#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-05-24 15:21:51 +0300 (Thu, 24 May 2018) $
#$Revision: 676 $
#$URL: svn://172.16.1.111/rod/cif/2/10/00/2100019.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2100019
loop_
_publ_author_name
'Toman, K.'
_publ_section_title
;
 Ordering in olivenite-adamite solid solutions Locality: Tsumeb, Southwest
 Africa
;
_journal_name_full               'Acta Crystallographica, Section B'
_journal_page_first              715
_journal_page_last               721
_journal_paper_doi               10.1107/S0567740878003933
_journal_volume                  34
_journal_year                    1978
_chemical_compound_source        R050583
_chemical_formula_sum            'As Cu0.86 H O5 Zn1.14'
_chemical_name_mineral           Zincolivenite
_space_group_IT_number           58
_symmetry_space_group_name_Hall  '-P 2 2n'
_symmetry_space_group_name_H-M   'P n n m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   8.50
_cell_length_b                   8.52
_cell_length_c                   5.99
_cell_volume                     433.796
_exptl_crystal_density_diffrn    4.366
_cod_original_formula_sum        'As Zn1.14 Cu.86 O5 H'
_cod_database_code               9011188
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R050583.rod
_rod_data_source.block           3500000
_rod_database.code               2100019
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011188 COD http://www.crystallography.net/cod/9011188.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
110.4850 0.0000000E+00
110.9671 45.12244
111.4492 147.8479
111.9313 300.2936
112.4134 514.2642
112.8956 654.4695
113.3777 669.2913
113.8598 602.8267
114.3419 514.4503
114.8240 380.7246
115.3061 253.2560
115.7883 156.4701
116.2704 94.89807
116.7525 57.93335
117.2346 48.03320
117.7167 60.94446
118.1988 83.05481
118.6810 116.0674
119.1631 152.7351
119.6452 186.2535
120.1273 212.3612
120.6094 238.8605
121.0915 270.9552
121.5737 307.5094
122.0558 341.5531
122.5379 370.6873
123.0200 394.3322
123.5021 411.3862
123.9842 414.0603
124.4664 412.6770
124.9485 420.4355
125.4306 440.7429
125.9127 464.4600
126.3948 482.8650
126.8769 496.6177
127.3591 508.9023
127.8412 515.2797
128.3233 521.3779
128.8054 545.8810
129.2875 596.7555
129.7696 662.0127
130.2518 727.4639
130.7339 794.6616
131.2160 859.8723
131.6981 908.0930
132.1802 942.3762
132.6623 991.1111
133.1445 1064.342
133.6266 1163.877
134.1087 1309.927
134.5908 1521.714
135.0729 1736.368
135.5550 1858.708
136.0372 1886.130
136.5193 1842.906
137.0014 1722.003
137.4835 1517.757
137.9656 1324.209
138.4477 1149.355
138.9299 990.2614
139.4120 826.6709
139.8941 647.6296
140.3762 485.8177
140.8583 364.8159
141.3404 294.1232
141.8226 236.7001
142.3047 187.3467
142.7868 146.4425
143.2689 110.8142
143.7510 79.65796
144.2331 54.62158
144.7152 39.25073
145.1974 42.09644
145.6795 41.11462
146.1616 28.59302
146.6437 2.641479
147.1258 27.10706
147.6079 42.71436
148.0901 51.70178
148.5722 59.52917
149.0543 66.50488
149.5364 72.19214
150.0185 76.41199
150.5006 81.83618
150.9828 82.68665
151.4649 77.50598
151.9470 66.73157
152.4291 55.25073
152.9112 43.81995
153.3933 31.55786
153.8755 17.68726
154.3576 3.880127
154.8397 12.95349
155.3218 36.12085
155.8039 67.94421
156.2860 91.91284
156.7682 91.68811
157.2503 85.21802
157.7324 95.01843
158.2145 143.4841
158.6966 195.6140
159.1787 234.8640
159.6609 249.8888
160.1430 273.2255
160.6251 318.9121
161.1072 380.0916
161.5893 441.5071
162.0714 500.8840
162.5536 556.3286
163.0357 605.7246
163.5178 634.7582
163.9999 673.4137
164.4820 739.7837
164.9641 830.4863
165.4463 922.6775
165.9284 1002.638
166.4105 1078.918
166.8926 1160.718
167.3747 1234.608
167.8568 1326.612
168.3390 1455.501
168.8211 1623.878
169.3032 1811.911
169.7853 2032.832
170.2674 2262.565
170.7495 2459.088
171.2317 2606.940
171.7138 2710.809
172.1959 2760.738
172.6780 2740.287
173.1601 2720.139
173.6422 2747.745
174.1244 2822.777
174.6065 2942.537
175.0886 3117.439
175.5707 3333.739
176.0528 3577.510
176.5349 3859.678
177.0171 4144.555
177.4992 4413.420
177.9813 4659.952
178.4634 4850.519
178.9455 4964.252
179.4276 5001.505
179.9098 4965.563
180.3919 4850.841
180.8740 4666.746
181.3561 4407.268
181.8382 4072.241
182.3203 3712.684
182.8025 3366.086
183.2846 3036.574
183.7667 2725.883
184.2488 2433.838
184.7309 2161.077
185.2130 1924.184
185.6951 1720.828
186.1773 1549.052
186.6594 1411.115
187.1415 1305.400
187.6236 1208.091
188.1057 1096.429
188.5878 978.9561
189.0700 895.7152
189.5521 858.5200
190.0342 845.5720
190.5163 815.5847
190.9984 768.7998
191.4805 726.8538
191.9627 707.6018
192.4448 709.2123
192.9269 711.2900
193.4090 707.9199
193.8911 703.9250
194.3732 714.0590
194.8554 739.1409
195.3375 773.9033
195.8196 813.6777
196.3017 858.2135
196.7838 910.8623
197.2659 975.6556
197.7481 1050.204
198.2302 1115.406
198.7123 1169.758
199.1944 1219.413
199.6765 1273.606
200.1586 1335.130
200.6408 1388.149
201.1229 1428.326
201.6050 1454.781
202.0871 1469.114
202.5692 1470.859
203.0513 1461.759
203.5335 1443.285
204.0156 1414.104
204.4977 1380.442
204.9798 1343.603
205.4619 1303.808
205.9440 1262.522
206.4262 1216.713
206.9083 1171.666
207.3904 1142.750
207.8725 1134.463
208.3546 1129.902
208.8367 1117.798
209.3189 1094.447
209.8010 1080.439
210.2831 1076.550
210.7652 1083.219
211.2473 1102.387
211.7294 1134.031
212.2116 1178.494
212.6937 1234.635
213.1758 1301.385
213.6579 1384.003
214.1400 1486.008
214.6221 1607.036
215.1043 1730.475
215.5864 1851.275
216.0685 1983.858
216.5506 2140.482
217.0327 2324.614
217.5148 2527.705
217.9970 2750.683
218.4791 2991.768
218.9612 3249.628
219.4433 3519.373
219.9254 3807.298
220.4075 4122.833
220.8897 4468.353
221.3718 4833.058
221.8539 5216.513
222.3360 5637.242
222.8181 6010.108
223.3002 6337.931
223.7824 6613.371
224.2645 6820.233
224.7466 6972.196
225.2287 7035.328
225.7108 6992.625
226.1929 6826.897
226.6750 6603.282
227.1572 6311.723
227.6393 5968.056
228.1214 5601.375
228.6035 5197.883
229.0856 4796.681
229.5677 4416.563
230.0499 4060.784
230.5320 3729.323
231.0141 3427.064
231.4962 3151.965
231.9783 2888.837
232.4604 2637.713
232.9426 2402.077
233.4247 2179.741
233.9068 1969.855
234.3889 1783.405
234.8710 1626.721
235.3531 1495.970
235.8353 1368.455
236.3174 1241.071
236.7995 1120.519
237.2816 1011.531
237.7637 914.0190
238.2458 828.7039
238.7280 759.2969
239.2101 705.4930
239.6922 646.2203
240.1743 575.4175
240.6564 505.1080
241.1385 447.5111
241.6207 409.5626
242.1028 370.5614
242.5849 325.1276
243.0670 272.3361
243.5491 224.6278
244.0313 182.6738
244.5134 145.2311
244.9955 110.2559
245.4776 74.15552
245.9597 46.97717
246.4418 33.91614
246.9240 38.96875
247.4061 34.38025
247.8882 15.41699
248.3703 9.668213
248.8524 29.06042
249.3345 41.25366
249.8167 50.38440
250.2988 57.45007
250.7809 62.08374
251.2630 66.16003
251.7451 69.54688
252.2272 72.46277
252.7094 75.77625
253.1915 81.83215
253.6736 84.29126
254.1557 79.74976
254.6378 64.48352
255.1199 54.64368
255.6021 55.02478
256.0842 58.60156
256.5663 48.14673
257.0484 14.10925
257.5305 17.50366
258.0126 31.59851
258.4948 13.84387
258.9769 20.72644
259.4590 61.32959
259.9411 123.8508
260.4232 175.6512
260.9053 208.5067
261.3875 245.9971
261.8696 302.3527
262.3517 382.2982
262.8338 462.2625
263.3159 537.3636
263.7980 612.4561
264.2802 701.2916
264.7623 806.7480
265.2444 921.6569
265.7265 1043.345
266.2086 1168.229
266.6907 1305.067
267.1729 1455.397
267.6550 1616.482
268.1371 1781.380
268.6192 1946.647
269.1013 2119.985
269.5834 2305.203
270.0656 2499.651
270.5477 2705.948
271.0298 2921.551
271.5119 3147.305
271.9940 3392.589
272.4761 3655.583
272.9583 3937.985
273.4404 4238.988
273.9225 4553.830
274.4046 4914.580
274.8867 5332.019
275.3688 5798.027
275.8510 6287.873
276.3331 6796.663
276.8152 7336.237
277.2973 7912.282
277.7794 8523.192
278.2615 9192.392
278.7437 9952.318
279.2258 10770.82
279.7079 11520.00
280.1900 12210.83
280.6721 12790.37
281.1542 13234.27
281.6364 13546.73
282.1185 13646.54
282.6006 13501.11
283.0827 13135.07
283.5648 12626.49
284.0469 11965.39
284.5291 11214.22
285.0112 10395.44
285.4933 9512.176
285.9754 8666.296
286.4575 7874.822
286.9396 7146.962
287.4217 6540.348
287.9038 6061.831
288.3860 5653.491
288.8681 5260.148
289.3502 4887.681
289.8323 4557.728
290.3144 4284.472
290.7965 4058.433
291.2787 3861.631
291.7608 3694.219
292.2429 3547.726
292.7250 3422.331
293.2071 3313.041
293.6892 3193.729
294.1714 3052.276
294.6535 2898.795
295.1356 2750.757
295.6177 2607.547
296.0998 2473.017
296.5819 2352.887
297.0641 2243.256
297.5462 2133.067
298.0283 2015.923
298.5104 1897.730
298.9925 1787.883
299.4746 1685.937
299.9568 1586.787
300.4389 1480.121
300.9210 1371.948
301.4031 1273.261
301.8852 1187.934
302.3673 1115.473
302.8495 1055.531
303.3316 1008.502
303.8137 970.0654
304.2958 942.9635
304.7779 921.8503
305.2600 897.2732
305.7422 860.0692
306.2243 819.9941
306.7064 786.2249
307.1885 758.9005
307.6706 738.9220
308.1527 729.8997
308.6349 728.0177
309.1170 727.9441
309.5991 731.5386
310.0812 733.6255
310.5633 728.2454
311.0454 715.8013
311.5276 705.8723
312.0097 704.2354
312.4918 709.2635
312.9739 718.1624
313.4560 722.7350
313.9381 735.9025
314.4203 769.2209
314.9024 822.9607
315.3845 879.0826
315.8666 930.1409
316.3487 976.8662
316.8308 1021.101
317.3130 1055.501
317.7951 1094.639
318.2772 1144.016
318.7593 1203.349
319.2414 1267.311
319.7235 1340.920
320.2057 1414.999
320.6878 1482.285
321.1699 1542.524
321.6520 1594.659
322.1341 1640.963
322.6162 1680.721
323.0984 1703.743
323.5805 1722.817
324.0626 1716.034
324.5447 1668.623
325.0268 1544.556
325.5089 1417.200
325.9911 1295.146
326.4732 1178.921
326.9553 1061.423
327.4374 936.5273
327.9195 814.1794
328.4016 698.5054
328.8838 579.0460
329.3659 479.5996
329.8480 409.1196
330.3301 363.1343
330.8122 311.3530
331.2943 243.8539
331.7765 179.9017
332.2586 130.5204
332.7407 101.4927
333.2228 76.59631
333.7049 54.19312
334.1870 35.15381
334.6692 23.78210
335.1513 25.55029
335.6334 26.07703
336.1155 15.58521
336.5976 12.37439
337.0797 30.67969
337.5619 35.28735
338.0440 30.19226
338.5261 27.55505
339.0082 28.98279
339.4903 28.04028
339.9724 18.83069
340.4546 0.1181640
340.9367 13.92603
341.4188 21.36865
341.9009 25.18262
342.3830 30.96301
342.8651 38.31213
343.3473 48.27075
343.8294 60.31775
344.3115 74.95593
344.7936 95.60815
345.2757 123.9098
345.7578 155.6748
346.2400 186.3923
346.7221 215.2535
347.2042 240.0468
347.6863 257.3871
348.1684 269.8672
348.6505 285.8943
349.1327 306.7506
349.6148 327.5880
350.0969 340.4534
350.5790 347.1182
351.0611 355.7632
351.5432 379.5151
352.0254 405.9299
352.5075 412.0178
352.9896 395.3341
353.4717 374.4205
353.9538 363.5695
354.4359 360.9369
354.9181 363.4529
355.4002 379.0341
355.8823 393.5864
356.3644 388.8389
356.8465 364.4313
357.3286 345.7812
357.8108 349.5211
358.2929 368.7664
358.7750 394.3462
359.2571 429.2377
359.7392 464.3333
360.2213 492.3247
360.7035 513.9326
361.1856 540.2241
361.6677 572.0649
362.1498 612.5730
362.6319 664.7197
363.1140 741.0256
363.5962 817.1033
364.0783 884.2593
364.5604 943.9529
365.0425 1006.826
365.5246 1067.851
366.0067 1137.791
366.4889 1223.029
366.9710 1352.254
367.4531 1464.967
367.9352 1548.772
368.4173 1609.753
368.8994 1674.904
369.3815 1747.944
369.8636 1822.170
370.3458 1894.501
370.8279 1970.803
371.3100 2036.448
371.7921 2092.255
372.2742 2137.731
372.7563 2172.441
373.2385 2197.996
373.7206 2208.725
374.2027 2202.257
374.6848 2178.677
375.1669 2139.549
375.6490 2080.604
376.1312 2009.284
376.6133 1937.365
377.0954 1866.035
377.5775 1791.860
378.0596 1708.480
378.5417 1617.654
379.0239 1542.991
379.5060 1489.463
379.9881 1438.303
380.4702 1366.439
380.9523 1274.221
381.4344 1180.089
381.9166 1084.700
382.3987 993.1362
382.8808 915.3728
383.3629 852.0210
383.8450 793.7655
384.3271 734.6422
384.8093 674.9476
385.2914 615.7874
385.7735 556.0187
386.2556 498.8256
386.7377 450.4545
387.2198 410.7639
387.7020 376.2692
388.1841 348.9983
388.6662 324.6729
389.1483 293.6930
389.6304 239.0909
390.1125 201.8835
390.5947 243.0646
391.0768 333.4667
391.5589 380.5677
392.0410 294.7073
392.5231 175.1034
393.0052 93.99292
393.4874 75.72083
393.9695 68.10718
394.4516 51.58398
394.9337 31.14600
395.4158 16.68945
395.8979 19.14917
396.3801 21.44666
396.8622 14.90393
397.3443 5.445801
397.8264 18.78259
398.3085 14.78064
398.7906 5.088867
399.2728 3.534912
399.7549 21.25159
400.2370 35.03528
400.7191 38.98621
401.2012 32.18677
401.6833 29.17590
402.1655 31.42163
402.6476 35.92371
403.1297 41.07764
403.6118 49.74316
404.0939 51.50598
404.5760 41.98438
405.0582 24.07019
405.5403 14.25122
406.0224 14.62134
406.5045 17.16003
406.9866 17.86267
407.4688 16.95154
407.9509 9.069458
408.4330 8.689697
408.9151 30.46228
409.3972 44.09839
409.8793 49.51428
410.3615 51.63928
410.8436 50.79602
411.3257 48.63806
411.8078 51.20361
412.2899 59.32739
412.7720 70.14490
413.2542 79.50232
413.7363 88.55188
414.2184 100.8953
414.7005 122.4397
415.1826 145.9259
415.6647 163.1019
416.1469 173.5747
416.6290 179.8826
417.1111 179.7511
417.5932 177.5383
418.0753 179.0023
418.5574 190.1381
419.0396 201.7476
419.5217 210.8746
420.0038 217.0883
420.4859 218.1196
420.9680 209.9785
421.4501 198.1719
421.9323 186.6377
422.4144 174.8561
422.8965 164.8138
423.3786 158.9337
423.8607 155.2747
424.3428 148.1587
424.8250 133.9906
425.3071 118.9763
425.7892 105.3026
426.2713 92.77075
426.7534 81.53113
427.2355 72.13281
427.7177 63.63293
428.1998 55.21899
428.6819 47.96960
429.1640 38.00525
429.6461 21.67224
430.1282 0.5192870
430.6104 11.84363
431.0925 9.671265
431.5746 3.478271
432.0567 3.708252
432.5388 10.66418
433.0209 12.86084
433.5031 5.371094
433.9852 6.326050
434.4673 7.381470
434.9494 1.937134
435.4315 12.00134
435.9136 16.40234
436.3958 16.14453
436.8779 12.90027
437.3600 5.676270
437.8421 0.9809570
438.3242 1.746582
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