#------------------------------------------------------------------------------
#$Date: 2017-10-05 18:15:36 +0300 (Thu, 05 Oct 2017) $
#$Revision: 219 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500018.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500018
loop_
_publ_author_name
'El Mendili, Y'
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa Aesar 99.9%'
_chemical_formula_structural     'O5 V2'
_chemical_formula_sum            'O5 V2'
_chemical_name_mineral           Shcherbianite
_chemical_name_systematic        'Vanadium oxide'
_space_group_IT_number           31
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac -2'
_symmetry_space_group_name_H-M   'P m n 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.503
_cell_length_b                   4.369
_cell_length_c                   3.557
_raman_determination_method      experimental
_[local]_chemical_compound_color Brown
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 180
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2500.29
_rod_data_source.file            Shcherbianite.rod
_rod_data_source.block           1000005
_rod_database.code               3500018
_solsa_sample.id                 CN-AA00-0019
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1011291 COD http://www.crystallography.net/cod/1011291.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 2.408401e+003
5.113732e+001 2.412581e+003
5.210155e+001 2.419055e+003
5.306579e+001 2.425079e+003
5.403002e+001 2.428563e+003
5.499426e+001 2.428154e+003
5.595849e+001 2.426526e+003
5.692272e+001 2.425641e+003
5.788696e+001 2.426048e+003
5.885119e+001 2.427757e+003
5.981542e+001 2.427472e+003
6.077965e+001 2.423998e+003
6.174389e+001 2.420881e+003
6.270812e+001 2.420316e+003
6.367235e+001 2.424039e+003
6.463658e+001 2.429624e+003
6.560081e+001 2.439552e+003
6.656505e+001 2.452607e+003
6.752928e+001 2.466310e+003
6.849352e+001 2.473410e+003
6.945775e+001 2.481967e+003
7.042198e+001 2.495753e+003
7.138622e+001 2.510751e+003
7.235045e+001 2.520441e+003
7.331468e+001 2.519898e+003
7.427892e+001 2.520753e+003
7.524315e+001 2.523442e+003
7.620738e+001 2.528925e+003
7.717162e+001 2.539183e+003
7.813585e+001 2.558734e+003
7.910008e+001 2.583931e+003
8.006432e+001 2.614758e+003
8.102855e+001 2.652055e+003
8.199278e+001 2.700619e+003
8.295702e+001 2.753801e+003
8.392125e+001 2.797775e+003
8.488548e+001 2.851724e+003
8.584972e+001 2.940482e+003
8.681395e+001 3.032803e+003
8.777818e+001 3.229392e+003
8.874242e+001 3.512856e+003
8.970665e+001 3.895680e+003
9.067088e+001 4.416647e+003
9.163512e+001 5.297301e+003
9.259935e+001 6.164937e+003
9.356358e+001 7.024803e+003
9.452782e+001 7.835734e+003
9.549205e+001 8.378357e+003
9.645628e+001 8.268324e+003
9.742052e+001 7.796116e+003
9.838475e+001 7.088562e+003
9.934898e+001 6.257695e+003
1.003132e+002 5.339088e+003
1.012775e+002 4.628361e+003
1.022417e+002 4.110960e+003
1.032059e+002 3.747631e+003
1.041701e+002 3.473480e+003
1.051344e+002 3.355954e+003
1.060986e+002 3.277674e+003
1.070628e+002 3.247048e+003
1.080271e+002 3.253931e+003
1.089913e+002 3.265061e+003
1.099555e+002 3.266931e+003
1.109198e+002 3.276557e+003
1.118840e+002 3.298330e+003
1.128482e+002 3.334599e+003
1.138125e+002 3.385916e+003
1.147767e+002 3.455154e+003
1.157409e+002 3.532018e+003
1.167052e+002 3.608427e+003
1.176694e+002 3.678630e+003
1.186336e+002 3.755122e+003
1.195979e+002 3.862981e+003
1.205621e+002 3.996347e+003
1.215263e+002 4.150868e+003
1.224906e+002 4.322319e+003
1.234548e+002 4.511204e+003
1.244190e+002 4.744911e+003
1.253833e+002 5.017765e+003
1.263475e+002 5.333843e+003
1.273117e+002 5.712163e+003
1.282760e+002 6.133925e+003
1.292402e+002 6.647624e+003
1.302044e+002 7.262772e+003
1.311687e+002 7.984084e+003
1.321329e+002 8.817262e+003
1.330971e+002 9.852900e+003
1.340614e+002 1.094348e+004
1.350256e+002 1.207045e+004
1.359898e+002 1.322293e+004
1.369541e+002 1.428898e+004
1.379183e+002 1.510689e+004
1.388825e+002 1.567197e+004
1.398468e+002 1.590073e+004
1.408110e+002 1.569220e+004
1.417752e+002 1.488831e+004
1.427395e+002 1.388938e+004
1.437037e+002 1.262299e+004
1.446679e+002 1.121486e+004
1.456322e+002 9.916287e+003
1.465964e+002 8.721050e+003
1.475606e+002 7.658266e+003
1.485249e+002 6.738587e+003
1.494891e+002 5.960562e+003
1.504533e+002 5.297892e+003
1.514176e+002 4.812893e+003
1.523818e+002 4.405708e+003
1.533460e+002 4.060977e+003
1.543103e+002 3.763663e+003
1.552745e+002 3.509900e+003
1.562387e+002 3.298249e+003
1.572030e+002 3.117831e+003
1.581672e+002 2.965242e+003
1.591314e+002 2.837895e+003
1.600957e+002 2.737153e+003
1.610599e+002 2.647813e+003
1.620241e+002 2.570997e+003
1.629884e+002 2.503817e+003
1.639526e+002 2.443164e+003
1.649168e+002 2.393444e+003
1.658811e+002 2.350346e+003
1.668453e+002 2.308575e+003
1.678095e+002 2.269785e+003
1.687738e+002 2.238202e+003
1.697380e+002 2.225892e+003
1.707022e+002 2.215092e+003
1.716665e+002 2.197199e+003
1.726307e+002 2.172781e+003
1.735949e+002 2.147840e+003
1.745592e+002 2.134760e+003
1.755234e+002 2.128473e+003
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1.774519e+002 2.122074e+003
1.784161e+002 2.121359e+003
1.793803e+002 2.130623e+003
1.803446e+002 2.147053e+003
1.813088e+002 2.168671e+003
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1.832373e+002 2.224943e+003
1.842015e+002 2.259486e+003
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1.861300e+002 2.342705e+003
1.870942e+002 2.397314e+003
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1.919154e+002 2.610606e+003
1.928796e+002 2.616563e+003
1.938438e+002 2.603416e+003
1.948081e+002 2.564327e+003
1.957723e+002 2.503936e+003
1.967365e+002 2.431004e+003
1.977008e+002 2.359877e+003
1.986650e+002 2.290063e+003
1.996292e+002 2.226425e+003
2.005935e+002 2.169874e+003
2.015577e+002 2.120049e+003
2.025219e+002 2.076848e+003
2.034862e+002 2.049253e+003
2.044504e+002 2.025337e+003
2.054146e+002 1.995624e+003
2.063788e+002 1.954760e+003
2.073431e+002 1.919042e+003
2.083073e+002 1.904399e+003
2.092715e+002 1.893865e+003
2.102358e+002 1.881772e+003
2.112000e+002 1.866427e+003
2.121642e+002 1.853896e+003
2.131285e+002 1.841251e+003
2.140927e+002 1.829280e+003
2.150569e+002 1.822907e+003
2.160212e+002 1.827498e+003
2.169854e+002 1.842022e+003
2.179496e+002 1.840418e+003
2.189139e+002 1.820968e+003
2.198781e+002 1.796444e+003
2.208423e+002 1.785452e+003
2.218066e+002 1.800835e+003
2.227708e+002 1.808684e+003
2.237350e+002 1.808656e+003
2.246993e+002 1.805944e+003
2.256635e+002 1.808276e+003
2.266277e+002 1.818728e+003
2.275920e+002 1.826090e+003
2.285562e+002 1.828234e+003
2.295204e+002 1.826473e+003
2.304847e+002 1.824094e+003
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2.324131e+002 1.827954e+003
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2.343416e+002 1.822191e+003
2.353058e+002 1.817060e+003
2.362701e+002 1.820572e+003
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2.468766e+002 1.835160e+003
2.478409e+002 1.840404e+003
2.488051e+002 1.842010e+003
2.497693e+002 1.839722e+003
2.507336e+002 1.840803e+003
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2.536263e+002 1.894554e+003
2.545905e+002 1.911259e+003
2.555547e+002 1.922961e+003
2.565190e+002 1.936192e+003
2.574832e+002 1.951911e+003
2.584474e+002 1.972831e+003
2.594117e+002 2.001643e+003
2.603759e+002 2.037513e+003
2.613401e+002 2.078836e+003
2.623044e+002 2.127382e+003
2.632686e+002 2.181821e+003
2.642328e+002 2.238435e+003
2.651971e+002 2.291065e+003
2.661613e+002 2.358699e+003
2.671255e+002 2.440113e+003
2.680898e+002 2.534532e+003
2.690540e+002 2.641475e+003
2.700182e+002 2.762360e+003
2.709825e+002 2.907583e+003
2.719467e+002 3.082313e+003
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2.738752e+002 3.524862e+003
2.748394e+002 3.802315e+003
2.758036e+002 4.120730e+003
2.767679e+002 4.418468e+003
2.777321e+002 4.691827e+003
2.786964e+002 4.939438e+003
2.796606e+002 5.125884e+003
2.806248e+002 5.242746e+003
2.815891e+002 5.308296e+003
2.825533e+002 5.316325e+003
2.835175e+002 5.267401e+003
2.844818e+002 5.177852e+003
2.854460e+002 5.038040e+003
2.864102e+002 4.877353e+003
2.873745e+002 4.698000e+003
2.883387e+002 4.508492e+003
2.893029e+002 4.324274e+003
2.902672e+002 4.158712e+003
2.912314e+002 4.006341e+003
2.921956e+002 3.878555e+003
2.931599e+002 3.781278e+003
2.941241e+002 3.715703e+003
2.950883e+002 3.656730e+003
2.960526e+002 3.602795e+003
2.970168e+002 3.551740e+003
2.979810e+002 3.504228e+003
2.989453e+002 3.461906e+003
2.999095e+002 3.404121e+003
3.008737e+002 3.333333e+003
3.018380e+002 3.256481e+003
3.028022e+002 3.174254e+003
3.037664e+002 3.084733e+003
3.047307e+002 2.994578e+003
3.056949e+002 2.909722e+003
3.066591e+002 2.826525e+003
3.076234e+002 2.740609e+003
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3.095518e+002 2.554461e+003
3.105161e+002 2.465440e+003
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3.124445e+002 2.310208e+003
3.134088e+002 2.254725e+003
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3.153372e+002 2.177957e+003
3.163015e+002 2.123552e+003
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3.191942e+002 2.025887e+003
3.201584e+002 2.004172e+003
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