#\#CIF_2.0 #------------------------------------------------------------------------------ #$Date: 2018-05-24 15:40:51 +0300 (Thu, 24 May 2018) $ #$Revision: 770 $ #$URL: svn://172.16.1.111/rod/cif/2/20/00/2200001.rod $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200001 loop_ _publ_author_name 'Uchida, Hinako' 'Downs, Robert T.' 'Thompson, Richard M.' _publ_section_title ; Reinvestigation of eakerite, Ca~2~SnAl~2~Si~6~O~18~(OH)~2~·2H~2~O: H-atom positions by single-crystal X-ray diffraction and correlation with Raman spectroscopic data ; _journal_coeditor_code HB2229 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first 47 _journal_page_last 49 _journal_paper_doi 10.1107/S1600536807002000 _journal_volume 63 _journal_year 2007 _chemical_compound_source R060319 _chemical_formula_iupac 'Ca2 Sn Al2 Si6 O18 (O H)2, 2H2 O' _chemical_formula_moiety 'Al2 H2 O20 Si6 Sn, 2(H2 O), 2(Ca)' _chemical_formula_sum 'Al2 Ca2 H6 O22 Si6 Sn' _chemical_formula_weight 779.40 _chemical_name_common eakerite _chemical_name_systematic ; dicalcium tin dialuminosilicate dihydroxide dihydrate ; _space_group_IT_number 14 _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.00 _cell_angle_beta 101.293(2) _cell_angle_gamma 90.00 _cell_formula_units_Z 2 _cell_length_a 15.8202(5) _cell_length_b 7.6963(3) _cell_length_c 7.4449(3) _cell_volume 888.92(6) _cod_data_source_file hb2229.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/a' _cod_database_code 2212176 _raman_determination_method experimental _raman_measurement_device.location 'Arizona University' _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model 'Nicolet Almega XR' _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.5 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 15 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 400 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _rod_data_source.file R060319.rod _rod_data_source.block 3500000 _rod_database.code 2200001 loop_ _raman_complementary.id _raman_complementary.method 1 XRD loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 2212176 COD http://www.crystallography.net/cod/2212176.html ; XRD analysis data was done. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 158.4706 0.0000000E+00 158.9528 2.564392 159.4349 2.806885 159.9170 0.2797850 160.3991 1.554260 160.8812 0.5257570 161.3633 3.019409 161.8455 8.216431 162.3276 14.45898 162.8097 21.14807 163.2918 29.97205 163.7739 41.99915 164.2560 55.09314 164.7382 60.74182 165.2203 63.67053 165.7024 67.67310 166.1845 73.59778 166.6666 81.78662 167.1487 91.07092 167.6309 101.4622 168.1130 112.6394 168.5951 123.6599 169.0772 135.2161 169.5593 146.0067 170.0414 155.3317 170.5236 163.9467 171.0057 169.2484 171.4878 168.5425 171.9699 162.9379 172.4520 155.7131 172.9341 147.8267 173.4163 139.6669 173.8984 131.3434 174.3805 121.7366 174.8626 113.7476 175.3447 110.5793 175.8268 111.5632 176.3090 113.7588 176.7911 115.5342 177.2732 117.0859 177.7553 118.8400 178.2374 121.5465 178.7195 123.7766 179.2017 122.6719 179.6838 118.6432 180.1659 115.5441 180.6480 116.7506 181.1301 121.1129 181.6122 126.1453 182.0944 131.6204 182.5765 137.0046 183.0586 141.4955 183.5407 144.9868 184.0228 148.1722 184.5049 151.1324 184.9871 154.1277 185.4692 157.9895 185.9513 163.8214 186.4334 170.4010 186.9155 174.3036 187.3976 175.2186 187.8798 176.5879 188.3619 183.2139 188.8440 194.2268 189.3261 203.4240 189.8082 208.4784 190.2903 210.2031 190.7725 211.3842 191.2546 212.0067 191.7367 212.3905 192.2188 213.0375 192.7009 213.9382 193.1830 214.5452 193.6652 215.2115 194.1473 215.6250 194.6294 213.7352 195.1115 209.5898 195.5936 203.0610 196.0757 193.1394 196.5579 179.7133 197.0400 166.3326 197.5221 154.1915 198.0042 143.3025 198.4863 133.1793 198.9684 123.6703 199.4506 115.3976 199.9327 109.4695 200.4148 105.9435 200.8969 103.7831 201.3790 103.1670 201.8611 104.1816 202.3433 103.5864 202.8254 100.7001 203.3075 97.23145 203.7896 96.40186 204.2717 98.68835 204.7538 101.0426 205.2360 102.1907 205.7181 102.0217 206.2002 101.4657 206.6823 100.3877 207.1644 99.07153 207.6465 98.00903 208.1287 97.19653 208.6108 96.67175 209.0929 96.56470 209.5750 97.01843 210.0571 97.20093 210.5392 96.94604 211.0214 96.63989 211.5035 97.14917 211.9856 98.70593 212.4677 100.4670 212.9498 102.0063 213.4319 103.1335 213.9140 104.7599 214.3962 106.9269 214.8783 109.5786 215.3604 112.4629 215.8425 115.4365 216.3246 118.0103 216.8067 121.7850 217.2889 127.5217 217.7710 131.5151 218.2531 133.2654 218.7352 133.4613 219.2173 133.7290 219.6994 134.0800 220.1816 134.4219 220.6637 134.7396 221.1458 135.0304 221.6279 135.2870 222.1100 135.2994 222.5921 135.3914 223.0743 136.5214 223.5564 139.0385 224.0385 142.0300 224.5206 144.9353 225.0027 147.5162 225.4848 150.8123 225.9670 154.4784 226.4491 158.9520 226.9312 165.6672 227.4133 175.3799 227.8954 186.0378 228.3775 196.3071 228.8597 205.5879 229.3418 216.4097 229.8239 229.2882 230.3060 243.5618 230.7881 257.1632 231.2702 270.6719 231.7524 282.8058 232.2345 293.1765 232.7166 303.2487 233.1987 308.3628 233.6808 307.2832 234.1629 301.5822 234.6451 295.3328 235.1272 289.0211 235.6093 281.8241 236.0914 273.0542 236.5735 261.4789 237.0556 250.7761 237.5378 240.6339 238.0199 231.5868 238.5020 225.0487 238.9841 221.9619 239.4662 220.4778 239.9483 219.7184 240.4305 219.7355 240.9126 219.5979 241.3947 219.0715 241.8768 218.3309 242.3589 218.1991 242.8410 220.1959 243.3232 220.9624 243.8053 218.9816 244.2874 213.6342 244.7695 206.7355 245.2516 198.0569 245.7337 187.8375 246.2159 176.4290 246.6980 162.8313 247.1801 149.2610 247.6622 136.4847 248.1443 124.4376 248.6264 113.8110 249.1086 105.2656 249.5907 97.79456 250.0728 89.07324 250.5549 77.74866 251.0370 67.10535 251.5191 58.48560 252.0013 52.29919 252.4834 47.10730 252.9655 43.37280 253.4476 40.34937 253.9297 36.41211 254.4118 30.30298 254.8940 25.64612 255.3761 24.03711 255.8582 26.36108 256.3403 28.22058 256.8224 29.52063 257.3046 30.44946 257.7867 31.23206 258.2688 31.83948 258.7509 32.45410 259.2330 33.13367 259.7151 33.91028 260.1973 34.84485 260.6794 36.18103 261.1615 37.44690 261.6436 37.78979 262.1257 36.84680 262.6078 35.86951 263.0900 35.02148 263.5721 34.18335 264.0542 34.54578 264.5363 36.24231 265.0184 38.94604 265.5005 42.51184 265.9827 47.21375 266.4648 51.79858 266.9469 55.75696 267.4290 59.03552 267.9111 62.86462 268.3932 67.44446 268.8754 72.19604 269.3575 76.07520 269.8396 78.46411 270.3217 82.46411 270.8038 88.96387 271.2859 97.94714 271.7681 107.9377 272.2502 119.4119 272.7323 130.9282 273.2144 140.5837 273.6965 148.1387 274.1786 155.6394 274.6608 164.4805 275.1429 173.8962 275.6250 178.8401 276.1071 179.3290 276.5892 175.3755 277.0714 165.7983 277.5535 149.9012 278.0356 134.4724 278.5177 120.3724 278.9998 107.7910 279.4819 97.92334 279.9641 91.09021 280.4462 85.32031 280.9283 78.33972 281.4104 70.07227 281.8925 65.01782 282.3746 64.49927 282.8568 67.14941 283.3389 69.31335 283.8210 70.94897 284.3031 72.34924 284.7852 74.25488 285.2673 76.49695 285.7495 76.68445 286.2316 74.44299 286.7137 70.05090 287.1958 63.16699 287.6779 53.66699 288.1600 44.85803 288.6422 39.62207 289.1243 37.27991 289.6064 33.15662 290.0885 26.47803 290.5706 18.79309 291.0527 12.38000 291.5349 7.217407 292.0170 2.804321 292.4991 1.426270 292.9812 5.147217 293.4633 6.754028 293.9454 5.869507 294.4276 4.095459 294.9097 2.918091 295.3918 2.450195 295.8739 3.401611 296.3560 7.777954 296.8381 13.67493 297.3203 16.37451 297.8024 15.63879 298.2845 13.20483 298.7666 9.594604 299.2487 5.549194 299.7308 3.211548 300.2130 4.480347 300.6951 7.626221 301.1772 10.04773 301.6593 11.73401 302.1414 12.82715 302.6235 13.63843 303.1057 13.90649 303.5878 13.04858 304.0699 9.861206 304.5520 6.211182 305.0341 4.322021 305.5162 4.056641 305.9984 4.227173 306.4805 4.845825 306.9626 5.170776 307.4447 4.027222 307.9268 0.1740720 308.4089 3.993774 308.8911 6.052246 309.3732 6.470215 309.8553 7.223267 310.3374 10.22766 310.8195 13.78015 311.3016 16.01001 311.7838 15.96887 312.2659 15.74902 312.7480 16.93909 313.2301 19.06958 313.7122 20.90601 314.1943 20.81555 314.6765 20.98291 315.1586 23.30762 315.6407 28.72900 316.1228 33.88599 316.6049 36.54968 317.0870 37.99988 317.5692 40.32288 318.0513 44.71130 318.5334 49.50073 319.0155 53.65442 319.4976 57.02576 319.9797 60.78088 320.4619 66.74573 320.9440 72.76233 321.4261 76.39661 321.9082 74.00696 322.3903 72.24829 322.8724 73.79492 323.3546 78.77844 323.8367 82.70996 324.3188 83.41919 324.8009 83.54675 325.2830 85.09680 325.7651 87.88428 326.2473 92.65430 326.7294 100.7079 327.2115 111.5349 327.6936 121.0184 328.1757 125.8585 328.6578 131.4771 329.1400 140.6147 329.6221 156.0090 330.1042 171.0477 330.5863 185.5560 331.0684 199.7236 331.5505 213.7498 332.0327 226.8960 332.5148 240.8418 332.9969 256.4397 333.4790 273.8551 333.9611 291.6748 334.4432 310.9967 334.9254 330.1298 335.4075 346.3491 335.8896 360.8365 336.3717 370.3234 336.8538 373.5149 337.3359 370.2189 337.8180 362.6069 338.3001 349.4161 338.7823 333.9222 339.2644 319.6245 339.7465 306.2948 340.2286 294.8192 340.7107 285.6705 341.1928 278.5809 341.6750 271.9294 342.1571 264.9456 342.6392 260.8027 343.1213 263.3529 343.6034 272.6602 344.0855 280.8483 344.5677 285.8162 345.0498 289.6439 345.5319 297.0636 346.0140 308.1082 346.4961 321.7506 346.9782 339.2501 347.4604 359.4902 347.9425 376.4574 348.4246 390.0103 348.9067 399.5791 349.3888 405.4595 349.8709 407.2246 350.3531 402.2970 350.8352 388.2274 351.3173 366.9407 351.7994 340.3627 352.2815 308.3474 352.7636 275.3405 353.2458 244.2162 353.7279 215.2053 354.2100 188.7800 354.6921 165.0919 355.1742 144.2192 355.6563 126.2319 356.1385 111.2400 356.6206 98.68518 357.1027 88.52319 357.5848 80.37073 358.0669 73.72253 358.5490 69.28174 359.0312 64.94604 359.5133 58.54773 359.9954 51.02405 360.4775 45.13586 360.9596 43.38391 361.4417 43.04785 361.9239 42.33826 362.4060 40.74500 362.8881 39.39001 363.3702 38.66357 363.8523 38.34302 364.3344 38.09900 364.8166 39.16260 365.2987 39.23596 365.7808 36.98987 366.2629 31.94177 366.7450 27.86230 367.2271 26.53137 367.7093 25.85107 368.1914 23.97937 368.6735 19.78845 369.1556 15.47717 369.6377 11.07629 370.1198 6.663330 370.6020 3.205811 371.0841 1.104126 371.5662 0.4169920 372.0483 1.741333 372.5304 2.864014 373.0125 3.798706 373.4947 4.355713 373.9768 4.796021 374.4589 5.955200 374.9410 8.658203 375.4231 10.38037 375.9052 9.871094 376.3874 6.753174 376.8695 4.344116 377.3516 2.824707 377.8337 1.646484 378.3158 7.5805999E-02 378.7979 2.496094 379.2801 4.325562 379.7622 4.799194 380.2443 4.456787 380.7264 6.047852 381.2085 9.767212 381.6906 13.93079 382.1728 17.00793 382.6549 19.21338 383.1370 21.68372 383.6191 24.55774 384.1012 27.91663 384.5833 32.12354 385.0655 37.11230 385.5476 42.31848 386.0297 47.64050 386.5118 52.98218 386.9939 58.00549 387.4760 62.50354 387.9582 67.76013 388.4403 75.02856 388.9224 84.03955 389.4045 94.12817 389.8866 106.2576 390.3687 118.6016 390.8509 129.6874 391.3330 139.4608 391.8151 148.0839 392.2972 156.8607 392.7793 163.8481 393.2614 167.3524 393.7436 168.0403 394.2257 163.5369 394.7078 149.9231 395.1899 130.0531 395.6720 111.4199 396.1541 95.00146 396.6363 81.48950 397.1184 71.67639 397.6005 66.71106 398.0826 62.08936 398.5647 55.86450 399.0468 50.06946 399.5290 47.16907 400.0111 49.86536 400.4932 52.75842 400.9753 54.85437 401.4574 56.16492 401.9395 58.10327 402.4217 61.33154 402.9038 64.48340 403.3859 66.47998 403.8680 66.40332 404.3501 67.34668 404.8322 69.63171 405.3144 72.98950 405.7965 76.61621 406.2786 80.45459 406.7607 84.80884 407.2428 89.71680 407.7249 95.19067 408.2071 101.6357 408.6892 109.0858 409.1713 117.4833 409.6534 126.7550 410.1355 136.8763 410.6176 147.9823 411.0998 160.0031 411.5819 173.1927 412.0640 188.8041 412.5461 206.6223 413.0282 224.6536 413.5103 240.5815 413.9925 255.4689 414.4746 271.9652 414.9567 290.9843 415.4388 310.3730 415.9209 330.1716 416.4030 348.8811 416.8852 363.3363 417.3673 370.4084 417.8494 373.3390 418.3315 375.8070 418.8136 378.0399 419.2957 374.9293 419.7779 362.2865 420.2600 343.4216 420.7421 321.8674 421.2242 295.7866 421.7063 269.9926 422.1884 244.4224 422.6706 219.8960 423.1527 198.4792 423.6348 181.8463 424.1169 167.7856 424.5990 155.2139 425.0811 144.1658 425.5633 134.6248 426.0454 125.8315 426.5275 118.8402 427.0096 115.0907 427.4917 116.6541 427.9738 118.3807 428.4560 119.1716 428.9381 119.0773 429.4202 119.2148 429.9023 119.5920 430.3844 120.3977 430.8665 121.3473 431.3487 122.0153 431.8308 124.7946 432.3129 130.2373 432.7950 137.2920 433.2771 143.8167 433.7592 149.8597 434.2414 156.1517 434.7235 162.4557 435.2056 169.0997 435.6877 177.1519 436.1698 186.6678 436.6519 197.1125 437.1341 207.7129 437.6162 218.5851 438.0983 230.5614 438.5804 244.5530 439.0625 258.8492 439.5446 271.6453 440.0268 283.1212 440.5089 293.9128 440.9910 305.0991 441.4731 315.1820 441.9552 323.7200 442.4373 331.3256 442.9195 334.4050 443.4016 330.0560 443.8837 320.5045 444.3658 308.4539 444.8479 294.4927 445.3300 278.3624 445.8122 259.4946 446.2943 238.1786 446.7764 215.5742 447.2585 188.0435 447.7406 162.1884 448.2227 141.4169 448.7049 128.5609 449.1870 115.6628 449.6691 102.4865 450.1512 89.43750 450.6333 77.24548 451.1154 65.27014 451.5976 55.33423 452.0797 48.28101 452.5618 43.91846 453.0439 40.15076 453.5260 37.10852 454.0081 34.44702 454.4903 32.07019 454.9724 29.98914 455.4545 27.46863 455.9366 24.24670 456.4187 20.96851 456.9008 18.71411 457.3830 17.42310 457.8651 16.80994 458.3472 17.01038 458.8293 17.69360 459.3114 18.10754 459.7935 18.25488 460.2757 18.91602 460.7578 21.32288 461.2399 24.44019 461.7220 26.74927 462.2041 27.42993 462.6862 27.96533 463.1684 29.19128 463.6505 30.99585 464.1326 33.10791 464.6147 35.11670 465.0968 37.64417 465.5789 41.26709 466.0611 46.23279 466.5432 50.51904 467.0253 53.67773 467.5074 55.95618 467.9895 57.52307 468.4716 55.37646 468.9538 56.48047 469.4359 62.66907 469.9180 72.34204 470.4001 80.48071 470.8822 86.48474 471.3643 91.97034 471.8465 97.53223 472.3286 103.2007 472.8107 108.9553 473.2928 114.8127 473.7749 120.6383 474.2570 126.3933 474.7392 132.0846 475.2213 136.8864 475.7034 140.6333 476.1855 143.3776 476.6676 146.0441 477.1497 148.3369 477.6319 147.5360 478.1140 141.0602 478.5961 130.7197 479.0782 118.9915 479.5603 105.9274 480.0424 92.85254 480.5246 80.02197 481.0067 68.05420 481.4888 57.82397 481.9709 50.32153 482.4530 43.65735 482.9352 36.91919 483.4173 30.23938 483.8994 24.04150 484.3815 17.95789 484.8636 12.78918 485.3457 9.181641 485.8279 7.658203 486.3100 5.733276 486.7921 2.546875 487.2742 0.7604980 487.7563 3.304932 488.2384 5.556152 488.7206 6.025024 489.2027 3.351807 489.6848 1.048096 490.1669 1.462646 490.6490 3.602905 491.1311 8.060669 491.6133 8.108154 492.0954 3.846069 492.5775 2.894775 493.0596 5.843262 493.5417 9.591431 494.0238 10.76038 494.5060 9.769043 494.9881 8.440552 495.4702 7.072632 495.9523 5.839966 496.4344 5.066895 496.9165 4.687622 497.3987 4.458984 497.8808 5.063232 498.3629 5.270996 498.8450 3.551147 499.3271 0.2969970 499.8092 4.022339 500.2914 6.809937 500.7735 8.707275 501.2556 9.820068 501.7377 9.257324 502.2198 8.965820 502.7019 9.434326 503.1841 10.47498 503.6662 11.58972 504.1483 12.73511 504.6304 13.99902 505.1125 15.61658 505.5946 17.70581 506.0768 18.70898 506.5589 18.10852 507.0410 17.21912 507.5231 16.92664 508.0052 17.16089 508.4873 18.77625 508.9695 22.36926 509.4516 26.58032 509.9337 28.49585 510.4158 28.24585 510.8979 28.28137 511.3800 29.77295 511.8622 32.23926 512.3443 34.69958 512.8264 37.12939 513.3085 39.59583 513.7906 42.87964 514.2728 45.94385 514.7549 47.16101 515.2370 45.63965 515.7191 44.05371 516.2012 43.75171 516.6833 44.55066 517.1655 46.15820 517.6476 50.00269 518.1297 53.15503 518.6118 54.12207 519.0939 53.13025 519.5760 52.85413 520.0582 54.17261 520.5403 55.80432 521.0224 57.27563 521.5045 58.72986 521.9866 59.46973 522.4688 58.80151 522.9509 58.15613 523.4330 59.80847 523.9151 64.45374 524.3972 67.28174 524.8793 66.46228 525.3615 63.82495 525.8436 64.65332 526.3257 68.89929 526.8078 72.96021 527.2899 74.36499 527.7720 74.17346 528.2542 74.69458 528.7363 76.04443 529.2184 77.80908 529.7005 79.25562 530.1826 81.01782 530.6647 84.15979 531.1469 90.10034 531.6290 95.55188 532.1111 97.68604 532.5932 98.03882 533.0753 99.74255 533.5574 105.2469 534.0396 110.7620 534.5217 114.2040 535.0038 115.2307 535.4859 119.3789 535.9680 128.5007 536.4501 138.9666 536.9323 148.7732 537.4144 157.9164 537.8965 166.4292 538.3786 173.6249 538.8607 181.1130 539.3428 191.6093 539.8250 205.4569 540.3071 218.9464 540.7892 230.5066 541.2713 241.3445 541.7534 254.4590 542.2355 269.6273 542.7177 284.3252 543.1998 296.1659 543.6819 307.0061 544.1640 320.2964 544.6461 336.4468 545.1282 351.4340 545.6104 362.6078 546.0925 370.7667 546.5746 376.8602 547.0567 381.0183 547.5388 383.7596 548.0209 385.4377 548.5031 385.2671 548.9852 382.1113 549.4673 373.1078 549.9494 364.6726 550.4315 357.9814 550.9136 352.8047 551.3958 348.5966 551.8779 346.1052 552.3600 343.8657 552.8421 340.4135 553.3242 335.3872 553.8063 332.6770 554.2885 332.6676 554.7706 334.5807 555.2527 337.4999 555.7348 341.5210 556.2169 346.5885 556.6990 352.6813 557.1812 360.0964 557.6633 369.1511 558.1454 379.5984 558.6275 390.7002 559.1096 402.0497 559.5917 413.6331 560.0739 424.7195 560.5560 435.4761 561.0381 448.2134 561.5202 464.2352 562.0023 482.3020 562.4844 501.4391 562.9666 521.9827 563.4487 542.9961 563.9308 564.8621 564.4129 586.7927 564.8950 607.5631 565.3771 627.1412 565.8593 645.8540 566.3414 664.0034 566.8235 681.3589 567.3056 698.7698 567.7877 716.7632 568.2698 729.2014 568.7520 732.1150 569.2341 726.7200 569.7162 717.5801 570.1983 705.1785 570.6804 686.6782 571.1625 657.6248 571.6447 621.3848 572.1268 583.0149 572.6089 542.1665 573.0910 501.8198 573.5731 463.4651 574.0552 427.0260 574.5374 391.3695 575.0195 354.3047 575.5016 320.2727 575.9837 291.2413 576.4658 267.1509 576.9479 244.5010 577.4301 223.3400 577.9122 203.7216 578.3943 185.2909 578.8764 167.8730 579.3585 153.3168 579.8406 141.9452 580.3228 132.6954 580.8049 124.9783 581.2870 118.7239 581.7691 112.0693 582.2512 104.3961 582.7333 96.97583 583.2155 92.40735 583.6975 89.83142 584.1796 86.35327 584.6617 78.49561 585.1439 70.71179 585.6260 67.71680 586.1081 68.68921 586.5902 69.48145 587.0723 68.83740 587.5544 66.92896 588.0366 63.71423 588.5187 59.03723 589.0008 53.81775 589.4829 46.38403 589.9650 39.68604 590.4471 36.19568 590.9293 37.80090 591.4114 38.14587 591.8935 36.20190 592.3756 33.52234 592.8577 33.24768 593.3398 35.55457 593.8220 37.38733 594.3041 37.74976 594.7862 37.00977 595.2683 36.10242 595.7504 34.95569 596.2325 32.98071 596.7147 29.11047 597.1968 24.60181 597.6789 20.48584 598.1610 16.83435 598.6431 14.55664 599.1252 15.91663 599.6074 17.89417 600.0895 17.86133 600.5716 13.55420 601.0537 10.38171 601.5358 9.988037 602.0179 10.85083 602.5001 11.10461 602.9822 10.73633 603.4643 9.653198 603.9464 7.312378 604.4285 4.421997 604.9106 3.510742 605.3928 4.770264 605.8749 6.149902 606.3570 6.715088 606.8391 6.594727 607.3212 6.119141 607.8033 5.297241 608.2855 4.465698 608.7676 3.892944 609.2497 3.470459 609.7318 3.192749 610.2139 3.158325 610.6960 2.718140 611.1782 0.2995610 611.6603 2.168457 612.1424 2.653564 612.6245 2.479248 613.1066 5.803833 613.5887 5.363892 614.0709 2.723389 614.5530 0.9504390 615.0351 0.6116940 615.5172 6.6895001E-02 615.9993 2.068970 616.4814 4.790771 616.9636 4.388672 617.4457 0.5435790 617.9278 2.872803 618.4099 2.936401 618.8920 0.7257080 619.3741 0.9396970 619.8563 1.969238 620.3384 2.673584 620.8205 3.809082 621.3026 4.574219 621.7847 3.591553 622.2668 0.5295410 622.7490 3.356812 623.2311 1.809692 623.7132 1.733887 624.1953 4.237305 624.6774 5.439697 625.1595 5.159668 625.6417 2.201416 626.1238 2.055054 626.6059 3.409912 627.0880 0.8653560 627.5701 1.485718 628.0522 2.044800 628.5344 1.216553 629.0165 1.374146 629.4986 2.551392 629.9807 3.011841 630.4628 0.5328370 630.9449 3.228882 631.4271 4.999146 631.9092 4.464722 632.3913 3.558960 632.8734 3.544434 633.3555 3.925293 633.8376 4.133667 634.3198 3.687622 634.8019 3.733887 635.2840 4.957642 635.7661 6.691528 636.2482 7.977173 636.7303 8.001221 637.2125 8.987671 637.6946 11.99658 638.1767 15.84985 638.6588 17.03662 639.1409 15.25867 639.6230 13.03015 640.1052 11.00110 640.5873 9.400635 641.0694 9.375244 641.5515 10.78638 642.0336 11.83301 642.5157 10.83398 642.9979 9.081543 643.4800 7.854248 643.9621 7.253418 644.4442 7.599121 644.9263 10.60803 645.4084 13.68042 645.8906 14.47913 646.3727 10.11121 646.8548 8.132080 647.3369 10.12854 647.8190 13.74133 648.3011 16.24744 648.7833 17.45325 649.2654 18.11084 649.7475 18.01831 650.2296 17.57153 650.7117 17.73352 651.1938 18.54285 651.6760 19.48669 652.1581 20.54065 652.6402 21.48071 653.1223 22.30078 653.6044 22.83057 654.0865 22.32263 654.5687 19.23303 655.0508 15.90381 655.5329 13.86292 656.0150 13.27844 656.4971 12.96704 656.9792 12.64612 657.4614 12.55005 657.9435 12.78809 658.4256 13.28931 658.9077 14.50818 659.3898 16.99548 659.8719 19.19482 660.3541 19.08972 660.8362 16.76477 661.3183 15.17822 661.8004 14.89600 662.2825 15.10852 662.7646 14.52759 663.2468 13.56152 663.7289 13.34229 664.2110 15.33838 664.6931 16.91370 665.1752 15.23535 665.6573 11.85706 666.1395 10.15320 666.6216 12.90637 667.1037 16.21973 667.5858 19.44934 668.0679 22.42505 668.5500 23.61011 669.0322 22.03821 669.5143 20.46484 669.9964 20.55371 670.4785 22.29919 670.9606 22.15186 671.4427 19.86755 671.9249 17.91931 672.4070 18.58508 672.8891 20.94727 673.3712 23.32947 673.8533 25.53943 674.3354 26.72766 674.8176 26.04016 675.2997 24.65869 675.7818 23.45142 676.2639 22.76611 676.7460 21.89673 677.2281 19.91064 677.7103 17.97607 678.1924 17.78442 678.6745 21.10388 679.1566 22.09888 679.6387 19.29858 680.1208 14.79272 680.6030 12.69202 681.0851 12.99976 681.5672 12.79419 682.0493 10.65918 682.5314 7.842163 683.0135 6.634155 683.4957 6.839722 683.9778 7.134521 684.4599 6.638550 684.9420 5.796021 685.4241 4.579956 685.9063 3.151978 686.3884 2.223145 686.8705 2.034790 687.3526 2.211304 687.8347 2.789673 688.3168 4.093140 688.7990 5.014038 689.2811 5.457275 689.7632 5.589966 690.2453 5.573853 690.7274 5.394043 691.2095 4.569580 691.6917 2.928589 692.1738 1.686768 692.6559 2.652222 693.1380 4.774048 693.6201 6.237427 694.1022 6.432983 694.5844 6.398926 695.0665 6.658081 695.5486 7.032715 696.0307 7.300415 696.5128 7.063599 696.9949 7.179077 697.4771 8.135864 697.9592 9.314087 698.4413 9.329590 698.9234 7.844482 699.4055 6.632568 699.8876 6.305176 700.3698 6.424805 700.8519 5.802002 701.3340 4.551392 701.8161 3.419189 702.2982 2.846313 702.7803 2.582764 703.2625 2.383301 703.7446 2.266235 704.2267 2.332397 704.7088 3.300903 705.1909 3.764648 705.6730 2.686890 706.1552 0.1662600 706.6373 1.881592 707.1194 2.546387 707.6015 1.935913 708.0836 0.6040040 708.5657 5.222168 709.0479 8.106445 709.5300 9.199951 710.0121 9.111206 710.4942 7.341309 710.9763 4.855347 711.4584 4.662720 711.9406 7.580322 712.4227 9.770020 712.9048 7.388184 713.3869 3.341431 713.8690 0.6868900 714.3511 7.6416001E-02 714.8333 0.4329830 715.3154 4.230469 715.7975 8.419434 716.2796 9.755615 716.7617 7.218262 717.2438 4.973999 717.7260 3.591309 718.2081 2.706787 718.6902 1.631592 719.1723 0.4356690 719.6544 0.3057860 720.1365 0.3122560 720.6187 3.6377002E-02 721.1008 0.6231690 721.5829 1.192383 722.0650 1.165894 722.5471 2.069214 723.0292 3.624023 723.5114 0.2098390 723.9935 7.870972 724.4756 12.50476 724.9577 11.93176 725.4398 11.29407 725.9219 12.20764 726.4041 14.29456 726.8862 15.19775 727.3683 14.82422 727.8504 14.56042 728.3325 15.01416 728.8146 16.19495 729.2968 18.70251 729.7789 22.31824 730.2610 25.02637 730.7431 24.60376 731.2252 23.51782 731.7073 23.29663 732.1895 24.05811 732.6716 26.05408 733.1537 31.17065 733.6358 35.79565 734.1179 37.73889 734.6000 36.13745 735.0822 36.94775 735.5643 40.63110 736.0464 45.07642 736.5285 48.95520 737.0106 52.07056 737.4927 53.26624 737.9749 52.25952 738.4570 51.16992 738.9391 51.28491 739.4212 52.66858 739.9033 55.93689 740.3854 63.08508 740.8676 67.53491 741.3497 64.95483 741.8318 60.18127 742.3139 58.35181 742.7960 61.33679 743.2781 62.28760 743.7603 59.78650 744.2424 56.71606 744.7245 57.71753 745.2066 62.27515 745.6887 66.60889 746.1708 70.31140 746.6530 72.17017 747.1351 69.38708 747.6172 64.04248 748.0993 59.81592 748.5814 58.61292 749.0635 58.09912 749.5457 58.06470 750.0278 58.08252 750.5099 57.36035 750.9920 56.31873 751.4741 53.65930 751.9562 48.61023 752.4384 42.27539 752.9205 37.93188 753.4026 35.49768 753.8847 32.09375 754.3668 25.59729 754.8489 18.74109 755.3311 15.95093 755.8132 16.15125 756.2953 16.27600 756.7774 14.76770 757.2595 12.94482 757.7416 11.37842 758.2238 10.04614 758.7059 8.550903 759.1880 6.734009 759.6701 4.988403 760.1522 3.351929 760.6343 1.876831 761.1165 0.5360110 761.5986 0.7048340 762.0807 0.9395750 762.5628 1.418335 763.0449 4.614258 763.5270 5.266724 764.0092 3.779785 764.4913 2.312012 764.9734 2.827637 765.4555 3.279419 765.9376 2.087891 766.4197 0.9088130 766.9019 2.819336 767.3840 3.364502 767.8661 2.965210 768.3482 1.401733 768.8303 1.269897 769.3124 2.599731 769.7946 2.568726 770.2767 1.768555 770.7588 0.4846190 771.2409 2.828125 771.7230 2.430054 772.2051 0.6810300 772.6873 4.019653 773.1694 7.286133 773.6515 9.315796 774.1336 8.466553 774.6157 3.641479 775.0978 2.337891 775.5800 7.118530 776.0621 12.22534 776.5442 14.01331 777.0263 12.28247 777.5084 11.49890 777.9905 11.66760 778.4727 12.84778 778.9548 15.74231 779.4369 19.45117 779.9190 22.83777 780.4011 25.68286 780.8832 26.62439 781.3654 23.00439 781.8475 18.80396 782.3296 17.18347 782.8117 19.41577 783.2938 21.73315 783.7759 24.11963 784.2581 26.66626 784.7402 29.47876 785.2223 32.56250 785.7044 35.82080 786.1865 39.31702 786.6686 42.09326 787.1508 41.75574 787.6329 40.60303 788.1150 42.91602 788.5971 50.04041 789.0792 55.87341 789.5613 55.91370 790.0435 54.50317 790.5256 55.28809 791.0077 59.58020 791.4898 62.99146 791.9719 65.35669 792.4540 67.05151 792.9362 68.48071 793.4183 69.60791 793.9004 69.66089 794.3825 68.52185 794.8646 66.94971 795.3467 65.38367 795.8289 63.95740 796.3110 63.06409 796.7931 63.05676 797.2752 62.32227 797.7573 58.40601 798.2394 54.82959 798.7216 54.72095 799.2037 60.40100 799.6858 63.39294 800.1679 63.28369 800.6500 61.40149 801.1321 58.52185 801.6143 54.87524 802.0964 51.49133 802.5785 48.45435 803.0606 45.95325 803.5427 44.56677 804.0248 43.63220 804.5070 42.47046 804.9891 41.06860 805.4712 39.10474 805.9533 35.74463 806.4354 32.36450 806.9175 30.18872 807.3997 29.88770 807.8818 27.54932 808.3639 22.44080 808.8460 17.88123 809.3281 18.99768 809.8102 23.20544 810.2924 22.98462 810.7745 16.78455 811.2566 11.44177 811.7387 12.76001 812.2208 16.55920 812.7029 19.31604 813.1851 20.60779 813.6672 20.30713 814.1493 17.29468 814.6314 14.06763 815.1135 12.98230 815.5956 14.15491 816.0778 13.55212 816.5599 10.79907 817.0420 7.986328 817.5241 7.290161 818.0062 7.795288 818.4883 8.068359 818.9705 7.880737 819.4526 7.827026 819.9347 8.626831 820.4168 9.467651 820.8989 9.558594 821.3810 8.587891 821.8632 8.099731 822.3453 8.189209 822.8274 8.617432 823.3095 9.896118 823.7916 11.67371 824.2737 10.65674 824.7559 6.507080 825.2380 2.203979 825.7201 8.4960997E-02 826.2022 0.3319090 826.6843 0.8598630 827.1664 3.762451 827.6486 5.523071 828.1307 3.911133 828.6128 2.312256 829.0949 2.395752 829.5770 4.525269 830.0591 6.365845 830.5413 7.796265 831.0234 8.536621 831.5055 8.217896 831.9876 7.244751 832.4697 6.233765 832.9518 5.203857 833.4340 4.354736 833.9161 3.628906 834.3982 3.294800 834.8803 3.893555 835.3624 5.542480 835.8445 5.716064 836.3267 3.598145 836.8088 1.624512 837.2909 1.141235 837.7730 1.856079 838.2551 1.859619 838.7372 1.227539 839.2194 0.9075930 839.7015 1.919678 840.1836 3.274048 840.6657 4.141724 841.1478 4.514038 841.6299 4.457520 842.1121 3.463501 842.5942 2.621826 843.0763 2.356934 843.5584 2.505493 844.0405 2.310791 844.5226 1.597290 845.0048 1.739868 845.4869 4.059326 845.9690 6.973755 846.4511 6.908447 846.9332 4.677246 847.4153 2.977661 847.8975 2.812256 848.3796 3.793335 848.8617 6.784546 849.3438 10.85205 849.8259 12.93311 850.3080 12.40845 850.7902 11.11401 851.2723 9.054077 851.7544 6.964355 852.2365 6.837036 852.7186 8.352051 853.2007 9.604370 853.6829 10.17395 854.1650 9.799072 854.6471 7.131348 855.1292 3.620239 855.6113 1.696289 856.0934 3.699463 856.5756 5.123901 857.0577 5.080811 857.5398 4.506958 858.0219 4.984497 858.5040 6.610474 858.9861 7.116577 859.4683 5.884155 859.9504 4.285889 860.4325 4.087158 860.9146 4.686646 861.3967 5.150513 861.8788 5.359619 862.3610 5.092163 862.8431 3.331909 863.3252 1.667114 863.8073 1.738281 864.2894 4.592896 864.7715 5.872559 865.2537 5.260864 865.7358 3.943237 866.2179 2.790039 866.7000 1.908081 867.1821 1.733398 867.6642 2.353882 868.1464 2.817505 868.6285 2.172607 869.1106 1.377808 869.5927 1.231201 870.0748 1.999634 870.5569 2.417603 871.0391 2.312500 871.5212 2.125977 872.0033 1.925415 872.4854 1.785278 872.9675 2.827271 873.4496 4.921753 873.9318 6.185425 874.4139 4.056763 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