4156 44.69217
459.8978 54.80954
460.3799 49.75162
460.8620 13.09552
461.3441 6.484589
461.8262 14.97736
462.3083 49.37436
462.7905 66.51865
463.2726 61.37000
463.7547 48.36847
464.2368 42.16238
464.7189 43.39346
465.2010 44.97330
465.6832 44.32611
466.1653 46.45776
466.6474 54.79745
467.1295 66.42371
467.6116 77.39990
468.0938 85.08569
468.5759 90.46091
469.0580 95.49417
469.5401 100.0361
470.0222 104.6929
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1275.639 5.2521002E-02
1276.121 3.256836
1276.603 0.0000000E+00
