#------------------------------------------------------------------------------
#$Date: 2018-01-23 19:24:51 +0200 (Tue, 23 Jan 2018) $
#$Revision: 364 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500028.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500028
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of gypsum from granite SOLSA sample
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'SOLSA Granite'
_chemical_formula_structural     'Ca H4 O6 S'
_chemical_formula_sum            'Ca H4 O6 S'
_chemical_name_mineral           Gypsum
_chemical_name_systematic        'calcium sulfate dihydrate'
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 151.55
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.47
_cell_length_b                   15.15
_cell_length_c                   6.51
_cell_volume                     491.9
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'IMMM Maine university'
_raman_measurement_device.company 'HORIBA Jobin Yvon'
_raman_measurement_device.model  T64000
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 100
_raman_measurement_device.microscope_numerical_aperture 0.90
_raman_measurement_device.excitation_laser_type Argon-Krypton
_raman_measurement_device.excitation_laser_wavelength 514
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 2
_raman_measurement_device.power_on_sample 2
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 0.8
_raman_measurement_device.diffraction_grating 600
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 120
_raman_measurement.range_min     48.9646
_raman_measurement.range_max     2211.87
_rod_data_source.file            gypsum.rod
_rod_data_source.block           1000000
_rod_database.code               3500028
_solsa_sample.id                 CN-NC00-0004
_raman_measurement.datetime_initiated 2017-01-13
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 Silicon_wafer
2 Diamond
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1010981 COD http://www.crystallography.net/cod/1010981.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
48.9646 153
53.7957 154.5
58.6245 178.75
63.4509 221.5
68.2725 440.25
73.0941 1321.75
77.9109 1954.75
82.7277 2085.8
87.5398 2090.8
92.3517 2093.3
97.159 2109
101.9639 2114.5
106.769 2122
111.569 2131.3
116.367 2344.3
121.162 2853.3
125.955 3100.25
130.746 2873.75
135.534 2308
140.32 2198
145.103 2115.25
149.884 2138
154.663 2143.25
159.437 2155
164.211 2161.25
168.983 2385
173.75 2597.5
178.517 2802.75
183.279 2515.25
188.041 2372
192.799 2225
197.554 2108
202.309 2115.5
207.06 2129.25
211.808 2146
216.554 2161
221.297 2173
226.038 2191.25
230.777 2207.75
235.514 2225
240.248 2244.75
244.98 2271
249.709 2284.5
254.434 2315.75
259.159 2311
263.882 2306
268.6 2353.5
273.317 2335
278.031 2339
282.744 2395
287.453 2348.25
292.159 2306.25
296.865 2356.75
301.567 2308.25
306.266 2291.25
310.964 2306.5
315.658 2307.25
320.351 2352.75
325.041 2357
329.729 2400.5
334.415 2406.75
339.096 2400.25
343.777 2373.5
348.455 2389.5
353.13 2363.5
357.804 2394
362.473 2400.75
367.143 2418.25
371.808 2470.75
376.473 2542.25
381.133 2615.5
385.792 2697.5
390.448 2733
395.103 2792
399.755 3098.75
404.404 3989.5
409.051 6070.75
413.695 6053
418.335 3897.75
422.975 3122.75
427.613 2820
432.249 2703
436.88 2663.25
441.511 2621.75
446.14 2639.75
450.764 2638
455.388 2614.75
460.008 2596.25
464.625 2615.25
469.243 2596.25
473.856 2617.75
478.467 2829
483.075 3271.25
487.682 3625.25
492.286 3637
496.888 3244
501.487 2886
506.085 2699
510.68 2750
515.273 2761.75
519.861 2709
524.45 2674.25
529.036 2716.5
533.618 2754.25
538.199 2817.75
542.777 2950.75
547.354 2878.25
551.927 2870
556.498 2830.75
561.069 2872
565.635 2864.5
570.199 2919
574.761 2871
579.321 2891
583.878 2890
588.434 2915.25
592.987 2902.25
597.538 2942.25
602.084 2904
606.631 2962.75
611.175 3118.75
615.715 3214.75
620.255 3299.25
624.79 3370.5
629.326 3193.5
633.857 3182.75
638.388 3059.5
642.915 3003.5
647.44 2950.25
651.962 2947.25
656.483 2941
661.001 2931.25
665.517 2941.75
670.03 2972.25
674.542 2941.75
679.052 3024.75
683.559 3018.75
688.062 3030
692.565 3091.5
697.066 3112.75
701.562 3204
706.059 3253.25
710.551 3194.25
715.041 3099
719.531 3084.5
724.016 3125
728.5 3077.25
732.981 3114.25
737.461 3164.25
741.938 3171.75
746.413 3195.75
750.886 3210.25
755.356 3231.75
759.825 3248.25
764.291 3284.75
768.754 3303.25
773.216 3322.75
777.676 3343
782.131 3425
786.587 3466.5
791.039 3484.5
795.488 3521
799.938 3592.5
804.383 3600.5
808.826 3616.25
813.267 3631.5
817.705 3658.75
822.142 3674
826.577 3591.25
831.009 3560.25
835.44 3724.75
839.868 3784.5
844.294 3718.75
848.716 3762.75
853.138 3718
857.557 3612.5
861.973 3676
866.389 3627.25
870.8 3679
875.209 3678.5
879.619 3621
884.024 3642.25
888.427 3660.75
892.828 3611.5
897.227 3713.75
901.623 3791.75
906.018 3795.5
910.411 3782
914.801 3735.5
919.19 3749
923.576 3631.75
927.958 3654.75
932.341 3595.5
936.721 3600.25
941.097 3623
945.473 3677.75
949.844 3637.5
954.214 3653.5
958.584 3680.25
962.95 3704
967.313 3794.75
971.675 3823.5
976.034 3924
980.392 4135.5
984.747 4483.25
989.1 5291
993.451 6590.75
997.799 12272.5
1002.146 23814
1006.49 19535.5
1010.83 7683.25
1015.17 4075
1019.51 3815.25
1023.85 3783
1028.18 3729.5
1032.51 3796.25
1036.84 3706.5
1041.17 3724
1045.49 3711.75
1049.81 3708.25
1054.14 3696.75
1058.45 3730.5
1062.77 3779.75
1067.08 3834.5
1071.4 3877.25
1075.71 3865.5
1080.01 3766
1084.32 3729
1088.62 3688.75
1092.92 3712.25
1097.22 3685
1100.4 3942.75
1104.69 3916
1108.97 3848.5
1113.26 3789.5
1117.54 3795.5
1121.82 3840.5
1126.1 3969.75
1130.37 4171.25
1134.64 4573.75
1138.92 5453
1143.19 6043
1147.45 5440.75
1151.72 4828.5
1155.98 4713.75
1160.24 3979.5
1164.5 3855.75
1168.76 3780.25
1173.01 3804
1177.27 3731.75
1181.52 3808.75
1185.76 3735
1190.01 3795.5
1194.25 3801
1198.5 3807
1202.74 3810
1206.97 3789.5
1211.21 3792.75
1215.44 3844.75
1219.68 3821.5
1223.9 3963
1228.13 3900
1232.36 3934
1236.58 3866
1240.8 3904.5
1245.02 3872
1249.24 3856
1253.45 3877
1257.67 3858.5
1261.87 3907.5
1266.08 3940
1270.29 3942.25
1274.5 3990.25
1278.7 3996
1282.9 3971.25
1287.1 4008
1291.29 4021.75
1295.49 4057.75
1299.68 4081.5
1303.87 4089
1308.06 4139.5
1312.24 4155.25
1316.43 4164.75
1320.61 4166.5
1324.79 4117.5
1328.97 4125.75
1333.14 4198.25
1337.32 4225
1341.49 4172.5
1345.66 4135.75
1349.82 4154
1353.99 4140
1358.15 4169
1362.31 4111.25
1366.47 4114.75
1370.63 4118
1374.78 4174
1378.94 4119
1383.09 4165.25
1387.24 4123.75
1391.38 4204.75
1395.53 4138.5
1399.67 4146.5
1403.81 4167.5
1407.95 4137.75
1412.09 4135.75
1416.23 4128.25
1420.36 4201.25
1424.49 4239.75
1428.62 4221
1432.75 4280.5
1436.87 4238.5
1440.99 4201.75
1445.11 4281.75
1449.23 4214.75
1453.35 4257
1457.46 4295
1461.58 4254.25
1465.69 4241
1469.8 4281.25
1473.9 4233.75
1478.01 4284.25
1482.11 4297.5
1486.21 4317
1490.31 4227.25
1494.41 4220.25
1498.5 4270.5
1502.59 4253.25
1506.69 4293.75
1510.77 4306.5
1514.86 4322
1518.95 4383.75
1523.03 4330.75
1527.11 4380
1531.19 4425.25
1535.26 4377.75
1539.34 4445.5
1543.41 4438.75
1547.48 4518
1551.55 4500.5
1555.62 4608.25
1559.68 4789
1563.75 5333.5
1567.81 6264
1571.87 6320
1575.92 5587.75
1579.98 6121
1584.03 7980.5
1588.08 9917.5
1592.13 8723
1596.18 6327.25
1600.23 5212.5
1604.27 4858.75
1608.31 4744.5
1612.35 4708.5
1616.39 4606.75
1620.42 4591.25
1624.46 4626.25
1628.49 4571
1632.52 4558
1636.55 4561.25
1640.57 4570.5
1644.59 4569.5
1648.62 4539.5
1652.64 4612.5
1656.65 4610.25
1660.67 4585.75
1664.68 4623.5
1668.7 4672.75
1672.71 4655.75
1676.72 4638
1680.72 4620
1684.73 4694
1688.73 4618.75
1692.73 4656
1696.73 4679.75
1700.72 4699.75
1704.72 4650.5
1708.71 4638.25
1712.7 4697.25
1716.69 4836.75
1720.68 4757
1724.67 4728.25
1728.65 4695
1732.63 4738
1736.61 4689
1740.59 4708
1744.56 4718
1748.54 4736.5
1752.51 4737
1756.48 4753.25
1760.45 4706
1764.41 4763
1768.38 4780.25
1772.34 4750.5
1776.3 4732.25
1780.26 4738
1784.21 4756.25
1788.17 4800.25
1792.12 4747.25
1796.07 4797
1800.02 4792.75
1803.97 4804.25
1807.91 4770.25
1811.86 4729.5
1815.8 4775.5
1819.74 4745.5
1823.67 4715.25
1827.61 4735.5
1831.54 4717
1835.48 4723.75
1839.41 4675.25
1843.33 4720.5
1847.26 4683.25
1851.18 4710.75
1855.11 4700.75
1859.03 4720.5
1862.95 4725
1866.86 4736.25
1870.78 4733
1874.69 4654.5
1878.6 4647.25
1882.51 4738.25
1886.42 4696
1890.33 4686.5
1894.23 4685.5
1898.13 4722.25
1902.03 4694.75
1905.93 4757.75
1909.83 4754
1913.72 4745.75
1917.61 4735.75
1921.5 4744.5
1925.39 4759.5
1929.28 4790
1933.17 4723.75
1937.05 4758.25
1940.93 4776
1944.81 4716.25
1948.69 4783
1952.56 4755.5
1956.44 4741.5
1960.31 4751.75
1964.18 4744
1968.05 4736
1971.92 4781.25
1975.78 4757.5
1979.65 4781
1983.51 4748.25
1987.37 4726.25
1991.22 4725.75
1995.08 4710.5
1998.93 4707
2002.79 4701.25
2006.64 4695.25
2010.48 4720
2014.33 4666.5
2018.18 4691.25
2022.02 4660
2025.86 4693.25
2029.7 4708.75
2033.54 4678.5
2037.37 4705.5
2041.21 4703.5
2045.04 4716.5
2048.87 4677.75
2052.7 4674.75
2056.52 4701.75
2060.35 4735.5
2064.17 4698
2067.99 4684
2071.81 4696.25
2075.63 4703
2079.44 4708.75
2083.26 4713.25
2087.07 4709.5
2090.88 4717.25
2094.69 4697.75
2098.5 4717.75
2102.3 4719.5
2106.11 4721.25
2109.91 4753.5
2113.71 4773.75
2117.5 4753.5
2121.3 4752.25
2125.09 4741.75
2128.89 4787.25
2132.68 4730
2136.47 4770.5
2140.25 4737.5
2144.04 4749.5
2147.82 4724.25
2151.6 4775.25
2155.38 4777
2159.16 4700
2162.94 4729.25
2166.71 4792.5
2170.49 4719
2174.26 4775.75
2178.03 4795.5
2181.79 4722
2185.56 4766.5
2189.32 4781.25
2193.08 4816.75
2196.85 4767
2200.6 4825.5
2204.36 4776.75
2208.12 4760
2211.87 4852.75
