#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 16:37:57 +0300 (Thu, 24 May 2018) $ #$Revision: 915 $ #$URL: svn://172.16.1.111/rod/cif/2/10/00/2100035.rod $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100035 loop_ _publ_author_name 'Howard, C. J.' 'Sabine, T. M.' 'Dickson, F.' _publ_section_title ; Structural and thermal parameters for rutile and anatase ; _journal_issue 4 _journal_name_full 'Acta Crystallographica, Section B' _journal_page_first 462 _journal_page_last 468 _journal_paper_doi 10.1107/S010876819100335X _journal_volume 47 _journal_year 1991 _chemical_compound_source 'Synthetic 3' _chemical_formula_sum 'O2 Ti' _chemical_name_mineral Anatase _space_group_IT_number 141 _symmetry_space_group_name_Hall 'I 4bw 2bw -1bw' _symmetry_space_group_name_H-M 'I 41/a m d :1' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 3.7845 _cell_length_b 3.7845 _cell_length_c 9.5143 _cell_volume 136.268 _exptl_crystal_density_diffrn 3.894 _cod_original_sg_symbol_H-M 'I 41/a m d' _cod_original_formula_sum 'Ti O2' _cod_database_code 9015929 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R070582.rod _rod_data_source.block 3500000 _rod_database.code 2100035 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9015929 COD http://www.crystallography.net/cod/9015929.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 115.5325 0.0000000E+00 116.0146 91.28076 116.4967 31.44580 116.9788 36.87793 117.4609 24.60498 117.9431 49.11133 118.4252 175.8291 118.9073 348.4624 119.3894 549.3110 119.8715 788.8608 120.3536 1080.524 120.8358 1429.439 121.3179 1828.907 121.8000 2272.164 122.2821 2721.850 122.7642 3234.043 123.2464 3829.444 123.7285 4503.499 124.2106 5239.270 124.6927 6025.965 125.1748 6876.321 125.6569 7785.859 126.1391 8774.906 126.6212 9814.714 127.1033 10879.12 127.5854 11979.96 128.0675 13086.86 128.5496 14183.72 129.0318 15275.18 129.5139 16356.51 129.9960 17428.09 130.4781 18489.83 130.9602 19554.47 131.4423 20604.70 131.9245 21674.85 132.4066 22788.15 132.8887 23939.85 133.3708 25093.74 133.8529 26194.35 134.3350 27220.66 134.8172 28351.68 135.2993 29700.10 135.7814 31090.71 136.2635 32438.41 136.7456 33728.93 137.2277 35011.35 137.7099 36364.96 138.1920 37883.18 138.6741 39300.24 139.1562 40666.11 139.6383 41911.98 140.1204 43036.42 140.6026 44031.35 141.0847 44827.67 141.5668 45177.47 142.0489 44942.71 142.5310 44375.39 143.0131 43481.50 143.4953 42276.91 143.9774 40772.82 144.4595 38947.91 144.9416 36822.29 145.4237 34656.23 145.9058 32436.84 146.3880 30207.86 146.8701 27915.28 147.3522 25585.20 147.8343 23335.88 148.3164 21259.40 148.7985 19374.27 149.2807 17603.59 149.7628 15909.73 150.2449 14326.38 150.7270 12906.32 151.2091 11652.01 151.6912 10526.30 152.1734 9518.791 152.6555 8609.175 153.1376 7777.620 153.6197 7029.197 154.1018 6359.103 154.5839 5753.243 155.0661 5227.075 155.5482 4753.355 156.0303 4300.059 156.5124 3865.905 156.9945 3465.476 157.4766 3108.279 157.9588 2794.540 158.4409 2514.043 158.9230 2280.378 159.4051 2073.043 159.8872 1882.935 160.3694 1708.750 160.8515 1546.326 161.3336 1388.140 161.8157 1229.578 162.2978 1091.512 162.7799 984.9598 163.2621 892.3169 163.7442 803.3011 164.2263 714.0286 164.7084 626.3337 165.1905 541.7045 165.6726 456.1554 166.1548 381.7247 166.6369 324.0520 167.1190 275.9116 167.6011 231.1798 168.0832 186.3828 168.5653 141.1262 169.0475 92.32300 169.5296 27.65820 170.0117 27.09302 170.4938 64.13232 170.9759 88.45642 171.4580 108.3553 171.9402 129.4954 172.4223 151.9216 172.9044 174.8348 173.3865 197.8301 173.8686 218.1864 174.3507 231.8627 174.8329 239.6909 175.3150 246.3203 175.7971 258.2383 176.2792 276.7665 176.7613 285.3235 177.2434 282.0238 177.7256 271.5465 178.2077 255.4861 178.6898 234.3253 179.1719 211.7870 179.6540 191.5560 180.1361 173.7920 180.6183 155.5565 181.1004 135.6262 181.5825 115.4551 182.0646 97.81958 182.5467 83.96240 183.0288 69.31091 183.5110 46.09375 183.9931 15.55566 184.4752 12.01428 184.9573 29.70813 185.4394 41.88135 185.9215 59.37720 186.4037 86.26959 186.8858 116.0242 187.3679 141.8175 187.8500 163.7906 188.3321 185.2684 188.8142 205.7126 189.2964 226.0044 189.7785 253.5352 190.2606 291.5774 190.7427 336.7814 191.2248 386.3270 191.7069 440.1412 192.1891 496.9278 192.6712 557.2314 193.1533 621.7712 193.6354 682.6638 194.1175 747.6185 194.5996 802.2319 195.0818 837.3353 195.5639 850.9101 196.0460 846.0094 196.5281 823.5515 197.0102 777.3071 197.4923 731.0286 197.9745 687.3490 198.4566 646.3412 198.9387 608.6321 199.4208 574.0606 199.9029 542.2902 200.3850 511.4444 200.8672 478.5938 201.3493 452.4750 201.8314 436.0038 202.3135 424.4231 202.7956 412.9832 203.2777 399.6155 203.7599 386.1648 204.2420 378.0308 204.7241 380.9718 205.2062 382.5329 205.6883 380.1914 206.1704 376.1631 206.6526 372.8348 207.1347 371.5394 207.6168 372.2170 208.0989 374.2411 208.5810 377.0779 209.0631 382.0984 209.5453 391.2519 210.0274 402.5599 210.5095 413.0702 210.9916 421.0099 211.4737 426.6115 211.9559 431.9378 212.4380 438.3888 212.9201 443.1445 213.4022 443.5306 213.8843 441.4593 214.3664 441.2288 214.8486 445.8797 215.3307 455.1973 215.8128 463.4456 216.2949 469.5553 216.7770 475.7970 217.2591 484.3214 217.7413 494.1340 218.2234 501.6245 218.7055 503.5664 219.1876 500.1703 219.6697 499.9665 220.1518 503.5866 220.6340 509.3804 221.1161 517.8409 221.5982 528.3542 222.0803 537.6768 222.5624 542.7938 223.0445 543.8265 223.5267 547.3457 224.0088 555.3295 224.4909 564.2003 224.9730 572.1613 225.4551 578.9952 225.9372 583.1906 226.4194 582.1049 226.9015 576.0453 227.3836 571.4396 227.8657 569.1320 228.3478 567.1236 228.8299 564.6175 229.3121 561.9020 229.7942 555.8909 230.2763 542.7128 230.7584 523.5257 231.2405 504.2242 231.7226 485.7264 232.2048 468.2153 232.6869 452.1099 233.1690 437.5947 233.6511 423.0616 234.1332 407.8847 234.6153 392.2227 235.0975 375.2574 235.5796 356.2551 236.0617 336.7580 236.5438 318.8038 237.0259 302.6023 237.5080 287.7150 237.9902 274.6066 238.4723 262.6441 238.9544 250.0518 239.4365 233.9240 239.9186 217.1056 240.4007 205.8133 240.8829 202.3680 241.3650 199.7853 241.8471 193.3069 242.3292 184.0570 242.8113 173.6662 243.2934 159.5654 243.7756 145.0402 244.2577 138.0146 244.7398 140.2074 245.2219 146.4053 245.7040 156.8461 246.1861 168.6814 246.6683 175.2408 247.1504 169.1013 247.6325 155.2474 248.1146 148.8247 248.5967 153.6366 249.0788 158.8952 249.5610 156.4773 250.0431 149.7485 250.5252 145.7840 251.0073 150.6735 251.4894 161.2469 251.9715 165.9322 252.4537 160.7292 252.9358 155.9915 253.4179 157.6768 253.9000 163.5080 254.3821 169.2129 254.8642 172.8066 255.3464 174.3499 255.8285 173.8661 256.3106 169.5536 256.7927 166.1899 257.2748 166.5287 257.7570 169.1154 258.2391 171.2646 258.7212 171.3809 259.2033 169.7537 259.6854 167.8741 260.1675 165.7864 260.6497 163.4963 261.1318 161.1201 261.6139 158.4735 262.0960 155.2701 262.5781 150.9928 263.0602 146.2605 263.5424 143.9891 264.0245 146.9867 264.5066 147.9256 264.9887 142.4488 265.4708 133.7304 265.9529 126.8793 266.4351 125.1858 266.9172 127.2339 267.3993 127.6610 267.8814 126.0639 268.3635 123.8345 268.8456 121.3364 269.3278 118.2931 269.8099 114.1373 270.2920 107.8291 270.7741 100.6841 271.2562 97.90701 271.7383 104.3188 272.2205 108.0755 272.7026 102.5418 273.1847 92.92830 273.6668 86.39175 274.1489 87.04771 274.6310 92.25432 275.1132 94.24960 275.5953 91.14258 276.0774 88.21783 276.5595 87.24960 277.0416 87.10730 277.5237 86.40114 278.0059 84.35001 278.4880 81.24939 278.9701 77.84122 279.4522 73.91258 279.9343 70.71658 280.4164 67.77847 280.8986 65.95480 281.3807 66.32578 281.8628 69.37711 282.3449 73.45207 282.8270 75.44574 283.3091 75.63965 283.7913 73.27396 284.2734 65.92801 284.7555 57.41710 285.2376 51.55421 285.7197 49.87503 286.2018 49.73878 286.6840 45.64600 287.1661 34.42209 287.6482 27.61731 288.1303 31.35342 288.6124 37.48700 289.0945 39.32590 289.5767 35.02301 290.0588 29.02927 290.5409 28.77222 291.0230 37.15353 291.5051 41.75861 291.9872 37.68362 292.4694 31.39774 292.9515 26.55679 293.4336 23.97269 293.9157 22.68192 294.3978 21.73865 294.8799 21.25687 295.3621 20.55911 295.8442 18.96893 296.3263 17.56180 296.8084 16.55896 297.2905 16.10358 297.7726 16.79672 298.2548 20.20026 298.7369 26.91858 299.2190 31.24411 299.7011 31.74323 300.1832 30.20496 300.6653 25.71860 301.1475 19.16687 301.6296 14.26227 302.1117 16.08139 302.5938 24.85205 303.0759 28.56015 303.5580 21.09027 304.0402 14.37589 304.5223 15.47015 305.0044 22.48373 305.4865 28.71292 305.9686 28.59872 306.4507 22.96271 306.9329 19.16965 307.4150 18.16211 307.8971 17.79858 308.3792 16.92615 308.8613 15.90070 309.3434 15.42468 309.8256 15.60156 310.3077 16.58514 310.7898 19.88229 311.2719 28.49466 311.7540 33.73767 312.2361 28.44897 312.7183 18.14792 313.2004 11.81735 313.6825 15.55023 314.1646 23.79590 314.6467 23.55093 315.1288 10.57724 315.6110 0.8714900 316.0931 5.999725 316.5752 16.59814 317.0573 21.77304 317.5394 16.54141 318.0215 7.308197 318.5037 3.435150 318.9858 5.974609 319.4679 7.725861 319.9500 4.705627 320.4321 6.1248999E-02 320.9142 3.315948 321.3964 4.797943 321.8785 5.205566 322.3606 5.030609 322.8427 4.301270 323.3248 3.767944 323.8069 2.416351 324.2891 2.493011 324.7712 7.163788 325.2533 17.37454 325.7354 26.65540 326.2175 30.60037 326.6996 29.68222 327.1818 25.46835 327.6639 14.78522 328.1460 5.727783 328.6281 8.468384 329.1102 22.80969 329.5923 34.84210 330.0745 36.54715 330.5566 31.14627 331.0387 26.00381 331.5208 21.80811 332.0029 19.06107 332.4850 18.84329 332.9672 20.71063 333.4493 23.07251 333.9314 27.42798 334.4135 31.19098 334.8957 29.43600 335.3778 21.12497 335.8599 13.22272 336.3420 11.82477 336.8241 15.97034 337.3062 20.30615 337.7884 27.87036 338.2705 32.86765 338.7526 27.84338 339.2347 13.57214 339.7168 0.4213260 340.1989 4.921570 340.6811 3.578522 341.1632 2.777161 341.6453 1.717316 342.1274 1.933990 342.6095 4.999878 343.0916 10.10040 343.5738 14.63995 344.0559 17.15152 344.5380 18.63889 345.0201 22.44186 345.5022 30.53027 345.9843 37.27499 346.4665 39.59091 346.9486 40.05255 347.4307 43.17145 347.9128 50.65240 348.3949 59.64178 348.8770 64.88641 349.3592 63.80432 349.8413 64.31827 350.3234 66.51797 350.8055 70.64587 351.2876 77.81970 351.7697 87.91525 352.2519 98.51447 352.7340 106.5396 353.2161 110.8428 353.6982 116.9858 354.1803 125.7564 354.6624 135.4386 355.1446 145.7656 355.6267 156.2528 356.1088 165.3904 356.5909 171.2636 357.0730 173.6631 357.5551 182.7019 358.0373 207.3848 358.5194 228.8689 359.0015 239.3366 359.4836 242.9604 359.9657 247.1673 360.4478 256.2538 360.9300 269.4667 361.4121 283.9189 361.8942 300.2111 362.3763 316.9225 362.8584 331.9798 363.3405 348.2536 363.8227 369.9800 364.3048 398.6385 364.7869 429.7003 365.2690 454.0783 365.7511 467.2656 366.2332 485.6954 366.7154 513.8458 367.1975 545.3697 367.6796 577.8245 368.1617 610.3396 368.6438 640.8353 369.1259 664.8229 369.6081 681.1723 370.0902 705.5632 370.5723 745.1172 371.0544 786.8138 371.5365 823.4838 372.0186 856.4033 372.5008 891.0618 372.9829 931.8928 373.4650 977.3978 373.9471 1021.101 374.4292 1061.644 374.9113 1103.143 375.3935 1148.485 375.8756 1196.245 376.3577 1244.018 376.8398 1290.283 377.3219 1337.047 377.8040 1387.983 378.2862 1443.358 378.7683 1496.953 379.2504 1542.511 379.7325 1586.689 380.2146 1639.458 380.6967 1703.658 381.1789 1770.563 381.6610 1837.911 382.1431 1904.113 382.6252 1962.388 383.1073 2009.984 383.5894 2050.417 384.0716 2088.744 384.5537 2125.083 385.0358 2160.125 385.5179 2194.457 386.0000 2227.549 386.4821 2256.524 386.9643 2280.359 387.4464 2306.336 387.9285 2343.507 388.4106 2393.785 388.8927 2434.163 389.3748 2466.276 389.8570 2487.552 390.3391 2491.981 390.8212 2483.167 391.3033 2473.130 391.7854 2469.621 392.2675 2470.504 392.7497 2462.265 393.2318 2445.077 393.7139 2419.779 394.1960 2383.408 394.6781 2339.220 395.1602 2291.313 395.6424 2241.035 396.1245 2189.286 396.6066 2138.172 397.0887 2094.489 397.5708 2039.654 398.0529 1964.134 398.5351 1885.150 399.0172 1815.567 399.4993 1755.722 399.9814 1695.940 400.4635 1624.599 400.9456 1540.000 401.4278 1465.821 401.9099 1411.655 402.3920 1358.788 402.8741 1300.191 403.3562 1238.155 403.8383 1177.061 404.3205 1119.517 404.8026 1064.865 405.2847 1009.489 405.7668 949.3207 406.2489 898.0798 406.7310 869.0869 407.2132 847.0295 407.6953 816.5833 408.1774 772.7696 408.6595 726.3451 409.1416 686.3446 409.6237 652.8406 410.1059 625.4548 410.5880 607.9769 411.0701 591.8527 411.5522 567.5615 412.0343 535.3513 412.5164 503.1959 412.9986 473.3535 413.4807 446.0156 413.9628 421.9932 414.4449 401.4856 414.9270 383.2438 415.4091 366.8715 415.8913 352.2390 416.3734 337.2705 416.8555 319.4263 417.3376 303.5621 417.8197 295.1606 418.3018 291.7399 418.7840 284.5150 419.2661 268.2313 419.7482 246.7079 420.2303 232.0358 420.7124 231.8196 421.1945 227.3634 421.6767 212.9668 422.1588 195.1414 422.6409 180.8987 423.1230 171.8674 423.6051 164.8762 424.0872 155.4045 424.5694 141.3710 425.0515 132.9035 425.5336 135.0848 426.0157 137.2409 426.4978 134.2769 426.9799 127.1774 427.4621 119.5204 427.9442 113.6557 428.4263 109.3638 428.9084 105.5777 429.3905 103.3553 429.8727 99.77771 430.3548 93.92563 430.8369 86.66260 431.3190 78.28461 431.8011 68.68347 432.2833 60.02060 432.7654 54.90833 433.2475 53.37302 433.7296 54.93411 434.2117 63.58450 434.6938 70.96347 435.1760 69.53693 435.6581 60.05634 436.1402 50.46930 436.6223 45.01846 437.1044 42.08218 437.5865 38.58176 438.0687 34.22800 438.5508 29.92947 439.0329 25.47437 439.5150 21.68817 439.9971 21.17804 440.4792 29.45285 440.9614 35.80408 441.4435 32.67004 441.9256 22.83920 442.4077 13.01700 442.8898 5.376312 443.3719 0.5125730 443.8541 6.1737001E-02 444.3362 6.956940 444.8183 11.59659 445.3004 12.60199 445.7825 11.59140 446.2646 9.493011 446.7468 6.640930 447.2289 3.336334 447.7110 0.3594360 448.1931 4.558899 448.6752 6.714844 449.1573 4.766296 449.6395 2.930695 450.1216 3.479767 450.6037 4.447479 451.0858 2.109039 451.5679 5.612091 452.0500 14.88724 452.5322 17.78348 453.0143 12.54703 453.4964 6.686615 453.9785 0.2999880 454.4606 6.144501 454.9427 9.203461 455.4249 9.434418 455.9070 8.326508 456.3891 6.282928 456.8712 3.693756 457.3533 1.955719 457.8354 1.254395 458.3176 1.140533 458.7997 2.245361 459.2818 3.689240 459.7639 3.250244 460.2460 2.010315 460.7281 6.666656 461.2103 5.860809 461.6924 0.7883300 462.1745 4.589844 462.6566 9.457062 463.1387 12.22754 463.6208 9.199707 464.1030 1.895660 464.5851 12.44250 465.0672 23.81030 465.5493 32.68631 466.0314 34.39059 466.5135 29.55081 466.9957 24.40729 467.4778 24.75333 467.9599 30.57739 468.4420 33.13824 468.9241 27.20883 469.4063 23.82156 469.8884 24.77969 470.3705 29.81961 470.8526 40.25818 471.3347 56.70941 471.8168 73.22369 472.2990 78.01959 472.7811 67.37875 473.2632 60.98279 473.7453 63.56744 474.2274 69.30289 474.7095 75.84372 475.1917 82.80579 475.6738 89.52591 476.1559 96.58484 476.6380 102.9712 477.1201 105.2216 477.6022 102.2567 478.0844 101.0512 478.5665 106.1617 479.0486 115.5880 479.5307 124.6711 480.0128 133.4904 480.4949 141.4990 480.9771 147.0855 481.4592 151.8737 481.9413 159.8857 482.4234 172.4794 482.9055 185.4768 483.3876 193.2133 483.8698 193.5513 484.3519 197.7360 484.8340 208.2003 485.3161 220.0303 485.7982 231.0143 486.2803 241.1490 486.7625 250.6973 487.2446 259.6397 487.7267 268.7468 488.2088 280.4019 488.6909 293.3538 489.1730 311.4499 489.6552 338.2381 490.1373 367.3560 490.6194 394.7215 491.1015 419.4781 491.5836 441.3430 492.0657 457.3655 492.5479 469.0672 493.0300 488.4498 493.5121 518.9401 493.9942 550.6091 494.4763 574.2145 494.9584 595.4385 495.4406 625.3557 495.9227 671.4943 496.4048 719.4389 496.8869 757.2535 497.3690 787.1581 497.8511 816.1511 498.3333 846.0892 498.8154 877.7841 499.2975 912.7512 499.7796 951.4094 500.2617 991.2421 500.7438 1033.899 501.2260 1076.090 501.7081 1115.021 502.1902 1151.717 502.6723 1188.022 503.1544 1224.756 503.6365 1262.776 504.1187 1304.997 504.6008 1356.925 505.0829 1404.527 505.5650 1447.817 506.0471 1485.523 506.5292 1515.663 507.0114 1539.132 507.4935 1558.823 507.9756 1575.671 508.4577 1590.197 508.9398 1608.171 509.4219 1633.527 509.9041 1656.170 510.3862 1673.028 510.8683 1682.251 511.3504 1679.085 511.8325 1656.294 512.3146 1630.570 512.7968 1617.558 513.2789 1613.917 513.7610 1608.139 514.2431 1597.454 514.7252 1579.660 515.2073 1550.109 515.6895 1505.541 516.1716 1463.966 516.6537 1428.698 517.1358 1393.681 517.6179 1353.246 518.1000 1309.887 518.5822 1271.611 519.0643 1243.243 519.5464 1220.085 520.0285 1188.221 520.5106 1141.032 520.9927 1097.754 521.4749 1063.904 521.9570 1032.385 522.4391 996.8052 522.9212 957.3310 523.4033 918.9094 523.8854 886.8274 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77.04404 551.3661 67.54541 551.8482 67.66925 552.3303 73.81915 552.8124 74.52570 553.2946 68.83453 553.7767 62.33417 554.2588 58.25851 554.7409 54.45016 555.2230 46.56516 555.7051 32.18793 556.1873 21.08551 556.6694 19.99673 557.1515 22.85974 557.6336 21.27075 558.1157 14.59561 558.5978 8.363525 559.0800 7.181549 559.5621 10.49997 560.0442 12.45566 560.5263 11.64984 561.0084 11.12381 561.4905 12.01920 561.9727 12.88199 562.4548 12.65793 562.9369 10.98276 563.4190 7.545715 563.9011 0.1495970 564.3832 11.15164 564.8654 14.16498 565.3475 4.905518 565.8296 2.528015 566.3117 3.508667 566.7938 14.80325 567.2759 18.70166 567.7581 10.91074 568.2402 2.109314 568.7223 3.956024 569.2044 6.438782 569.6865 1.554565 570.1686 11.10703 570.6508 22.33783 571.1329 23.02518 571.6150 13.20224 572.0971 6.780670 572.5792 4.709595 573.0613 4.668579 573.5435 7.876007 574.0256 12.04034 574.5077 14.59616 574.9898 14.90610 575.4719 14.28445 575.9540 14.44870 576.4362 15.33398 576.9183 14.52859 577.4004 11.33072 577.8825 7.702545 578.3646 3.756104 578.8467 0.3138730 579.3289 0.8404240 579.8110 1.972961 580.2932 4.048645 580.7753 1.882355 581.2574 2.864014 581.7395 7.483887 582.2216 11.39963 582.7037 13.97308 583.1859 14.14810 583.6680 11.89359 584.1501 12.51352 584.6322 20.97647 585.1143 26.15207 585.5964 21.39120 586.0786 14.28094 586.5607 14.55136 587.0428 24.16678 587.5249 35.18884 588.0070 36.67429 588.4891 29.85757 588.9713 32.58344 589.4534 49.57129 589.9355 66.27887 590.4176 75.30801 590.8997 78.61865 591.3818 77.97241 591.8640 70.72781 592.3461 66.27386 592.8282 70.02258 593.3103 79.34879 593.7924 92.00626 594.2745 107.0476 594.7567 119.9851 595.2388 126.2990 595.7209 126.6333 596.2030 131.0992 596.6851 145.4200 597.1672 156.8900 597.6494 159.5054 598.1315 161.2783 598.6136 170.7632 599.0957 188.7391 599.5778 208.1217 600.0599 222.2042 600.5421 232.3538 601.0242 244.1472 601.5063 257.7687 601.9884 272.3809 602.4705 287.6806 602.9526 303.7466 603.4348 320.6913 603.9169 339.1206 604.3990 356.7546 604.8811 371.4538 605.3632 386.1050 605.8453 404.2150 606.3275 425.6382 606.8096 447.3116 607.2917 466.9482 607.7738 485.5255 608.2559 506.7154 608.7380 530.9541 609.2202 557.0861 609.7023 581.8575 610.1844 610.7935 610.6665 650.3330 611.1486 698.6335 611.6307 745.4492 612.1129 783.1115 612.5950 816.3350 613.0771 852.1178 613.5592 890.2555 614.0413 930.5795 614.5234 972.5513 615.0056 1017.062 615.4877 1065.615 615.9698 1118.926 616.4519 1174.298 616.9340 1226.577 617.4161 1285.512 617.8983 1363.319 618.3804 1451.323 618.8625 1529.986 619.3446 1589.792 619.8267 1643.105 620.3088 1713.978 620.7910 1804.998 621.2731 1891.014 621.7552 1965.463 622.2373 2039.579 622.7194 2125.758 623.2015 2218.488 623.6837 2301.404 624.1658 2363.326 624.6479 2423.773 625.1300 2494.709 625.6121 2575.807 626.0942 2668.321 626.5764 2772.198 627.0585 2873.564 627.5406 2958.341 628.0227 3025.776 628.5048 3095.517 628.9869 3176.182 629.4691 3250.667 629.9512 3312.617 630.4333 3368.231 630.9154 3426.843 631.3975 3488.810 631.8796 3539.800 632.3618 3563.723 632.8439 3567.771 633.3260 3572.747 633.8081 3579.443 634.2902 3584.322 634.7723 3588.068 635.2545 3587.478 635.7366 3574.802 636.2187 3550.901 636.7008 3515.617 637.1829 3463.841 637.6650 3404.907 638.1472 3345.186 638.6293 3284.537 639.1114 3217.893 639.5935 3141.977 640.0756 3061.772 640.5577 2988.927 641.0399 2924.452 641.5220 2859.908 642.0041 2799.002 642.4862 2731.856 642.9683 2646.900 643.4504 2550.100 643.9326 2461.590 644.4147 2394.963 644.8968 2329.321 645.3789 2244.773 645.8610 2151.454 646.3431 2074.397 646.8253 2019.067 647.3074 1967.345 647.7895 1899.698 648.2716 1815.812 648.7537 1739.624 649.2358 1674.896 649.7180 1613.267 650.2001 1552.307 650.6822 1494.119 651.1643 1440.908 651.6464 1393.358 652.1285 1349.326 652.6107 1312.249 653.0928 1276.708 653.5749 1231.010 654.0570 1174.905 654.5391 1117.034 655.0212 1059.431 655.5034 1006.183 655.9855 966.6365 656.4676 949.7605 656.9497 925.6204 657.4318 886.0026 657.9139 847.0220 658.3961 818.4501 658.8782 797.0930 659.3603 775.9661 659.8424 752.2535 660.3245 726.3096 660.8066 697.4528 661.2888 665.9159 661.7709 636.2908 662.2530 609.5898 662.7351 584.4382 663.2172 558.8792 663.6993 534.0911 664.1815 514.0936 664.6636 503.4205 665.1457 490.1660 665.6278 466.7172 666.1099 442.0162 666.5920 426.0786 667.0742 418.9397 667.5563 414.5223 668.0384 409.1951 668.5205 401.7383 669.0026 387.1677 669.4847 362.8504 669.9669 342.4236 670.4490 329.5848 670.9311 319.9745 671.4132 311.2552 671.8953 302.8274 672.3774 291.8199 672.8596 273.1668 673.3417 255.9481 673.8238 249.2651 674.3059 248.0674 674.7880 241.2589 675.2701 225.9905 675.7523 209.0734 676.2344 197.4705 676.7165 190.6968 677.1986 185.1412 677.6807 182.0814 678.1628 177.8190 678.6450 171.0446 679.1271 163.2530 679.6092 154.7682 680.0913 145.8135 680.5734 140.1459 681.0555 143.6337 681.5377 148.9090 682.0198 145.9022 682.5019 135.8555 682.9840 125.7182 683.4661 118.3144 683.9482 112.8786 684.4304 107.9016 684.9125 102.6201 685.3946 101.3527 685.8767 111.9189 686.3588 117.8586 686.8409 109.7180 687.3231 95.27795 687.8052 85.82812 688.2873 84.64349 688.7694 85.43854 689.2515 83.11368 689.7336 79.33606 690.2158 77.49646 690.6979 77.71088 691.1800 78.16959 691.6621 78.07666 692.1442 77.23444 692.6263 74.99368 693.1085 69.35132 693.5906 66.24673 694.0727 70.29361 694.5548 72.12662 695.0369 64.22528 695.5190 51.15631 696.0012 42.37515 696.4833 42.23807 696.9654 44.05731 697.4475 39.07526 697.9296 29.97229 698.4117 26.82050 698.8939 31.21759 699.3760 37.45752 699.8581 42.96008 700.3402 46.54041 700.8223 43.68893 701.3044 23.24710 701.7866 12.01819 702.2687 17.95450 702.7508 26.63934 703.2329 28.43558 703.7150 24.77536 704.1971 21.96170 704.6793 23.28879 705.1614 26.10379 705.6435 27.04718 706.1256 26.33807 706.6077 25.64697 707.0898 25.62073 707.5720 22.99551 708.0541 13.56409 708.5362 0.7848210 709.0183 7.438660 709.5004 8.8287003E-02 709.9825 5.978912 710.4647 8.144485 710.9468 8.664642 711.4289 9.453110 711.9110 10.13924 712.3931 8.629913 712.8752 2.915909 713.3574 3.868713 713.8395 6.808594 714.3216 6.322784 714.8037 5.093079 715.2858 3.454041 715.7679 2.028351 716.2501 1.215973 716.7322 1.050613 717.2143 1.974640 717.6964 5.403214 718.1785 7.922287 718.6606 8.098770 719.1428 7.947952 719.6249 9.532608 720.1070 12.46643 720.5891 14.69244 721.0712 15.19363 721.5533 13.97910 722.0355 9.751770 722.5176 3.227448 722.9997 6.9091998E-02 723.4818 1.502518 723.9639 4.207199 724.4460 4.840454 724.9282 3.535172 725.4103 2.057678 725.8924 1.956619 726.3745 2.957291 726.8566 2.869232 727.3387 9.547012 727.8209 12.56822 728.3030 11.83028 728.7851 9.369812 729.2672 5.747360 729.7493 1.892578 730.2314 0.6790620 730.7136 2.266769 731.1957 5.131805 731.6778 10.13370 732.1599 12.76508 732.6420 8.059113 733.1241 2.946106 733.6063 9.280106 734.0884 8.435959 734.5705 6.087250 735.0526 1.051025 735.5347 3.995819 736.0168 7.421555 736.4990 9.093369 736.9811 9.259308 737.4632 7.270706 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33.57097 764.9438 34.64796 765.4260 36.84363 765.9081 39.44904 766.3902 42.09882 766.8723 44.23653 767.3544 44.08731 767.8365 40.81232 768.3187 38.72079 768.8008 40.17276 769.2829 43.73749 769.7650 47.02209 770.2471 50.81947 770.7292 51.78020 771.2114 45.87259 771.6935 41.33032 772.1756 41.95006 772.6577 46.00745 773.1398 52.00583 773.6219 59.33931 774.1041 64.92560 774.5862 65.55394 775.0683 63.39102 775.5504 61.37109 776.0325 59.69243 776.5146 58.12888 776.9968 56.40625 777.4789 56.94954 777.9611 64.05238 778.4432 78.26434 778.9253 83.80296 779.4074 74.98958 779.8895 67.36432 780.3716 65.85246 780.8538 66.17201 781.3359 64.39362 781.8180 60.58636 782.3001 57.96147 782.7822 58.09029 783.2643 59.43495 783.7465 61.36372 784.2286 63.65656 784.7107 66.65167 785.1928 69.92477 785.6749 71.28130 786.1570 68.42619 786.6392 63.50114 787.1213 63.30078 787.6034 68.46521 788.0855 72.06929 788.5676 72.15245 789.0497 71.71022 789.5319 73.63234 790.0140 77.09955 790.4961 77.82480 790.9782 72.80962 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