#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500021.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500021
loop_
_publ_author_name
'El Mendili, Y'
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source
'Graphite blocks from Saint Laurent French reactors'
_chemical_formula_structural     C
_chemical_formula_sum            C
_chemical_name_mineral           Graphite
_chemical_name_systematic        Graphite
_space_group_IT_number           166
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-P 3* 2'
_symmetry_space_group_name_H-M   'R -3 m :R'
_cell_angle_alpha                39.49
_cell_angle_beta                 39.49
_cell_angle_gamma                39.49
_cell_formula_units_Z            2
_cell_length_a                   3.635
_cell_length_b                   3.635
_cell_length_c                   3.635
_cell_volume                     17.5
_raman_determination_method      experimental
_[local]_chemical_compound_color gray
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'IMMM Maine university'
_raman_measurement_device.company 'HORIBA Jobin Yvon'
_raman_measurement_device.model  T64000
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 100
_raman_measurement_device.microscope_numerical_aperture 0.90
_raman_measurement_device.excitation_laser_type Argon-Krypton
_raman_measurement_device.excitation_laser_wavelength 514
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 2
_raman_measurement_device.power_on_sample 2
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 0.8
_raman_measurement_device.diffraction_grating 600
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 60
_raman_measurement.range_min     85.719
_raman_measurement.range_max     2253.98
_rod_data_source.file            Graphite.rod
_rod_data_source.block           1000005
_rod_database.code               3500021
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 Silicon_wafer
2 Diamond
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1200018 COD http://www.crystallography.net/cod/1200018.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
85.719 413
90.5304 357
95.3371 387
100.144 407
104.946 450
109.747 489
114.545 508
119.339 495
124.134 472
128.924 440
133.712 416
138.497 422
143.28 402
148.06 377
152.839 357
157.614 367
162.388 352
167.159 367
171.925 347
176.692 364
181.456 319
186.215 352
190.974 331
195.729 372
200.484 349
205.233 360
209.983 374
214.729 355
219.472 346
224.212 365
228.95 361
233.689 356
238.422 353
243.153 353
247.882 353
252.607 370
257.331 343
262.053 381
266.773 362
271.49 348
276.203 360
280.915 361
285.623 346
290.331 327
295.035 355
299.738 315
304.437 327
309.134 323
313.828 315
318.522 310
323.212 322
327.899 320
332.584 298
337.267 280
341.947 308
346.625 318
351.299 282
355.972 308
360.644 278
365.31 292
369.977 302
374.642 286
379.301 298
383.959 279
388.617 287
393.27 288
397.921 293
402.571 294
407.218 276
411.862 287
416.503 282
421.143 271
425.78 261
430.415 303
435.048 267
439.678 286
444.304 301
448.93 269
453.554 293
458.173 277
462.792 270
467.407 291
472.021 260
476.632 264
481.24 271
485.848 277
490.451 261
495.052 246
499.652 250
504.248 265
508.843 258
513.435 258
518.025 264
522.613 261
527.199 255
531.782 248
536.362 256
540.94 244
545.517 247
550.09 244
554.662 242
559.23 257
563.796 245
568.362 260
572.923 254
577.482 249
582.039 252
586.596 251
591.148 242
595.699 243
600.247 245
604.793 248
609.334 257
613.876 264
618.415 248
622.953 256
627.485 246
632.018 245
636.547 267
641.075 251
645.599 257
650.123 247
654.643 273
659.161 240
663.676 256
668.191 252
672.702 242
677.211 252
681.718 262
686.223 265
690.723 254
695.223 258
699.721 235
704.217 249
708.709 262
713.2 252
717.688 267
722.175 251
726.658 230
731.141 266
735.62 247
740.096 228
744.571 241
749.043 254
753.513 243
757.981 260
762.447 261
766.911 258
771.372 247
775.832 269
780.289 261
784.742 260
789.195 283
793.646 276
798.093 281
802.54 287
806.982 295
811.423 292
815.863 280
820.299 291
824.733 317
829.165 299
833.595 304
838.022 286
842.448 317
846.872 295
851.293 307
855.712 303
860.129 290
864.542 293
868.955 311
873.364 279
877.773 288
882.177 292
886.582 282
890.982 292
895.383 302
899.779 295
904.173 293
908.565 297
912.955 289
917.343 294
921.729 303
926.113 293
930.494 311
934.874 293
939.249 310
943.625 306
947.998 310
952.367 337
956.737 326
961.102 322
965.467 336
969.828 331
974.187 310
978.544 333
982.9 316
987.253 322
991.604 336
995.953 324
1000.3 313
1004.64 360
1008.98 330
1013.32 353
1017.66 350
1022 360
1026.33 367
1030.66 373
1034.99 362
1039.32 391
1043.64 387
1047.97 392
1052.29 438
1056.6 444
1060.92 467
1065.23 473
1069.55 496
1073.86 507
1078.16 507
1082.47 514
1086.77 511
1091.07 504
1095.37 499
1099.67 471
1103.96 479
1108.26 482
1112.55 485
1116.84 504
1121.12 517
1125.41 507
1129.69 506
1133.97 491
1138.25 492
1142.52 501
1146.8 506
1151.07 486
1155.34 486
1159.6 491
1163.87 484
1168.13 510
1172.39 520
1176.65 515
1180.91 542
1185.16 529
1189.42 538
1193.66 543
1197.91 530
1202.16 524
1206.4 531
1210.64 537
1214.88 601
1219.12 579
1223.36 618
1227.59 585
1231.82 631
1236.05 593
1240.28 645
1244.51 662
1248.73 685
1252.95 684
1257.17 728
1261.39 755
1265.6 778
1269.81 807
1274.02 827
1278.23 886
1282.44 963
1286.64 999
1290.85 1058
1295.05 1143
1299.24 1205
1303.44 1408
1307.64 1496
1311.83 1706
1316.02 1877
1320.2 2164
1324.39 2440
1328.57 2796
1332.76 3149
1336.93 3366
1341.11 3644
1345.29 3800
1349.46 3860
1353.63 3711
1357.8 3430
1361.97 3043
1366.14 2709
1370.3 2317
1374.46 2031
1378.62 1801
1382.78 1585
1386.93 1440
1391.08 1265
1395.24 1197
1399.39 1124
1403.53 1072
1407.68 1008
1411.82 951
1415.96 913
1420.1 906
1424.24 868
1428.37 867
1432.5 814
1436.64 836
1440.77 793
1444.89 772
1449.02 779
1453.14 818
1457.26 805
1461.38 797
1465.49 797
1469.61 797
1473.72 779
1477.83 774
1481.94 833
1486.05 800
1490.15 874
1494.26 841
1498.36 885
1502.46 873
1506.55 917
1510.65 946
1514.74 1011
1518.83 1026
1522.92 1072
1527.01 1127
1531.09 1258
1535.17 1351
1539.25 1574
1543.34 1742
1547.41 2124
1551.49 2601
1555.56 3336
1559.63 4363
1563.7 5538
1567.77 6599
1571.83 7084
1575.89 6726
1579.96 5874
1584.01 4896
1588.07 4039
1592.13 3381
1596.18 2799
1600.23 2564
1604.28 2412
1608.33 2310
1612.37 2133
1616.41 1833
1620.46 1542
1624.5 1258
1628.53 1115
1632.57 917
1636.6 837
1640.63 750
1644.66 710
1648.69 666
1652.72 644
1656.74 627
1660.76 548
1664.78 578
1668.8 528
1672.82 542
1676.83 501
1680.84 488
1684.85 483
1688.86 450
1692.87 457
1696.87 450
1700.88 445
1704.88 450
1708.88 424
1712.87 445
1716.87 430
1720.86 421
1724.85 436
1728.84 423
1732.83 427
1736.81 414
1740.79 394
1744.78 403
1748.76 406
1752.73 382
1756.71 387
1760.68 393
1764.65 369
1768.63 374
1772.59 368
1776.56 358
1780.52 349
1784.49 337
1788.45 346
1792.4 350
1796.36 359
1800.31 332
1804.27 338
1808.22 325
1812.17 334
1816.12 341
1820.06 331
1824 333
1827.94 329
1831.88 330
1835.82 335
1839.76 308
1843.69 356
1847.62 343
1851.55 323
1855.48 329
1859.41 335
1863.33 309
1867.26 334
1871.17 318
1875.09 317
1879.01 323
1882.93 314
1886.84 320
1890.75 325
1894.66 329
1898.57 327
1902.47 316
1906.38 325
1910.28 314
1914.18 346
1918.08 308
1921.97 319
1925.87 303
1929.76 283
1933.65 310
1937.54 310
1941.43 320
1945.31 302
1949.2 307
1953.08 342
1956.96 325
1960.84 302
1964.71 312
1968.59 330
1972.46 320
1976.33 320
1980.2 299
1984.06 308
1987.93 312
1991.79 313
1995.66 307
1999.51 301
2003.37 309
2007.23 310
2011.08 297
2014.93 328
2018.78 308
2022.63 312
2026.48 318
2030.32 327
2034.17 293
2038.01 312
2041.85 305
2045.69 325
2049.52 318
2053.35 283
2057.19 280
2061.02 297
2064.84 303
2068.67 289
2072.5 307
2076.32 291
2080.14 292
2083.96 285
2087.78 286
2091.59 276
2095.41 293
2099.22 309
2103.03 309
2106.84 313
2110.65 293
2114.45 289
2118.25 299
2122.06 283
2125.85 305
2129.65 297
2133.45 302
2137.24 296
2141.04 300
2144.83 302
2148.62 271
2152.4 314
2156.19 300
2159.97 300
2163.75 295
2167.53 294
2171.31 316
2175.09 305
2178.86 325
2182.64 299
2186.41 302
2190.17 308
2193.94 318
2197.71 328
2201.47 315
2205.23 314
2209 312
2212.75 283
2216.51 324
2220.27 315
2224.02 329
2227.77 312
2231.52 321
2235.27 320
2239.02 329
2242.76 315
2246.5 334
2250.24 306
2253.98 325