#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-06-07 11:18:42 +0300 (Thu, 07 Jun 2018) $ #$Revision: 1076 $ #$URL: svn://172.16.1.111/rod/cif/2/10/00/2100048.rod $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100048 loop_ _publ_author_name 'Howard, C. J.' 'Hill, R. J.' 'Reichert, B. E.' _publ_section_title ; Structures of the ZrO2 polymorphs at room temperature by high-resolution neutron powder diffraction ; _journal_issue 2 _journal_name_full 'Acta Crystallographica, Section B' _journal_page_first 116 _journal_page_last 120 _journal_paper_doi 10.1107/S0108768187010279 _journal_volume 44 _journal_year 1988 _chemical_compound_source 'Synthetic 2' _chemical_formula_sum 'O2 Zr' _chemical_name_mineral Baddeleyite _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 99.230 _cell_angle_gamma 90 _cell_length_a 5.1505 _cell_length_b 5.2116 _cell_length_c 5.3173 _cell_volume 140.881 _exptl_crystal_density_diffrn 5.810 _cod_original_formula_sum 'Zr O2' _cod_database_code 9016714 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060078.rod _rod_data_source.block 3500000 _rod_database.code 2100048 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9016714 COD http://www.crystallography.net/cod/9016714.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 94.71033 0.0000000E+00 95.19244 2.051746 95.67456 4.355915 96.15668 4.634624 96.63879 0.9131320 97.12091 1.011261 97.60303 1.133553 98.08514 7.1686000E-02 98.56726 1.694542 99.04938 3.684273 99.53149 7.066162 100.0136 11.90668 100.4957 18.10101 100.9778 26.95105 101.4600 38.31409 101.9421 52.38107 102.4242 70.08183 102.9063 93.04756 103.3884 115.6141 103.8705 135.6422 104.3527 155.9930 104.8348 165.1136 105.3169 160.0048 105.7990 142.2895 106.2811 122.8421 106.7632 99.92581 107.2454 77.21254 107.7275 57.67633 108.2096 41.28316 108.6917 27.86147 109.1738 17.55594 109.6559 10.43239 110.1381 5.201233 110.6202 2.833450 111.1023 1.949860 111.5844 1.196671 112.0665 0.1187130 112.5486 0.6614070 113.0308 7.1560000E-03 113.5129 2.144333 113.9950 4.498306 114.4771 7.234879 114.9592 9.987793 115.4413 12.29453 115.9235 13.66110 116.4056 14.81453 116.8877 16.05182 117.3698 17.56616 117.8519 18.94751 118.3340 20.03473 118.8162 20.88429 119.2983 21.62122 119.7804 22.21323 120.2625 22.79175 120.7446 23.45245 121.2267 24.31839 121.7089 25.15758 122.1910 25.55165 122.6731 25.67075 123.1552 26.30978 123.6373 28.63159 124.1194 31.52979 124.6016 33.66690 125.0837 33.72510 125.5658 33.42831 126.0479 34.61713 126.5300 37.24844 127.0121 40.32742 127.4943 42.89600 127.9764 45.24971 128.4585 48.19395 128.9406 52.66325 129.4227 57.74988 129.9048 61.63622 130.3869 64.23105 130.8691 66.35390 131.3512 68.77014 131.8333 70.40189 132.3154 70.57455 132.7975 70.64474 133.2796 70.99536 133.7618 71.27798 134.2439 71.46466 134.7260 71.71323 135.2081 72.37921 135.6902 73.49850 136.1723 74.43832 136.6545 74.66638 137.1366 74.18552 137.6187 74.25964 138.1008 74.97827 138.5829 76.24789 139.0650 78.17450 139.5472 81.06329 140.0293 83.50485 140.5114 84.48074 140.9935 83.61713 141.4756 83.05899 141.9577 83.05029 142.4399 83.47897 142.9220 83.77347 143.4041 83.74466 143.8862 83.88629 144.3683 84.57336 144.8504 85.89682 145.3326 87.49539 145.8147 89.06696 146.2968 90.69089 146.7789 93.68362 147.2610 99.34949 147.7431 105.2563 148.2253 109.3586 148.7074 110.0297 149.1895 111.1523 149.6716 113.2777 150.1537 116.4349 150.6358 120.1774 151.1180 124.3565 151.6001 129.1545 152.0822 134.6915 152.5643 140.2261 153.0464 146.4387 153.5285 153.0770 154.0107 159.7077 154.4928 168.0676 154.9749 177.1279 155.4570 188.3531 155.9391 203.4998 156.4212 221.6347 156.9034 244.7383 157.3855 273.2416 157.8676 306.3210 158.3497 346.1624 158.8318 395.0111 159.3139 450.8350 159.7961 510.4776 160.2782 582.1403 160.7603 650.7670 161.2424 709.4855 161.7245 756.6591 162.2066 795.6102 162.6888 823.0810 163.1709 842.9732 163.6530 863.8784 164.1351 887.5660 164.6172 914.2467 165.0993 943.9050 165.5815 976.0944 166.0636 1012.063 166.5457 1052.860 167.0278 1098.144 167.5099 1146.949 167.9920 1197.119 168.4742 1251.282 168.9563 1311.355 169.4384 1375.715 169.9205 1449.258 170.4026 1533.423 170.8847 1628.976 171.3669 1738.218 171.8490 1859.281 172.3311 1995.724 172.8132 2151.565 173.2953 2327.144 173.7774 2524.232 174.2596 2741.273 174.7417 2979.883 175.2238 3247.935 175.7059 3556.003 176.1880 3894.326 176.6701 4249.499 177.1523 4669.094 177.6344 5067.316 178.1165 5382.216 178.5986 5612.713 179.0807 5669.672 179.5628 5419.123 180.0450 4936.606 180.5271 4400.631 181.0092 3807.896 181.4913 3222.586 181.9734 2757.327 182.4555 2412.822 182.9377 2159.476 183.4198 1982.850 183.9019 1875.274 184.3840 1812.719 184.8661 1789.236 185.3482 1802.862 185.8304 1848.220 186.3125 1924.883 186.7946 2035.740 187.2767 2184.341 187.7588 2370.984 188.2409 2589.189 188.7231 2854.507 189.2052 3152.435 189.6873 3456.262 190.1694 3782.485 190.6515 4050.423 191.1336 4184.448 191.6158 4183.533 192.0979 4024.725 192.5800 3630.774 193.0621 3041.518 193.5442 2499.068 194.0263 1993.202 194.5085 1546.186 194.9906 1199.006 195.4727 950.7700 195.9548 757.4881 196.4369 611.8947 196.9190 512.0934 197.4012 431.6239 197.8833 372.4825 198.3654 328.2607 198.8475 292.2619 199.3296 264.5775 199.8117 241.6862 200.2939 222.4649 200.7760 206.9926 201.2581 194.4819 201.7402 185.2304 202.2223 178.6572 202.7044 173.8734 203.1866 170.9451 203.6687 169.3969 204.1508 169.6670 204.6329 172.0745 205.1150 173.0937 205.5971 172.2715 206.0793 170.5254 206.5614 169.6176 207.0435 169.6850 207.5256 170.0647 208.0077 170.4368 208.4898 170.7464 208.9720 171.4863 209.4541 172.4961 209.9362 174.0812 210.4183 176.9019 210.9004 181.0143 211.3825 185.8256 211.8647 191.2946 212.3468 197.6343 212.8289 203.8916 213.3110 209.7433 213.7931 215.6227 214.2752 222.2720 214.7574 229.3841 215.2395 238.2562 215.7216 249.2750 216.2037 261.8676 216.6858 278.3337 217.1679 298.7834 217.6500 323.1628 218.1322 351.0374 218.6143 382.9700 219.0964 417.8573 219.5785 455.2532 220.0606 497.3283 220.5427 537.6192 221.0249 579.9420 221.5070 618.3924 221.9891 638.7654 222.4712 642.0941 222.9533 625.7667 223.4354 586.2407 223.9176 513.8505 224.3997 443.8519 224.8818 373.5557 225.3639 306.5442 225.8460 249.2192 226.3281 202.8044 226.8103 164.6619 227.2924 135.2553 227.7745 116.6207 228.2566 99.95523 228.7387 85.22562 229.2208 72.43369 229.7030 62.08087 230.1851 54.70862 230.6672 48.73181 231.1493 43.62390 231.6314 39.67639 232.1135 35.80640 232.5957 31.93750 233.0778 28.17105 233.5599 24.78925 234.0420 21.77243 234.5241 19.17398 235.0062 17.14136 235.4884 16.05029 235.9705 14.42477 236.4526 11.86697 236.9347 8.929993 237.4168 6.766296 237.8989 5.678925 238.3811 4.870911 238.8632 4.084167 239.3453 3.339233 239.8274 2.512329 240.3095 1.441467 240.7916 0.3678590 241.2738 0.2041320 241.7559 5.1757999E-02 242.2380 0.2800290 242.7201 0.1531370 243.2022 0.4631350 243.6843 0.9501950 244.1665 1.194366 244.6486 1.369507 245.1307 1.777435 245.6128 2.466827 246.0949 3.313538 246.5770 4.394104 247.0592 5.931915 247.5413 6.772064 248.0234 6.554840 248.5055 5.888458 248.9876 5.747162 249.4697 6.410797 249.9519 7.086761 250.4340 7.520111 250.9161 7.638824 251.3982 7.870544 251.8803 8.137756 252.3624 8.579468 252.8446 9.586823 253.3267 11.99374 253.8088 13.28589 254.2909 12.40866 254.7730 8.942352 255.2551 6.564697 255.7373 5.599335 256.2194 5.387024 256.7015 5.175568 257.1836 4.886078 257.6657 4.774384 258.1478 4.927155 258.6299 5.364746 259.1121 5.916199 259.5942 6.761078 260.0763 7.525391 260.5584 7.716095 261.0405 7.018311 261.5226 6.578979 262.0048 6.736206 262.4869 7.477051 262.9690 7.979431 263.4511 8.180511 263.9332 8.225067 264.4153 8.196594 264.8975 7.985718 265.3796 8.001587 265.8617 8.372192 266.3438 9.054474 266.8259 9.690216 267.3080 10.44733 267.7902 10.83771 268.2723 10.27911 268.7544 8.394836 269.2365 6.970825 269.7186 6.484955 270.2007 6.682220 270.6829 6.144897 271.1650 4.674835 271.6471 2.954071 272.1292 1.553619 272.6113 0.5436710 273.0934 0.5367130 273.5756 1.734619 274.0577 3.012421 274.5398 4.250031 275.0219 5.358673 275.5040 6.642212 275.9861 8.374176 276.4683 10.61600 276.9504 12.69623 277.4325 14.46088 277.9146 16.10739 278.3967 17.96103 278.8788 19.89505 279.3610 22.63251 279.8431 27.02328 280.3252 33.11560 280.8073 38.27026 281.2894 42.07785 281.7715 45.31897 282.2537 49.37103 282.7358 54.25662 283.2179 59.80219 283.7000 66.06216 284.1821 73.04550 284.6642 79.97595 285.1464 86.66003 285.6285 93.82098 286.1106 102.6049 286.5927 113.0076 287.0748 124.2911 287.5569 136.3345 288.0391 149.1034 288.5212 161.9899 289.0033 175.0779 289.4854 188.1846 289.9675 201.0035 290.4496 213.6261 290.9318 226.3475 291.4139 239.3498 291.8960 252.6895 292.3781 266.3574 292.8602 280.5236 293.3423 294.5977 293.8245 307.5005 294.3066 319.7099 294.7887 333.5952 295.2708 350.2214 295.7529 368.6224 296.2350 386.6451 296.7172 404.2137 297.1993 422.2364 297.6814 441.2115 298.1635 461.3951 298.6456 483.0258 299.1277 505.9621 299.6099 531.2127 300.0920 560.1295 300.5741 592.7221 301.0562 626.2647 301.5383 659.4139 302.0204 692.6265 302.5026 726.3177 302.9847 761.2708 303.4668 795.9727 303.9489 831.3688 304.4310 865.7637 304.9131 895.5865 305.3953 919.7050 305.8774 937.3625 306.3595 947.5454 306.8416 950.4754 307.3237 944.2938 307.8058 926.0610 308.2880 897.3784 308.7701 862.0021 309.2522 817.8650 309.7343 769.7333 310.2164 720.5288 310.6985 669.5729 311.1807 621.9544 311.6628 580.6079 312.1449 544.7808 312.6270 514.5081 313.1091 488.9597 313.5912 468.9347 314.0734 455.3397 314.5555 448.2651 315.0376 445.1165 315.5197 445.2393 316.0018 448.3036 316.4839 453.9242 316.9661 464.4539 317.4482 475.1997 317.9303 483.4353 318.4124 489.6963 318.8945 497.6797 319.3766 508.6452 319.8588 521.8235 320.3409 536.4973 320.8230 552.5039 321.3051 570.1920 321.7872 589.9337 322.2693 611.4787 322.7515 634.0690 323.2336 655.7184 323.7157 679.6761 324.1978 707.7809 324.6799 741.2220 325.1620 776.2639 325.6442 810.4579 326.1263 846.2545 326.6084 887.9754 327.0905 934.6797 327.5726 988.4899 328.0547 1050.555 328.5369 1121.195 329.0190 1197.834 329.5011 1284.796 329.9832 1375.254 330.4653 1461.490 330.9474 1547.949 331.4296 1624.941 331.9117 1694.774 332.3938 1758.025 332.8759 1794.823 333.3580 1805.435 333.8401 1789.853 334.3223 1746.409 334.8044 1664.403 335.2865 1574.365 335.7686 1475.237 336.2507 1369.983 336.7328 1279.802 337.2150 1204.001 337.6971 1142.990 338.1792 1096.645 338.6613 1066.110 339.1434 1047.279 339.6255 1040.297 340.1077 1044.622 340.5898 1059.600 341.0719 1085.389 341.5540 1119.879 342.0361 1162.245 342.5182 1212.709 343.0003 1269.974 343.4825 1334.618 343.9646 1403.637 344.4467 1474.790 344.9288 1547.313 345.4109 1613.627 345.8930 1673.329 346.3752 1724.448 346.8573 1758.390 347.3394 1776.052 347.8215 1771.533 348.3036 1737.741 348.7857 1676.286 349.2679 1593.486 349.7500 1486.204 350.2321 1363.520 350.7142 1239.159 351.1963 1114.358 351.6784 995.4185 352.1606 886.3187 352.6427 788.0662 353.1248 700.8633 353.6069 624.2587 354.0890 557.7012 354.5711 501.4540 355.0533 454.9047 355.5354 415.1878 356.0175 382.7751 356.4996 355.8713 356.9817 332.0596 357.4638 311.1088 357.9460 294.5288 358.4281 284.4916 358.9102 279.1646 359.3923 276.0862 359.8744 273.5505 360.3565 273.4536 360.8387 277.3911 361.3208 285.2243 361.8029 294.7849 362.2850 304.5803 362.7671 315.8126 363.2492 329.5110 363.7314 345.9780 364.2135 365.0365 364.6956 386.7366 365.1777 410.8965 365.6598 436.8727 366.1419 465.5735 366.6241 495.4899 367.1062 525.4234 367.5883 554.6014 368.0704 585.2253 368.5525 617.3738 369.0346 651.1311 369.5168 687.0401 369.9989 726.4429 370.4810 766.6251 370.9631 806.9313 371.4452 847.0920 371.9273 889.6393 372.4095 933.1310 372.8916 979.4785 373.3737 1030.920 373.8558 1088.918 374.3379 1149.545 374.8200 1212.111 375.3022 1277.245 375.7843 1347.110 376.2664 1423.651 376.7485 1502.469 377.2306 1581.845 377.7127 1662.946 378.1949 1740.957 378.6770 1816.074 379.1591 1886.620 379.6412 1947.964 380.1233 2000.600 380.6054 2044.969 381.0876 2082.551 381.5697 2112.546 382.0518 2131.009 382.5339 2138.261 383.0160 2131.395 383.4981 2108.110 383.9803 2068.021 384.4624 2009.894 384.9445 1931.337 385.4266 1836.746 385.9087 1728.638 386.3908 1608.271 386.8730 1484.974 387.3551 1359.203 387.8372 1235.288 388.3193 1119.493 388.8014 1012.744 389.2835 914.7759 389.7657 826.6173 390.2478 746.7305 390.7299 673.6497 391.2120 606.8486 391.6941 546.1136 392.1762 492.2960 392.6584 446.0008 393.1405 404.7410 393.6226 368.8891 394.1047 336.7250 394.5868 306.9062 395.0689 278.7242 395.5511 253.0369 396.0332 230.3605 396.5153 210.5308 396.9974 192.6772 397.4795 177.1055 397.9616 163.0529 398.4438 150.1848 398.9259 138.9209 399.4080 128.0217 399.8901 117.3291 400.3722 106.9098 400.8543 96.99670 401.3365 86.93481 401.8186 78.06284 402.3007 70.81772 402.7828 65.31012 403.2649 60.56396 403.7470 57.21762 404.2292 53.92242 404.7113 49.27466 405.1934 42.39627 405.6755 36.65314 406.1576 32.76224 406.6397 30.29291 407.1219 27.94604 407.6040 25.81097 408.0861 23.42877 408.5682 20.17664 409.0503 16.13663 409.5324 13.26352 410.0146 11.90289 410.4967 10.95184 410.9788 8.629761 411.4609 5.116852 411.9430 1.910858 412.4251 0.4689030 412.9073 2.105927 413.3894 3.001343 413.8715 3.179718 414.3536 3.589539 414.8357 5.227814 415.3178 7.622009 415.8000 9.886017 416.2821 11.89139 416.7642 13.62448 417.2463 14.97925 417.7284 16.05426 418.2105 17.06442 418.6927 18.40891 419.1748 19.55179 419.6569 19.97565 420.1390 19.55573 420.6211 19.14847 421.1032 19.23840 421.5854 19.51498 422.0675 19.64200 422.5496 19.16693 423.0317 18.90323 423.5138 19.52808 423.9959 20.77750 424.4781 21.02261 424.9602 19.06268 425.4423 16.76315 425.9244 15.00632 426.4065 14.15582 426.8886 13.23526 427.3708 12.18176 427.8529 11.08417 428.3350 10.13696 428.8171 9.717377 429.2992 8.728149 429.7813 6.606201 430.2635 3.418915 430.7456 1.374573 431.2277 1.031494 431.7098 0.6381230 432.1919 1.480621 432.6740 5.502014 433.1562 9.028748 433.6383 11.68228 434.1204 13.82693 434.6025 16.04126 435.0846 18.33063 435.5667 20.94196 436.0489 24.11465 436.5310 27.74222 437.0131 31.46631 437.4952 35.29388 437.9773 39.27084 438.4594 43.46548 438.9416 47.84552 439.4236 52.31702 439.9058 56.72198 440.3879 61.38660 440.8700 66.57944 441.3521 72.32663 441.8342 78.71011 442.3163 86.14966 442.7985 94.00922 443.2806 101.7594 443.7627 109.1378 444.2448 116.9616 444.7269 124.9565 445.2090 133.6993 445.6912 143.8415 446.1733 156.8209 446.6554 169.9254 447.1375 181.7275 447.6196 192.5056 448.1017 205.1783 448.5839 219.8560 449.0660 236.4729 449.5481 254.8914 450.0302 275.7438 450.5123 297.2951 450.9944 318.5602 451.4766 340.9799 451.9587 366.9082 452.4408 397.2791 452.9229 428.9594 453.4050 460.9739 453.8871 493.5670 454.3693 530.9592 454.8514 573.3561 455.3335 620.3535 455.8156 672.0134 456.2977 728.2816 456.7798 790.2798 457.2620 858.9875 457.7441 932.7145 458.2262 1010.787 458.7083 1092.478 459.1904 1178.202 459.6725 1268.682 460.1547 1362.190 460.6368 1455.946 461.1189 1550.704 461.6010 1646.914 462.0831 1744.540 462.5652 1844.415 463.0474 1945.126 463.5295 2044.356 464.0116 2150.620 464.4937 2268.064 464.9758 2395.722 465.4579 2528.232 465.9401 2658.229 466.4222 2798.054 466.9043 2952.414 467.3864 3122.511 467.8685 3300.767 468.3506 3485.605 468.8328 3679.029 469.3149 3882.399 469.7970 4098.677 470.2791 4320.069 470.7612 4550.847 471.2433 4783.886 471.7255 5001.631 472.2076 5207.397 472.6897 5389.998 473.1718 5553.647 473.6539 5697.484 474.1360 5794.229 474.6182 5846.058 475.1003 5843.281 475.5824 5776.193 476.0645 5644.823 476.5466 5452.508 477.0287 5192.691 477.5109 4883.427 477.9930 4537.142 478.4751 4160.872 478.9572 3788.104 479.4393 3426.431 479.9214 3082.902 480.4036 2770.460 480.8857 2488.145 481.3678 2233.729 481.8499 2007.916 482.3320 1807.508 482.8141 1631.921 483.2963 1483.675 483.7784 1353.363 484.2605 1241.151 484.7426 1144.904 485.2247 1060.370 485.7068 991.8727 486.1890 931.1841 486.6711 875.8022 487.1532 825.7775 487.6353 781.0576 488.1174 743.0898 488.5995 710.2006 489.0817 681.4106 489.5638 657.6309 490.0459 636.4438 490.5280 617.4265 491.0101 600.9568 491.4922 587.5948 491.9744 577.1234 492.4565 570.5566 492.9386 569.0820 493.4207 572.0427 493.9028 574.5612 494.3849 576.4191 494.8671 580.2177 495.3492 588.9240 495.8313 601.5939 496.3134 615.9005 496.7955 631.8391 497.2776 648.0792 497.7598 662.8481 498.2419 676.6660 498.7240 690.3828 499.2061 707.2612 499.6882 722.2949 500.1703 733.1573 500.6525 739.6207 501.1346 738.9261 501.6167 729.5637 502.0988 712.8502 502.5809 689.8307 503.0630 660.5576 503.5452 624.6017 504.0273 578.5487 504.5094 526.4371 504.9915 476.2182 505.4736 427.2246 505.9557 381.1426 506.4379 338.3916 506.9200 299.0274 507.4021 264.6189 507.8842 235.6836 508.3663 209.5701 508.8484 183.7642 509.3306 158.2059 509.8127 136.2662 510.2948 118.6691 510.7769 103.4258 511.2590 87.68707 511.7411 71.80115 512.2233 58.20285 512.7054 48.30225 513.1875 40.78220 513.6696 33.59216 514.1517 26.78873 514.6339 20.81873 515.1160 16.02585 515.5981 12.23373 516.0802 9.188354 516.5623 6.815216 517.0444 4.997833 517.5266 3.659180 518.0087 2.774811 518.4908 2.367065 518.9729 1.943970 519.4550 2.721527 519.9371 5.617493 520.4193 10.05710 520.9014 13.45993 521.3835 14.33487 521.8656 15.72058 522.3477 18.94824 522.8298 24.34595 523.3120 29.99548 523.7941 36.01382 524.2762 42.00598 524.7583 47.13464 525.2404 51.35013 525.7225 56.92664 526.2047 64.47784 526.6868 73.08853 527.1689 80.69769 527.6510 87.62943 528.1331 96.08368 528.6152 108.4361 529.0974 122.3615 529.5795 134.3605 530.0616 144.6707 530.5437 155.6172 531.0258 168.7558 531.5079 183.3525 531.9901 199.1098 532.4722 216.2087 532.9543 233.8946 533.4364 253.2075 533.9185 272.6311 534.4006 290.4807 534.8828 305.5846 535.3649 319.8729 535.8470 334.1608 536.3291 348.1370 536.8112 359.0245 537.2933 367.5092 537.7755 371.8238 538.2576 370.8667 538.7397 364.3102 539.2218 354.5393 539.7039 341.2504 540.1860 325.9369 540.6682 309.6921 541.1503 292.7537 541.6324 276.8322 542.1145 262.1689 542.5966 249.1444 543.0787 238.1306 543.5609 229.2155 544.0430 222.7194 544.5251 218.8322 545.0072 217.4153 545.4893 218.7006 545.9714 222.6007 546.4536 228.0571 546.9357 234.1878 547.4178 241.8438 547.8999 251.7812 548.3820 264.6722 548.8641 278.5479 549.3463 292.5792 549.8284 307.5347 550.3105 324.4848 550.7926 344.7876 551.2747 364.9245 551.7568 384.4073 552.2390 403.5285 552.7211 424.2271 553.2032 447.2545 553.6853 469.5824 554.1674 490.5278 554.6495 509.9326 555.1317 525.3882 555.6138 536.7145 556.0959 543.7104 556.5780 546.4681 557.0601 544.6643 557.5422 537.2977 558.0244 523.9846 558.5065 505.5141 558.9886 481.8754 559.4707 453.7486 559.9528 423.0973 560.4349 388.2476 560.9171 353.0208 561.3992 318.9680 561.8813 286.0266 562.3634 254.6504 562.8455 224.0385 563.3276 195.4493 563.8098 169.1524 564.2919 145.2509 564.7740 123.8089 565.2561 104.9243 565.7382 88.40573 566.2203 74.06531 566.7025 62.13885 567.1846 51.14178 567.6667 40.77823 568.1488 31.07056 568.6309 22.05768 569.1130 13.69415 569.5952 6.656342 570.0773 1.392212 570.5594 2.480133 571.0415 5.649811 571.5236 8.183167 572.0057 10.57440 572.4879 13.60196 572.9700 16.45737 573.4521 18.29834 573.9342 18.96539 574.4163 18.97870 574.8984 17.94223 575.3806 16.66931 575.8627 15.97885 576.3448 16.98813 576.8269 17.45593 577.3090 17.58261 577.7911 16.96298 578.2733 14.33453 578.7554 8.372131 579.2375 3.175720 579.7196 0.3356630 580.2017 0.5217290 580.6838 2.773712 581.1660 6.601471 581.6481 10.65753 582.1302 13.71332 582.6123 16.11945 583.0944 19.52606 583.5765 24.19193 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637.5735 601.4151 638.0557 581.1735 638.5378 559.3261 639.0199 535.7863 639.5020 510.5192 639.9841 482.7668 640.4662 452.9286 640.9484 423.4543 641.4305 394.9961 641.9126 367.5381 642.3947 340.3104 642.8768 313.8881 643.3589 289.1405 643.8411 266.5905 644.3232 245.8376 644.8053 226.4354 645.2874 208.6201 645.7695 191.7585 646.2516 175.7732 646.7338 160.8339 647.2159 147.2538 647.6980 134.9166 648.1801 123.6147 648.6622 113.1963 649.1443 103.8593 649.6265 95.80505 650.1086 89.03534 650.5907 82.47455 651.0728 75.98621 651.5549 69.87280 652.0370 64.58069 652.5192 59.88290 653.0013 55.33130 653.4834 50.73135 653.9655 46.42261 654.4476 42.87439 654.9297 39.86646 655.4119 36.97424 655.8940 33.77170 656.3761 30.97073 656.8582 29.13528 657.3403 27.96683 657.8224 26.36215 658.3046 24.02881 658.7867 21.60239 659.2688 19.12247 659.7509 16.63898 660.2330 14.80127 660.7151 13.68591 661.1973 12.77023 661.6794 11.85535 662.1615 10.87976 662.6436 9.416870 663.1257 7.443176 663.6078 5.813477 664.0900 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