#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 10:43:43 +0300 (Thu, 07 Jun 2018) $
#$Revision: 961 $
#$URL: svn://172.16.1.111/rod/cif/2/31/00/2310011.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2310011
loop_
_publ_author_name
'Giglio, M.'
_publ_section_title
;
 Die kristallstruktur von Na2Zn(SO4)2*4H2O (Zn-blodit) Locality: synthetic
;
_journal_name_full               'Acta Crystallographica'
_journal_page_first              789
_journal_page_last               794
_journal_paper_doi               10.1107/S0365110X5800222X
_journal_volume                  11
_journal_year                    1958
_chemical_compound_source        R110213
_chemical_formula_sum            'H8 Na2 O12 S2 Zn'
_chemical_name_mineral           Changoite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.58
_cell_angle_gamma                90
_cell_length_a                   11.05
_cell_length_b                   8.23
_cell_length_c                   5.54
_cell_volume                     495.251
_exptl_crystal_density_diffrn    2.518
_cod_original_formula_sum        'Zn Na2 S2 O12 H8'
_cod_database_code               9011018
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 15
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110213.rod
_rod_data_source.block           3500000
_rod_database.code               2310011
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011018 COD http://www.crystallography.net/cod/9011018.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
198.4863 0.0000000E+00
198.9684 0.4553220
199.4506 0.4628910
199.9327 3.715820
200.4148 8.401123
200.8969 14.05054
201.3790 20.67261
201.8611 27.11353
202.3433 33.23413
202.8254 39.15723
203.3075 42.16675
203.7896 41.18652
204.2717 37.73242
204.7538 35.33789
205.2360 33.83301
205.7181 33.57837
206.2002 35.17480
206.6823 38.93994
207.1644 41.77026
207.6465 43.00488
208.1287 43.24121
208.6108 44.75708
209.0929 48.11157
209.5750 51.07739
210.0571 52.22900
210.5392 51.40308
211.0214 49.64551
211.5035 46.76904
211.9856 43.17871
212.4677 39.74756
212.9498 35.67017
213.4319 33.76489
213.9140 36.67480
214.3962 46.48633
214.8783 53.88452
215.3604 57.54980
215.8425 58.33032
216.3246 59.18164
216.8067 60.07715
217.2889 61.07983
217.7710 62.28711
218.2531 63.81128
218.7352 64.93481
219.2173 65.11035
219.6994 64.76758
220.1816 65.97632
220.6637 69.05591
221.1458 73.01343
221.6279 77.43408
222.1100 83.19702
222.5921 87.21216
223.0743 89.43994
223.5564 89.79834
224.0385 87.20850
224.5206 78.82788
225.0027 72.13721
225.4848 72.98901
225.9670 87.00708
226.4491 94.89990
226.9312 93.30640
227.4133 84.39526
227.8954 78.50293
228.3775 77.03296
228.8597 76.67651
229.3418 75.55664
229.8239 73.61621
230.3060 70.80078
230.7881 66.02515
231.2702 60.14722
231.7524 57.75806
232.2345 60.37793
232.7166 64.09644
233.1987 66.71362
233.6808 68.18750
234.1629 68.30811
234.6451 66.30005
235.1272 62.83716
235.6093 60.96069
236.0914 61.28369
236.5735 62.31274
237.0556 63.54077
237.5378 66.19092
238.0199 66.43481
238.5020 63.27612
238.9841 57.65649
239.4662 53.12476
239.9483 49.50391
240.4305 47.44482
240.9126 47.79883
241.3947 53.07153
241.8768 55.30664
242.3589 52.84033
242.8410 47.23877
243.3232 44.59619
243.8053 42.46948
244.2874 43.24243
244.7695 48.63867
245.2516 63.81567
245.7337 71.70630
246.2159 68.99707
246.6980 59.21069
247.1801 53.83740
247.6622 54.42725
248.1443 56.85742
248.6264 59.39136
249.1086 62.52466
249.5907 64.55884
250.0728 65.26953
250.5549 64.96411
251.0370 64.20020
251.5191 62.02197
252.0013 61.05640
252.4834 62.78003
252.9655 68.51904
253.4476 73.67871
253.9297 78.62402
254.4118 82.89062
254.8940 85.37109
255.3761 85.28589
255.8582 84.89844
256.3403 84.36597
256.8224 84.01733
257.3046 84.56348
257.7867 86.09155
258.2688 88.10938
258.7509 88.78076
259.2330 87.04150
259.7151 85.89014
260.1973 86.55859
260.6794 89.33667
261.1615 92.70288
261.6436 97.92529
262.1257 102.6416
262.6078 102.0369
263.0900 93.56494
263.5721 86.31274
264.0542 83.97119
264.5363 87.89771
265.0184 87.90869
265.5005 82.27759
265.9827 75.08740
266.4648 72.50928
266.9469 76.41553
267.4290 79.15869
267.9111 78.22241
268.3932 73.40161
268.8754 67.80542
269.3575 60.42578
269.8396 53.81567
270.3217 51.93164
270.8038 55.99072
271.2859 60.12744
271.7681 61.70532
272.2502 60.70947
272.7323 61.57593
273.2144 65.06055
273.6965 69.30664
274.1786 72.92651
274.6608 76.41309
275.1429 76.88281
275.6250 72.79688
276.1071 65.00879
276.5892 58.70264
277.0714 53.70801
277.5535 50.47852
278.0356 50.66895
278.5177 54.81689
278.9998 56.23560
279.4819 52.27954
279.9641 44.77173
280.4462 42.86987
280.9283 47.94067
281.4104 52.67725
281.8925 50.25757
282.3746 40.59180
282.8568 32.09961
283.3389 26.38696
283.8210 22.69214
284.3031 18.77417
284.7852 14.62451
285.2673 11.17285
285.7495 10.31885
286.2316 11.72485
286.7137 9.004150
287.1958 0.5947270
287.6779 11.70044
288.1600 11.24268
288.6422 0.9582520
289.1243 12.55786
289.6064 14.57300
290.0885 8.713379
290.5706 3.167725
291.0527 1.892822
291.5349 5.311523
292.0170 3.983398
292.4991 1.572266
292.9812 6.503906
293.4633 6.869629
293.9454 4.350586
294.4276 4.662598
294.9097 8.492188
295.3918 13.42578
295.8739 16.95068
296.3560 19.08936
296.8381 20.10840
297.3203 20.21973
297.8024 19.28320
298.2845 16.23340
298.7666 10.79492
299.2487 5.936035
299.7308 5.038574
300.2130 7.182617
300.6951 9.700195
301.1772 11.61182
301.6593 13.21484
302.1414 15.14795
302.6235 17.35107
303.1057 19.11182
303.5878 19.26123
304.0699 18.57812
304.5520 18.57227
305.0341 20.78906
305.5162 22.93799
305.9984 22.37695
306.4805 19.38037
306.9626 15.83887
307.4447 12.01367
307.9268 8.736328
308.4089 7.394531
308.8911 9.637695
309.3732 11.91553
309.8553 10.70654
310.3374 6.971680
310.8195 3.952148
311.3016 4.826660
311.7838 6.540039
312.2659 6.108887
312.7480 2.036133
313.2301 2.097168
313.7122 5.540039
314.1943 7.550781
314.6765 6.485840
315.1586 2.771973
315.6407 12.25391
316.1228 16.57080
316.6049 13.99023
317.0870 10.67920
317.5692 8.563965
318.0513 7.571777
318.5334 7.613770
319.0155 11.42090
319.4976 13.91260
319.9797 11.53320
320.4619 3.481445
320.9440 2.047363
321.4261 5.2246001E-02
321.9082 4.462891
322.3903 6.749512
322.8724 2.979492
323.3546 0.3764650
323.8367 1.498535
324.3188 0.4340820
324.8009 0.6577150
325.2830 2.383789
325.7651 3.497070
326.2473 3.229980
326.7294 1.938477
327.2115 1.148926
327.6936 8.657715
328.1757 18.79248
328.6578 23.18945
329.1400 16.70508
329.6221 8.556152
330.1042 2.489258
330.5863 0.6083980
331.0684 3.187500
331.5505 5.467773
332.0327 7.091797
332.5148 7.031738
332.9969 2.953125
333.4790 1.9530000E-03
333.9611 0.4125980
334.4432 1.511230
334.9254 6.803223
335.4075 18.40283
335.8896 30.88330
336.3717 35.34717
336.8538 27.13818
337.3359 20.95703
337.8180 22.27930
338.3001 31.18066
338.7823 34.50391
339.2644 30.32617
339.7465 23.83984
340.2286 20.35107
340.7107 20.39844
341.1928 22.26025
341.6750 26.66113
342.1571 32.21973
342.6392 33.54980
343.1213 30.18555
343.6034 25.52197
344.0855 21.08252
344.5677 16.98779
345.0498 16.08252
345.5319 19.33154
346.0140 24.50342
346.4961 25.91602
346.9782 23.42578
347.4604 22.75244
347.9425 28.86963
348.4246 39.72607
348.9067 47.34277
349.3888 50.90674
349.8709 52.95264
350.3531 56.85889
350.8352 61.78662
351.3173 64.95996
351.7994 62.70605
352.2815 58.76123
352.7636 59.70068
353.2458 65.48096
353.7279 72.86523
354.2100 79.93311
354.6921 86.55664
355.1742 92.67383
355.6563 99.65674
356.1385 104.6646
356.6206 103.2275
357.1027 96.61621
357.5848 91.25928
358.0669 92.34619
358.5490 95.81641
359.0312 97.75439
359.5133 96.90283
359.9954 95.73633
360.4775 94.91650
360.9596 94.90137
361.4417 96.59766
361.9239 104.3477
362.4060 110.9648
362.8881 111.3130
363.3702 103.3740
363.8523 97.38477
364.3344 98.82861
364.8166 103.2290
365.2987 105.5151
365.7808 102.7769
366.2629 99.45410
366.7450 97.02783
367.2271 95.50000
367.7093 92.48242
368.1914 84.69238
368.6735 77.14307
369.1556 73.09570
369.6377 76.54199
370.1198 78.58105
370.6020 77.76855
371.0841 74.96582
371.5662 74.11523
372.0483 79.16309
372.5304 81.54443
373.0125 76.87061
373.4947 60.20801
373.9768 49.67383
374.4589 48.03564
374.9410 50.20020
375.4231 47.64795
375.9052 38.42773
376.3874 30.17480
376.8695 25.53271
377.3516 24.44922
377.8337 22.96777
378.3158 20.92090
378.7979 19.05664
379.2801 18.63574
379.7622 19.72949
380.2443 21.62891
380.7264 25.09326
381.2085 28.49219
381.6906 27.02881
382.1728 20.69189
382.6549 13.97559
383.1370 9.129395
383.6191 6.149414
384.1012 5.830566
384.5833 8.522949
385.0655 12.37256
385.5476 15.50391
386.0297 17.55127
386.5118 17.99805
386.9939 15.93799
387.4760 13.27344
387.9582 13.11279
388.4403 15.42871
388.9224 17.09277
389.4045 14.65723
389.8866 10.23584
390.3687 6.847168
390.8509 6.373047
391.3330 6.281738
391.8151 5.369141
392.2972 3.751465
392.7793 1.345215
393.2614 4.275879
393.7436 9.331055
394.2257 10.71387
394.7078 6.114258
395.1899 2.257813
395.6720 2.933594
396.1541 5.681641
396.6363 6.513184
397.1184 1.696777
397.6005 2.553711
398.0826 3.378418
398.5647 3.4179999E-03
399.0468 1.300293
399.5290 2.991699
400.0111 7.938477
400.4932 9.531250
400.9753 4.073242
401.4574 0.2646480
401.9395 0.5195310
402.4217 1.093750
402.9038 2.066895
403.3859 2.011719
403.8680 1.932129
404.3501 2.315918
404.8322 3.259766
405.3144 4.327148
405.7965 5.535645
406.2786 6.794922
406.7607 7.861816
407.2428 8.639160
407.7249 9.711914
408.2071 11.26074
408.6892 13.24463
409.1713 15.39795
409.6534 17.71387
410.1355 20.19092
410.6176 23.22412
411.0998 26.57617
411.5819 28.38525
412.0640 27.26221
412.5461 26.14014
413.0282 32.61377
413.5103 44.88818
413.9925 52.65869
414.4746 44.99805
414.9567 30.66553
415.4388 24.27148
415.9209 27.63574
416.4030 32.26221
416.8852 30.54102
417.3673 25.43359
417.8494 21.77344
418.3315 24.47900
418.8136 26.78662
419.2957 22.37256
419.7779 12.63867
420.2600 6.432617
420.7421 10.88037
421.2242 18.65820
421.7063 24.27441
422.1884 25.53711
422.6706 27.22412
423.1527 31.29395
423.6348 36.52734
424.1169 40.63135
424.5990 43.60449
425.0811 45.08398
425.5633 44.08350
426.0454 39.87354
426.5275 37.90234
427.0096 37.69678
427.4917 39.95117
427.9738 45.74658
428.4560 57.91699
428.9381 67.44336
429.4202 72.92334
429.9023 74.99463
430.3844 75.77344
430.8665 74.67529
431.3487 73.90723
431.8308 74.26123
432.3129 75.69189
432.7950 79.60742
433.2771 86.54932
433.7592 94.67041
434.2414 101.7783
434.7235 107.9824
435.2056 114.2603
435.6877 121.1079
436.1698 128.1455
436.6519 134.2881
437.1341 139.6548
437.6162 145.7373
438.0983 154.9175
438.5804 165.3677
439.0625 173.1226
439.5446 176.3643
440.0268 180.8701
440.5089 193.0146
440.9910 210.2295
441.4731 226.9995
441.9552 241.3145
442.4373 254.2397
442.9195 265.1177
443.4016 274.0757
443.8837 286.0879
444.3658 306.0703
444.8479 328.2900
445.3300 348.0537
445.8122 364.4009
446.2943 378.4175
446.7764 388.2925
447.2585 395.9316
447.7406 406.2681
448.2227 426.4790
448.7049 442.5776
449.1870 449.5869
449.6691 445.5977
450.1512 444.2134
450.6333 448.3965
451.1154 451.7988
451.5976 447.9858
452.0797 435.0566
452.5618 422.9995
453.0439 413.4175
453.5260 405.4121
454.0081 396.6777
454.4903 387.4541
454.9724 377.0718
455.4545 362.6938
455.9366 345.4404
456.4187 334.4653
456.9008 330.8696
457.3830 329.3657
457.8651 324.4893
458.3472 316.4473
458.8293 305.8979
459.3114 290.6562
459.7935 275.1523
460.2757 266.2441
460.7578 262.7998
461.2399 258.4897
461.7220 246.8315
462.2041 233.9653
462.6862 226.1152
463.1684 224.7427
463.6505 224.2749
464.1326 223.8623
464.6147 222.7930
465.0968 219.8838
465.5789 211.3540
466.0611 204.7588
466.5432 203.9062
467.0253 207.9863
467.5074 209.0049
467.9895 203.0273
468.4716 196.7246
468.9538 193.2354
469.4359 193.5708
469.9180 194.6030
470.4001 197.0186
470.8822 199.5845
471.3643 200.7314
471.8465 200.7358
472.3286 197.9741
472.8107 190.3042
473.2928 179.3472
473.7749 175.5083
474.2570 180.0469
474.7392 185.0181
475.2213 184.0474
475.7034 177.9756
476.1855 172.7671
476.6676 169.2427
477.1497 165.7671
477.6319 161.1440
478.1140 155.7080
478.5961 150.0073
479.0782 143.2104
479.5603 136.0571
480.0424 129.9819
480.5246 124.9629
481.0067 120.0718
481.4888 113.8052
481.9709 107.7847
482.4530 103.5317
482.9352 101.7124
483.4173 100.6099
483.8994 100.1016
484.3815 99.69922
484.8636 98.67334
485.3457 98.53320
485.8279 96.00684
486.3100 88.36377
486.7921 75.63818
487.2742 67.65088
487.7563 68.19824
488.2384 69.70654
488.7206 67.72900
489.2027 60.21582
489.6848 55.06055
490.1669 52.83057
490.6490 52.58154
491.1311 53.33545
491.6133 55.28174
492.0954 56.00098
492.5775 53.77393
493.0596 49.94580
493.5417 50.01953
494.0238 53.97363
494.5060 58.70898
494.9881 63.31934
495.4702 66.74268
495.9523 65.50146
496.4344 58.08643
496.9165 50.53320
497.3987 49.08984
497.8808 51.78564
498.3629 54.95605
498.8450 59.63867
499.3271 62.19482
499.8092 58.83936
500.2914 50.63232
500.7735 43.42822
501.2556 39.74463
501.7377 37.58984
502.2198 36.14600
502.7019 36.17773
503.1841 34.82959
503.6662 30.19775
504.1483 24.72559
504.6304 21.23389
505.1125 20.27637
505.5946 20.48828
506.0768 22.03906
506.5589 24.60693
507.0410 26.90918
507.5231 29.24170
508.0052 30.34131
508.4873 28.97412
508.9695 25.13086
509.4516 22.12793
509.9337 19.63721
510.4158 18.44092
510.8979 20.53857
511.3800 24.97607
511.8622 27.30420
512.3443 25.78516
512.8264 22.43262
513.3085 18.86572
513.7906 15.52490
514.2728 13.94092
514.7549 17.83301
515.2370 22.34521
515.7191 22.76416
516.2012 18.29248
516.6833 12.52148
517.1655 6.058105
517.6476 2.4410000E-03
518.1297 4.836426
518.6118 7.577637
519.0939 9.906738
519.5760 13.47070
520.0582 16.70215
520.5403 15.94141
521.0224 7.521973
521.5045 0.2924800
521.9866 3.230957
522.4688 3.026367
522.9509 1.848145
523.4330 1.178223
523.9151 3.324707
524.3972 2.043945
524.8793 2.701660
525.3615 6.959961
525.8436 10.29932
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1288.552 21.60010
1289.034 17.85498
1289.516 11.54639
1289.998 9.810547
1290.481 11.34619
1290.963 12.71387
1291.445 13.19385
1291.927 12.80469
1292.409 11.11572
1292.891 10.33936
1293.373 14.19434
1293.855 18.18066
1294.338 14.20361
1294.820 6.869141
1295.302 5.658691
1295.784 13.41357
1296.266 17.37500
1296.748 17.48486
1297.230 14.82520
1297.712 5.812500
1298.194 0.8081050
1298.677 5.106934
1299.159 15.21191
1299.641 18.62646
1300.123 15.09668
1300.605 13.54004
1301.087 13.51367
1301.569 12.43018
1302.051 7.422363
1302.533 2.540039
1303.016 0.0000000E+00
