#------------------------------------------------------------------------------
#$Date: 2018-07-20 15:02:54 +0300 (Fri, 20 Jul 2018) $
#$Revision: 1269 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500013.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500013
loop_
_publ_author_name
'El Mendili, Y.'
_publ_section_title
;
 Raman spectrum of commercial niobium(V) oxide
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa Aesar 99.5%'
_chemical_formula_structural     'Nb2 O5'
_chemical_formula_sum            'Nb2 O5'
_chemical_name_mineral           Niobite
_chemical_name_systematic        'niobium(V) oxide'
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 120.8
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   28.51
_cell_length_b                   3.83
_cell_length_c                   17.48
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 180
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2500.29
_rod_data_source.file            Nb2O5.rod
_rod_data_source.block           1000005
_rod_database.code               3500013
_solsa_sample.id                 CN-AA00-0014
_raman_measurement.datetime_initiated 2017-09-18
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1534156 COD http://www.crystallography.net/cod/1534156.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 6.300334e+003
5.113732e+001 7.038441e+003
5.210155e+001 7.463780e+003
5.306579e+001 7.623334e+003
5.403002e+001 7.543913e+003
5.499426e+001 7.125084e+003
5.595849e+001 6.596286e+003
5.692272e+001 6.069556e+003
5.788696e+001 5.577400e+003
5.885119e+001 5.133828e+003
5.981542e+001 4.778180e+003
6.077965e+001 4.497604e+003
6.174389e+001 4.316111e+003
6.270812e+001 4.251215e+003
6.367235e+001 4.318147e+003
6.463658e+001 4.439781e+003
6.560081e+001 4.617693e+003
6.656505e+001 4.834064e+003
6.752928e+001 5.075741e+003
6.849352e+001 5.357610e+003
6.945775e+001 5.626876e+003
7.042198e+001 5.936118e+003
7.138622e+001 6.226564e+003
7.235045e+001 6.404917e+003
7.331468e+001 6.367916e+003
7.427892e+001 6.217531e+003
7.524315e+001 5.939513e+003
7.620738e+001 5.554654e+003
7.717162e+001 5.123118e+003
7.813585e+001 4.732913e+003
7.910008e+001 4.387751e+003
8.006432e+001 4.116865e+003
8.102855e+001 3.941496e+003
8.199278e+001 3.879466e+003
8.295702e+001 3.871660e+003
8.392125e+001 3.910628e+003
8.488548e+001 3.979163e+003
8.584972e+001 4.056943e+003
8.681395e+001 4.149486e+003
8.777818e+001 4.248938e+003
8.874242e+001 4.354521e+003
8.970665e+001 4.469819e+003
9.067088e+001 4.603661e+003
9.163512e+001 4.777099e+003
9.259935e+001 4.949497e+003
9.356358e+001 5.119947e+003
9.452782e+001 5.286248e+003
9.549205e+001 5.434521e+003
9.645628e+001 5.538865e+003
9.742052e+001 5.612723e+003
9.838475e+001 5.658720e+003
9.934898e+001 5.679812e+003
1.003132e+002 5.672848e+003
1.012775e+002 5.653920e+003
1.022417e+002 5.623067e+003
1.032059e+002 5.606291e+003
1.041701e+002 5.641561e+003
1.051344e+002 5.660494e+003
1.060986e+002 5.893526e+003
1.070628e+002 6.295392e+003
1.080271e+002 6.887203e+003
1.089913e+002 7.780200e+003
1.099555e+002 9.376058e+003
1.109198e+002 1.097367e+004
1.118840e+002 1.255044e+004
1.128482e+002 1.405336e+004
1.138125e+002 1.513126e+004
1.147767e+002 1.527358e+004
1.157409e+002 1.498505e+004
1.167052e+002 1.450808e+004
1.176694e+002 1.404144e+004
1.186336e+002 1.362243e+004
1.195979e+002 1.336019e+004
1.205621e+002 1.321948e+004
1.215263e+002 1.309516e+004
1.224906e+002 1.283426e+004
1.234548e+002 1.237310e+004
1.244190e+002 1.187414e+004
1.253833e+002 1.126537e+004
1.263475e+002 1.060577e+004
1.273117e+002 1.010208e+004
1.282760e+002 9.995393e+003
1.292402e+002 9.832802e+003
1.302044e+002 9.573590e+003
1.311687e+002 9.189340e+003
1.321329e+002 8.621468e+003
1.330971e+002 7.656349e+003
1.340614e+002 6.616522e+003
1.350256e+002 5.640714e+003
1.359898e+002 4.818021e+003
1.369541e+002 4.185130e+003
1.379183e+002 3.764255e+003
1.388825e+002 3.504110e+003
1.398468e+002 3.354240e+003
1.408110e+002 3.260182e+003
1.417752e+002 3.240421e+003
1.427395e+002 3.242542e+003
1.437037e+002 3.284860e+003
1.446679e+002 3.348150e+003
1.456322e+002 3.388327e+003
1.465964e+002 3.376075e+003
1.475606e+002 3.361355e+003
1.485249e+002 3.342786e+003
1.494891e+002 3.323047e+003
1.504533e+002 3.309751e+003
1.514176e+002 3.315351e+003
1.523818e+002 3.331589e+003
1.533460e+002 3.358540e+003
1.543103e+002 3.393856e+003
1.552745e+002 3.429377e+003
1.562387e+002 3.455463e+003
1.572030e+002 3.473682e+003
1.581672e+002 3.478065e+003
1.591314e+002 3.463604e+003
1.600957e+002 3.427812e+003
1.610599e+002 3.427444e+003
1.620241e+002 3.467414e+003
1.629884e+002 3.526060e+003
1.639526e+002 3.577704e+003
1.649168e+002 3.615930e+003
1.658811e+002 3.663847e+003
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1.678095e+002 3.790273e+003
1.687738e+002 3.849183e+003
1.697380e+002 3.887996e+003
1.707022e+002 3.930808e+003
1.716665e+002 3.989471e+003
1.726307e+002 4.059215e+003
1.735949e+002 4.125525e+003
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1.755234e+002 4.192040e+003
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1.793803e+002 4.200825e+003
1.803446e+002 4.157311e+003
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2.073431e+002 5.131591e+003
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2.131285e+002 5.183700e+003
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2.160212e+002 5.455254e+003
2.169854e+002 5.553092e+003
2.179496e+002 5.661632e+003
2.189139e+002 5.780741e+003
2.198781e+002 5.903917e+003
2.208423e+002 6.020749e+003
2.218066e+002 6.112982e+003
2.227708e+002 6.219153e+003
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loop_
_rod_maintainer_comment.id
_rod_maintainer_comment.author
_rod_maintainer_comment.date
_rod_maintainer_comment.text
1 elmendili 2017-10-06T15:23:09+0300 'Mineral name changed'