#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500011.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500011
loop_
_publ_author_name
'El Mendili, Y'
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa Aesar 98%'
_chemical_formula_structural     'K Al (S O4)2'
_chemical_formula_sum            'Al K O8 S2'
_chemical_name_mineral           Steklite
_chemical_name_systematic        'Al K O8 S2'
_space_group_IT_number           150
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  'P 3 2"'
_symmetry_space_group_name_H-M   'P 3 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   4.706
_cell_length_b                   4.706
_cell_length_c                   7.96
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 60
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2500.29
_rod_data_source.file            Steklite.rod
_rod_data_source.block           1000005
_rod_database.code               3500011
_solsa_sample.id                 CN-AA00-0012
_raman_measurement.datetime_initiated 2017-09-18
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1011235 COD http://www.crystallography.net/cod/1011235.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 2.511040e+002
5.113732e+001 2.465089e+002
5.210155e+001 2.419805e+002
5.306579e+001 2.372934e+002
5.403002e+001 2.321462e+002
5.499426e+001 2.259654e+002
5.595849e+001 2.202461e+002
5.692272e+001 2.169646e+002
5.788696e+001 2.154923e+002
5.885119e+001 2.140671e+002
5.981542e+001 2.059999e+002
6.077965e+001 1.939273e+002
6.174389e+001 1.827120e+002
6.270812e+001 1.746614e+002
6.367235e+001 1.703069e+002
6.463658e+001 1.672843e+002
6.560081e+001 1.653193e+002
6.656505e+001 1.647347e+002
6.752928e+001 1.656636e+002
6.849352e+001 1.678718e+002
6.945775e+001 1.714784e+002
7.042198e+001 1.766830e+002
7.138622e+001 1.829931e+002
7.235045e+001 1.897683e+002
7.331468e+001 1.991661e+002
7.427892e+001 2.073919e+002
7.524315e+001 2.122507e+002
7.620738e+001 2.135772e+002
7.717162e+001 2.131954e+002
7.813585e+001 2.155691e+002
7.910008e+001 2.185369e+002
8.006432e+001 2.199521e+002
8.102855e+001 2.183650e+002
8.199278e+001 2.138758e+002
8.295702e+001 2.096847e+002
8.392125e+001 2.051942e+002
8.488548e+001 2.004700e+002
8.584972e+001 1.956256e+002
8.681395e+001 1.896672e+002
8.777818e+001 1.855661e+002
8.874242e+001 1.847499e+002
8.970665e+001 1.863331e+002
9.067088e+001 1.873465e+002
9.163512e+001 1.847352e+002
9.259935e+001 1.818662e+002
9.356358e+001 1.793135e+002
9.452782e+001 1.775461e+002
9.549205e+001 1.772562e+002
9.645628e+001 1.800031e+002
9.742052e+001 1.837330e+002
9.838475e+001 1.868925e+002
9.934898e+001 1.881889e+002
1.003132e+002 1.875502e+002
1.012775e+002 1.872306e+002
1.022417e+002 1.873031e+002
1.032059e+002 1.881865e+002
1.041701e+002 1.905405e+002
1.051344e+002 1.977164e+002
1.060986e+002 2.027167e+002
1.070628e+002 2.037243e+002
1.080271e+002 2.016762e+002
1.089913e+002 2.009352e+002
1.099555e+002 2.037310e+002
1.109198e+002 2.071452e+002
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1.128482e+002 2.153802e+002
1.138125e+002 2.190492e+002
1.147767e+002 2.208580e+002
1.157409e+002 2.215317e+002
1.167052e+002 2.215271e+002
1.176694e+002 2.212618e+002
1.186336e+002 2.206521e+002
1.195979e+002 2.188639e+002
1.205621e+002 2.159433e+002
1.215263e+002 2.126179e+002
1.224906e+002 2.100202e+002
1.234548e+002 2.087197e+002
1.244190e+002 2.083501e+002
1.253833e+002 2.093626e+002
1.263475e+002 2.114522e+002
1.273117e+002 2.134473e+002
1.282760e+002 2.143291e+002
1.292402e+002 2.154934e+002
1.302044e+002 2.173999e+002
1.311687e+002 2.200426e+002
1.321329e+002 2.224381e+002
1.330971e+002 2.232558e+002
1.340614e+002 2.240618e+002
1.350256e+002 2.260067e+002
1.359898e+002 2.298900e+002
1.369541e+002 2.352919e+002
1.379183e+002 2.399178e+002
1.388825e+002 2.437928e+002
1.398468e+002 2.473395e+002
1.408110e+002 2.510917e+002
1.417752e+002 2.549174e+002
1.427395e+002 2.586014e+002
1.437037e+002 2.628837e+002
1.446679e+002 2.674058e+002
1.456322e+002 2.711415e+002
1.465964e+002 2.722949e+002
1.475606e+002 2.739080e+002
1.485249e+002 2.768699e+002
1.494891e+002 2.807189e+002
1.504533e+002 2.833969e+002
1.514176e+002 2.836959e+002
1.523818e+002 2.830852e+002
1.533460e+002 2.813382e+002
1.543103e+002 2.784735e+002
1.552745e+002 2.750695e+002
1.562387e+002 2.726234e+002
1.572030e+002 2.707183e+002
1.581672e+002 2.689166e+002
1.591314e+002 2.668306e+002
1.600957e+002 2.642006e+002
1.610599e+002 2.608891e+002
1.620241e+002 2.569604e+002
1.629884e+002 2.529656e+002
1.639526e+002 2.496276e+002
1.649168e+002 2.480774e+002
1.658811e+002 2.459924e+002
1.668453e+002 2.421079e+002
1.678095e+002 2.374184e+002
1.687738e+002 2.337612e+002
1.697380e+002 2.326892e+002
1.707022e+002 2.328152e+002
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1.726307e+002 2.361747e+002
1.735949e+002 2.380690e+002
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1.755234e+002 2.373310e+002
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1.861300e+002 2.921722e+002
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2.025219e+002 1.709529e+002
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2.044504e+002 1.531700e+002
2.054146e+002 1.479876e+002
2.063788e+002 1.453179e+002
2.073431e+002 1.412828e+002
2.083073e+002 1.342278e+002
2.092715e+002 1.264132e+002
2.102358e+002 1.185841e+002
2.112000e+002 1.112941e+002
2.121642e+002 1.058121e+002
2.131285e+002 1.032480e+002
2.140927e+002 1.023172e+002
2.150569e+002 1.022040e+002
2.160212e+002 1.021974e+002
2.169854e+002 1.021798e+002
2.179496e+002 1.007711e+002
2.189139e+002 9.783080e+001
2.198781e+002 9.445625e+001
2.208423e+002 9.225908e+001
2.218066e+002 9.249098e+001
2.227708e+002 9.186525e+001
2.237350e+002 9.023441e+001
2.246993e+002 8.816286e+001
2.256635e+002 8.653177e+001
2.266277e+002 8.574710e+001
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2.324131e+002 7.496447e+001
2.333774e+002 7.328371e+001
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2.488051e+002 4.697993e+001
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2.507336e+002 4.368815e+001
2.516978e+002 4.150983e+001
2.526620e+002 3.915130e+001
2.536263e+002 3.700911e+001
2.545905e+002 3.545085e+001
2.555547e+002 3.444499e+001
2.565190e+002 3.291584e+001
2.574832e+002 3.087905e+001
2.584474e+002 2.882267e+001
2.594117e+002 2.737651e+001
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2.632686e+002 2.468379e+001
2.642328e+002 2.416851e+001
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2.661613e+002 2.443024e+001
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2.690540e+002 2.122064e+001
2.700182e+002 2.041157e+001
2.709825e+002 1.999658e+001
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2.729109e+002 1.978167e+001
2.738752e+002 1.987546e+001
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2.758036e+002 1.962136e+001
2.767679e+002 1.898182e+001
2.777321e+002 1.762407e+001
2.786964e+002 1.571722e+001
2.796606e+002 1.489326e+001
2.806248e+002 1.653992e+001
2.815891e+002 1.778280e+001
2.825533e+002 1.757513e+001
2.835175e+002 1.598530e+001
2.844818e+002 1.499642e+001
2.854460e+002 1.663503e+001
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2.893029e+002 1.960662e+001
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2.912314e+002 2.104040e+001
2.921956e+002 2.160750e+001
2.931599e+002 2.178690e+001
2.941241e+002 2.170475e+001
2.950883e+002 2.221940e+001
2.960526e+002 2.329842e+001
2.970168e+002 2.449404e+001
2.979810e+002 2.544484e+001
2.989453e+002 2.592852e+001
2.999095e+002 2.684499e+001
3.008737e+002 2.866467e+001
3.018380e+002 3.069194e+001
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3.037664e+002 3.335703e+001
3.047307e+002 3.489251e+001
3.056949e+002 3.847692e+001
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3.105161e+002 4.806287e+001
3.114803e+002 5.075340e+001
3.124445e+002 5.324160e+001
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loop_
_rod_maintainer_comment.id
_rod_maintainer_comment.author
_rod_maintainer_comment.date
_rod_maintainer_comment.text
1 elmendili 2017-10-06T15:16:14+0300 'COD entry is wrong'