#\#CIF_2.0
#------------------------------------------------------------------------------
#$Date: 2018-06-07 11:28:54 +0300 (Thu, 07 Jun 2018) $
#$Revision: 1132 $
#$URL: svn://172.16.1.111/rod/cif/2/31/00/2310012.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2310012
loop_
_publ_author_name
'Giglio, M.'
_publ_section_title
;
 Die kristallstruktur von Na2Zn(SO4)2*4H2O (Zn-blodit) Locality: synthetic
;
_journal_name_full               'Acta Crystallographica'
_journal_page_first              789
_journal_page_last               794
_journal_paper_doi               10.1107/S0365110X5800222X
_journal_volume                  11
_journal_year                    1958
_chemical_compound_source        R110213
_chemical_formula_sum            'H8 Na2 O12 S2 Zn'
_chemical_name_mineral           Changoite
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.58
_cell_angle_gamma                90
_cell_length_a                   11.05
_cell_length_b                   8.23
_cell_length_c                   5.54
_cell_volume                     495.251
_exptl_crystal_density_diffrn    2.518
_cod_original_formula_sum        'Zn Na2 S2 O12 H8'
_cod_database_code               9011018
_raman_determination_method      experimental
_raman_measurement_device.location 'Arizona University'
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  'Nicolet Almega XR'
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.5
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 780
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 4
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 400
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 10
_rod_data_source.file            R110213.rod
_rod_data_source.block           3500000
_rod_database.code               2310012
loop_
_raman_complementary.id
_raman_complementary.method
1 XRD
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9011018 COD http://www.crystallography.net/cod/9011018.html
;
XRD analysis data was done.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
158.1356 0.0000000E+00
158.6177 4.5441002E-02
159.0999 0.5473630
159.5820 1.035706
160.0641 1.494690
160.5462 1.578735
161.0283 0.6288760
161.5104 0.1755980
161.9926 0.3150940
162.4747 2.225861
162.9568 4.355743
163.4389 5.451172
163.9210 5.558411
164.4031 5.357910
164.8853 4.749542
165.3674 3.951904
165.8495 3.196136
166.3316 2.394073
166.8137 1.975342
167.2958 2.680542
167.7780 4.214874
168.2601 5.448700
168.7422 5.574768
169.2243 4.904755
169.7064 4.736084
170.1885 5.693604
170.6707 6.518372
171.1528 6.055756
171.6349 4.624176
172.1170 3.574921
172.5991 4.480377
173.0812 7.495300
173.5634 9.161438
174.0455 7.713654
174.5276 6.070007
175.0097 5.472778
175.4918 5.899048
175.9739 6.598755
176.4561 6.755463
176.9382 6.190674
177.4203 5.678467
177.9024 5.010651
178.3845 4.560730
178.8666 4.641052
179.3488 5.252899
179.8309 6.089142
180.3130 6.681580
180.7951 7.028229
181.2772 7.092926
181.7593 6.626495
182.2415 6.101715
182.7236 5.870972
183.2057 6.096283
183.6878 6.636169
184.1699 7.138672
184.6520 7.610504
185.1342 7.700104
185.6163 7.017792
186.0984 6.120483
186.5805 5.676361
187.0626 5.929199
187.5447 6.468353
188.0269 6.670135
188.5090 6.553314
188.9911 6.371185
189.4732 6.018372
189.9553 5.676575
190.4374 5.716888
190.9196 6.378998
191.4017 7.207794
191.8838 7.549744
192.3659 7.413849
192.8480 7.090515
193.3301 6.625549
193.8123 6.047089
194.2944 5.446045
194.7765 4.697021
195.2586 4.109192
195.7407 4.089722
196.2228 4.654602
196.7050 5.110657
197.1871 4.963531
197.6692 4.220245
198.1513 3.391449
198.6334 2.663666
199.1155 2.037903
199.5977 1.383209
200.0798 0.5843810
200.5619 0.1073300
201.0440 0.4224240
201.5261 0.3070070
202.0082 0.1919250
202.4904 0.1540220
202.9725 8.2794003E-02
203.4546 0.1360780
203.9367 0.5046080
204.4188 0.8688050
204.9009 0.9737850
205.3831 0.5943910
205.8652 0.6693120
206.3473 1.902130
206.8294 3.056702
207.3115 3.332092
207.7936 2.645447
208.2758 1.523712
208.7579 0.6266780
209.2400 0.2333680
209.7221 0.3579100
210.2042 0.7478640
210.6863 2.104431
211.1685 3.055786
211.6506 3.471008
212.1327 3.654846
212.6148 4.064392
213.0969 4.944305
213.5790 5.514618
214.0612 5.818817
214.5433 5.815094
215.0254 5.209839
215.5075 4.011810
215.9896 2.935944
216.4717 2.997345
216.9539 5.020630
217.4360 6.198425
217.9181 5.725952
218.4002 4.768341
218.8823 4.512817
219.3644 5.248230
219.8466 6.362366
220.3287 7.026123
220.8108 7.155792
221.2929 7.344543
221.7750 7.815186
222.2571 8.330841
222.7393 8.567017
223.2214 8.435089
223.7035 8.156952
224.1856 7.984863
224.6677 7.910187
225.1498 7.854767
225.6320 7.853027
226.1141 7.846039
226.5962 7.698792
227.0783 7.337189
227.5604 6.990509
228.0425 7.004272
228.5247 7.282349
229.0068 7.365845
229.4889 6.895111
229.9710 6.116150
230.4531 5.630798
230.9352 5.640991
231.4174 5.648560
231.8995 5.231232
232.3816 4.502960
232.8637 3.765350
233.3458 3.047455
233.8279 2.420685
234.3101 2.143951
234.7922 2.405151
235.2743 2.724945
235.7564 2.689575
236.2385 2.501678
236.7206 2.597443
237.2028 3.455048
237.6849 4.806885
238.1670 5.495758
238.6491 5.246277
239.1312 4.670074
239.6133 3.708069
240.0955 2.693817
240.5776 2.175812
241.0597 2.559662
241.5418 3.650116
242.0239 4.536591
242.5060 5.118256
242.9882 5.650940
243.4703 6.152985
243.9524 6.680267
244.4345 7.311676
244.9166 8.093384
245.3987 8.970398
245.8809 9.689087
246.3630 10.03830
246.8451 10.53229
247.3272 11.42282
247.8093 12.44989
248.2914 13.24704
248.7736 13.60172
249.2557 13.66599
249.7378 14.04477
250.2199 14.94238
250.7020 15.93982
251.1841 17.24875
251.6663 18.54095
252.1484 19.35062
252.6305 19.44843
253.1126 19.10223
253.5947 19.15604
254.0768 20.09491
254.5590 20.87271
255.0411 21.17343
255.5232 21.42828
256.0053 22.17682
256.4874 23.63113
256.9695 25.44901
257.4517 26.82425
257.9338 27.48688
258.4159 27.95242
258.8980 27.73709
259.3801 27.44858
259.8622 27.95151
260.3444 29.56165
260.8265 31.58084
261.3086 32.57602
261.7907 31.49484
262.2728 30.85355
262.7549 30.74353
263.2371 31.03326
263.7192 31.81509
264.2013 33.09650
264.6834 34.28864
265.1655 34.43921
265.6476 32.90009
266.1298 31.90790
266.6119 31.84296
267.0940 32.16260
267.5761 32.47653
268.0582 32.70978
268.5403 32.79892
269.0225 32.66306
269.5046 32.23688
269.9867 31.68338
270.4688 30.66733
270.9509 29.76340
271.4330 29.63937
271.9152 30.35660
272.3973 31.23450
272.8794 31.65079
273.3615 31.52124
273.8436 31.25507
274.3257 30.46323
274.8079 29.85403
275.2900 30.27982
275.7721 31.67499
276.2542 32.85754
276.7363 32.91910
277.2184 31.94623
277.7006 31.06412
278.1827 30.05865
278.6648 29.32712
279.1469 29.46118
279.6290 30.36691
280.1111 30.95108
280.5933 30.40292
281.0754 29.03003
281.5575 28.06613
282.0396 27.83151
282.5217 27.61661
283.0038 26.91046
283.4860 25.80832
283.9681 24.81226
284.4502 24.19363
284.9323 23.78333
285.4144 23.14603
285.8965 22.06540
286.3787 21.28210
286.8608 21.48926
287.3429 22.39362
287.8250 22.89316
288.3071 22.47015
288.7892 21.70425
289.2714 21.52795
289.7535 22.02933
290.2356 22.30542
290.7177 21.81015
291.1998 20.76367
291.6819 19.73621
292.1641 18.84396
292.6462 18.03595
293.1283 17.24088
293.6104 16.45416
294.0925 15.71082
294.5746 14.98746
295.0568 14.34366
295.5389 13.95300
296.0210 13.93246
296.5031 13.82333
296.9852 12.93219
297.4673 11.57339
297.9495 10.67709
298.4316 11.02701
298.9137 11.85568
299.3958 11.97031
299.8779 11.23807
300.3600 10.25232
300.8422 9.112366
301.3243 8.025726
301.8064 7.437408
302.2885 7.748840
302.7706 8.304077
303.2527 8.286438
303.7349 7.650055
304.2170 7.085632
304.6991 7.019684
305.1812 7.171326
305.6633 7.153900
306.1454 6.882507
306.6276 6.528595
307.1097 6.243713
307.5918 6.023468
308.0739 5.763275
308.5560 5.400757
309.0381 4.999390
309.5203 4.568024
310.0024 4.084869
310.4845 3.797699
310.9666 4.102783
311.4487 4.826996
311.9308 5.052643
312.4130 4.348511
312.8951 3.454132
313.3772 3.142517
313.8593 3.315521
314.3414 3.329437
314.8235 2.416473
315.3057 1.122772
315.7878 1.167725
316.2699 3.371490
316.7520 5.259369
317.2341 4.454163
317.7162 1.964417
318.1984 9.2864998E-02
318.6805 0.8254390
319.1626 0.7510680
319.6447 0.6613460
320.1268 0.5899350
320.6089 0.3197630
321.0911 0.6478880
321.5732 1.795441
322.0553 2.363281
322.5374 2.081635
323.0195 1.386353
323.5016 0.6549990
323.9838 0.1137700
324.4659 0.9114380
324.9480 1.935730
325.4301 2.837708
325.9122 3.196899
326.3943 2.935394
326.8765 2.385132
327.3586 1.532471
327.8407 0.4970400
328.3228 2.0630000E-02
328.8049 0.2173160
329.2870 0.9444890
329.7692 2.069458
330.2513 3.539490
330.7334 4.650452
331.2155 4.568756
331.6976 3.927795
332.1797 4.517365
332.6619 7.074249
333.1440 9.308228
333.6261 8.786926
334.1082 6.461792
334.5903 4.433899
335.0724 3.699005
335.5546 3.425415
336.0367 2.383209
336.5188 0.4754640
337.0009 1.139038
337.4830 1.633698
337.9651 1.425171
338.4473 1.293793
338.9294 1.316742
339.4115 1.440216
339.8936 1.621063
340.3757 1.864746
340.8578 2.166840
341.3400 2.476929
341.8221 2.918243
342.3042 3.660675
342.7863 4.735809
343.2684 5.920288
343.7505 7.262878
344.2327 8.626892
344.7148 9.575317
345.1969 9.862518
345.6790 10.13538
346.1611 11.24246
346.6432 13.04770
347.1254 14.93192
347.6075 16.78677
348.0896 18.60739
348.5717 20.36838
349.0538 22.07828
349.5359 23.64386
350.0181 24.78403
350.5002 25.72968
350.9823 27.41324
351.4644 30.82742
351.9465 34.16876
352.4286 35.99069
352.9108 36.57788
353.3929 37.35873
353.8750 39.04269
354.3571 41.31943
354.8392 43.43222
355.3214 45.43011
355.8035 47.17639
356.2856 48.55939
356.7677 49.68732
357.2498 50.73026
357.7319 51.73209
358.2141 52.63028
358.6962 53.27951
359.1783 53.58435
359.6604 54.24753
360.1425 55.98849
360.6246 57.77814
361.1068 58.53296
361.5889 58.19263
362.0710 57.50427
362.5531 57.06528
363.0352 56.88510
363.5173 56.67639
363.9995 56.81479
364.4816 56.55402
364.9637 55.45715
365.4458 53.67242
365.9279 51.45221
366.4100 48.81662
366.8922 46.08438
367.3743 44.37958
367.8564 44.68161
368.3385 44.54486
368.8206 43.58765
369.3027 42.10437
369.7849 40.41592
370.2670 38.58719
370.7491 36.40927
371.2312 33.54236
371.7133 29.57288
372.1954 26.31436
372.6776 24.31390
373.1597 22.42267
373.6418 19.76166
374.1239 16.62772
374.6060 14.00974
375.0881 12.69733
375.5703 12.57718
376.0524 11.99753
376.5345 10.87134
377.0166 9.597656
377.4987 8.042999
377.9808 6.443604
378.4630 5.148804
378.9451 4.356689
379.4272 3.931763
379.9093 3.550842
380.3914 3.443604
380.8735 2.839783
381.3557 0.9617610
381.8378 0.8652340
382.3199 1.499207
382.8020 0.9001460
383.2841 2.0354999E-02
383.7662 0.2290650
384.2484 0.3807370
384.7305 0.6011660
385.2126 0.1509400
385.6947 0.4828490
386.1768 1.036621
386.6589 1.582947
387.1411 2.453308
387.6232 3.984314
388.1053 5.742798
388.5874 6.134338
389.0695 4.352478
389.5516 2.953552
390.0338 2.312012
390.5159 2.135010
390.9980 2.460449
391.4801 3.457153
391.9622 4.750061
392.4443 5.682312
392.9265 6.114624
393.4086 6.693176
393.8907 7.656311
394.3728 8.752075
394.8549 9.681274
395.3370 10.47437
395.8192 11.43677
396.3013 12.98108
396.7834 14.84369
397.2655 16.01740
397.7476 16.17407
398.2297 16.48785
398.7119 17.81091
399.1940 19.58887
399.6761 21.14557
400.1582 22.32214
400.6403 23.20844
401.1224 23.67511
401.6046 23.77515
402.0867 24.35034
402.5688 25.91760
403.0509 27.77521
403.5330 28.92816
404.0151 29.34839
404.4973 30.17212
404.9794 32.29144
405.4615 35.02521
405.9436 37.24097
406.4257 38.78845
406.9078 39.87347
407.3900 40.51300
407.8721 40.76868
408.3542 41.04175
408.8363 41.06750
409.3184 41.38007
409.8005 42.47009
410.2827 44.16931
410.7648 45.87317
411.2469 47.31219
411.7290 48.60992
412.2111 50.05383
412.6932 51.74768
413.1754 53.30127
413.6575 54.35541
414.1396 55.38641
414.6217 57.07544
415.1038 59.46814
415.5859 61.83594
416.0681 63.44818
416.5502 64.23090
417.0323 64.94360
417.5144 65.18677
417.9965 65.77667
418.4786 67.19519
418.9608 69.18390
419.4429 71.30621
419.9250 73.35083
420.4071 75.25952
420.8892 76.86298
421.3713 77.94885
421.8535 79.01923
422.3356 80.29950
422.8177 81.44098
423.2998 81.86493
423.7819 81.69073
424.2640 81.85858
424.7462 83.53754
425.2283 86.90314
425.7104 89.25415
426.1925 89.27814
426.6746 89.67365
427.1567 91.57318
427.6389 94.26233
428.1210 96.55640
428.6031 97.85748
429.0852 98.63135
429.5673 99.75024
430.0494 101.2272
430.5316 103.0087
431.0137 105.3465
431.4958 107.8111
431.9779 110.2521
432.4600 112.6176
432.9421 114.6589
433.4243 115.9326
433.9064 116.6708
434.3885 117.9237
434.8706 119.8829
435.3527 122.0409
435.8348 124.1376
436.3170 126.2059
436.7991 128.3298
437.2812 130.5478
437.7633 132.7831
438.2454 134.9733
438.7275 137.1248
439.2097 139.1221
439.6918 140.6453
440.1739 142.3844
440.6560 145.5438
441.1381 150.1764
441.6202 154.8902
442.1024 159.4636
442.5845 163.8201
443.0666 167.6495
443.5487 170.9908
444.0308 174.5433
444.5129 178.9636
444.9951 184.0851
445.4772 188.4998
445.9593 191.7474
446.4414 194.9156
446.9235 198.8492
447.4056 202.7617
447.8878 205.4874
448.3699 206.6322
448.8520 206.6157
449.3341 206.1158
449.8162 205.4522
450.2983 203.2165
450.7805 198.6362
451.2626 193.4650
451.7447 188.5162
452.2268 183.7457
452.7089 178.7188
453.1910 173.1547
453.6732 167.1578
454.1553 161.1320
454.6374 154.5505
455.1195 148.8943
455.6016 144.9728
456.0837 141.5781
456.5659 137.5886
457.0480 132.8265
457.5301 128.2516
458.0122 124.9374
458.4943 122.8484
458.9764 120.8412
459.4586 119.0869
459.9407 117.0911
460.4228 114.2353
460.9049 111.0562
461.3870 108.5303
461.8691 107.0950
462.3513 106.2892
462.8334 105.8513
463.3155 105.7480
463.7976 105.0455
464.2797 103.1599
464.7618 100.8969
465.2440 99.24890
465.7261 98.20508
466.2082 97.37109
466.6903 96.52899
467.1724 95.86639
467.6545 95.75659
468.1367 96.18414
468.6188 96.57806
469.1009 96.63940
469.5830 96.33087
470.0651 95.45667
470.5472 92.90259
471.0294 91.26611
471.5115 92.11932
471.9936 93.87567
472.4757 94.46729
472.9578 93.38251
473.4399 91.59766
473.9221 90.28998
474.4042 89.63129
474.8863 88.43207
475.3684 86.52557
475.8505 84.31348
476.3326 81.61261
476.8148 78.78717
477.2969 76.40265
477.7790 74.74915
478.2611 73.56049
478.7432 72.33569
479.2253 71.14612
479.7075 69.73712
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