#------------------------------------------------------------------------------ #$Date: 2017-10-10 13:48:59 +0300 (Tue, 10 Oct 2017) $ #$Revision: 252 $ #$URL: svn://172.16.1.111/rod/cif/3/50/00/3500033.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500033 loop_ _publ_author_name 'El Mendili, Y' _publ_section_title ; Raman spectrum of goethite from granite SOLSA sample ; _journal_name_full 'Personal communication to ROD' _journal_year 2017 _chemical_compound_source 'SOLSA Tiebaghi HSA' _chemical_formula_structural 'Fe H O2' _chemical_formula_sum 'Fe H O2' _chemical_name_mineral Goethite _chemical_name_systematic Goethite _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 9.9134 _cell_length_b 3.0128 _cell_length_c 4.5800 _cell_volume 136.791 _raman_determination_method experimental _[local]_chemical_compound_color black _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.name DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 3 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 100 _raman_measurement.range_min 49.93432 _raman_measurement.range_max 2500.051 _rod_data_source.file Goethite.rod _rod_data_source.block 1000000 _rod_database.code 3500033 _solsa_sample.id CN-MB00-0001 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9002158 COD http://www.crystallography.net/cod/9002158.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 49.93432 12.66544 50.89856 11.7534 51.86279 11.43827 52.82702 11.17796 53.79126 10.54317 54.75549 9.33521 55.71972 8.76844 56.68396 9.12238 57.64819 9.93595 58.61242 10.50398 59.57666 10.62245 60.54089 10.34402 61.50512 9.58378 62.46936 8.4801 63.43359 7.46341 64.39782 6.62057 65.36205 6.09263 66.32629 5.91954 67.29052 6.11792 68.25475 6.75757 69.21899 8.30204 70.18322 10.27786 71.14745 11.96602 72.11169 12.53255 73.07592 11.50532 74.04015 10.98268 75.00439 10.99694 75.96862 11.4477 76.93285 12.05898 77.89709 12.70636 78.86132 14.51965 79.82555 17.26867 80.78979 20.88801 81.75402 26.46911 82.71825 33.43239 83.68249 42.68211 84.64672 55.63499 85.61095 73.33352 86.57519 92.92822 87.53942 114.344 88.50365 134.2583 89.46789 148.2489 90.43212 150.1075 91.39635 138.0898 92.36059 121.7593 93.32482 100.2668 94.28905 75.19611 95.25329 55.00814 96.21752 41.46434 97.18176 30.44403 98.14599 21.81697 99.11022 15.80805 100.0745 11.41947 101.0387 8.8959 102.0029 7.4536 102.9672 6.77899 103.9314 6.65469 104.8956 6.6569 105.8599 6.56139 106.8241 6.42889 107.7883 6.39327 108.7526 6.72415 109.7168 7.39546 110.681 7.74851 111.6453 7.71822 112.6095 7.31362 113.5737 6.61017 114.5379 5.28413 115.5022 3.92846 116.4664 2.58006 117.4306 1.22851 118.3949 0.26596 119.3591 -0.00904 120.3233 -0.06667 121.2876 -0.11172 122.2518 -0.25815 123.216 -0.52323 124.1803 -0.89635 125.1445 -1.28643 126.1087 -1.58779 127.073 -1.65637 128.0372 -1.52053 129.0014 -1.34838 129.9657 -1.18669 130.9299 -1.16195 131.8941 -1.65573 132.8584 -3.0193 133.8226 -4.00658 134.7868 -4.24781 135.7511 -3.70723 136.7153 -3.25618 137.6796 -2.58945 138.6438 -2.01246 139.608 -1.75204 140.5723 -1.96676 141.5365 -2.2597 142.5007 -2.81717 143.465 -3.31707 144.4292 -3.35573 145.3934 -2.46174 146.3577 -1.02542 147.3219 0.00607 148.2861 0.55205 149.2504 0.53078 150.2146 -0.17542 151.1788 -1.54624 152.1431 -2.2406 153.1073 -1.99236 154.0715 -1.00054 155.0358 -0.31581 156 -0.8635 156.9642 -0.90875 157.9285 0.25612 158.8927 2.71713 159.8569 4.91152 160.8212 6.08969 161.7854 6.63175 162.7496 6.6503 163.7139 6.23893 164.6781 5.46686 165.6423 4.22422 166.6066 2.81384 167.5708 1.55891 168.535 0.77793 169.4993 0.55443 170.4635 0.59587 171.4277 0.94642 172.392 1.44101 173.3562 1.77295 174.3204 1.69977 175.2847 1.6303 176.2489 1.54125 177.2131 1.42434 178.1774 1.28268 179.1416 0.86491 180.1058 0.60816 181.0701 0.83295 182.0343 1.58726 182.9985 2.58498 183.9628 3.56713 184.927 4.31694 185.8912 4.46561 186.8555 3.85999 187.8197 2.6953 188.7839 2.54251 189.7482 3.32928 190.7124 4.44251 191.6766 5.34994 192.6409 5.7832 193.6051 5.95953 194.5693 5.77665 195.5336 5.79941 196.4978 6.6604 197.462 9.09751 198.4263 11.32767 199.3905 12.3324 200.3547 12.77645 201.319 13.84345 202.2832 17.84818 203.2474 21.61519 204.2117 22.41665 205.1759 20.45714 206.1401 16.98899 207.1044 14.74181 208.0686 13.48949 209.0328 12.42568 209.9971 11.35661 210.9613 10.33172 211.9255 9.99428 212.8898 10.86566 213.854 11.88165 214.8182 12.61941 215.7825 12.905 216.7467 13.0789 217.7109 13.64042 218.6752 14.09482 219.6394 14.03196 220.6036 13.19652 221.5679 12.60098 222.5321 13.26589 223.4963 14.42695 224.4606 15.3776 225.4248 15.4635 226.389 14.78168 227.3533 14.55473 228.3175 14.88125 229.2817 15.69269 230.246 16.83893 231.2102 18.40382 232.1744 20.43444 233.1387 22.76552 234.1029 25.25729 235.0671 27.76441 236.0314 30.48848 236.9956 33.20905 237.9598 36.16216 238.9241 39.11455 239.8883 41.6109 240.8525 43.2397 241.8168 43.92136 242.781 43.40674 243.7452 41.84059 244.7095 39.63736 245.6737 37.71883 246.6379 35.9726 247.6022 34.28089 248.5664 32.59871 249.5306 30.95392 250.4949 29.69467 251.4591 28.89042 252.4233 27.92044 253.3876 26.61927 254.3518 25.01089 255.316 23.23305 256.2802 21.18835 257.2445 19.47487 258.2087 18.31851 259.1729 17.75694 260.1372 17.62307 261.1014 17.96 262.0656 18.36465 263.0299 18.47615 263.9941 18.02858 264.9583 17.21693 265.9226 16.76636 266.8868 16.63017 267.851 16.75217 268.8153 17.08314 269.7795 17.73748 270.7437 18.29247 271.708 18.78648 272.6722 19.13032 273.6364 19.1406 274.6007 18.3143 275.5649 18.02164 276.5291 18.87645 277.4934 20.40625 278.4576 21.92719 279.4218 22.64768 280.3861 23.32329 281.3503 24.91415 282.3145 27.30532 283.2788 29.9207 284.243 31.53581 285.2072 31.99397 286.1715 33.73637 287.1357 37.07261 288.0999 41.68136 289.0642 46.54251 290.0284 51.69542 290.9926 57.98824 291.9569 65.9329 292.9211 75.28516 293.8853 84.83461 294.8496 96.04069 295.8138 104.525 296.778 108.9884 297.7423 109.2576 298.7065 106.2568 299.6707 99.11604 300.635 90.33989 301.5992 81.87183 302.5634 74.42363 303.5277 67.88808 304.4919 61.79946 305.4561 55.86005 306.4204 51.23288 307.3846 48.70295 308.3488 48.34423 309.3131 47.2429 310.2773 45.24236 311.2415 43.13131 312.2058 41.04601 313.17 39.03559 314.1342 37.37231 315.0985 36.1087 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973.6699 22.45744 974.6341 22.62316 975.5983 21.63906 976.5626 20.84568 977.5268 20.57133 978.491 20.56083 979.4553 20.65931 980.4195 20.90818 981.3837 21.41491 982.348 22.08741 983.3122 22.90612 984.2764 24.50517 985.2407 26.87975 986.2049 28.74551 987.1691 29.3592 988.1334 29.12138 989.0976 29.09141 990.0618 28.9854 991.0261 29.33481 991.9903 30.91753 992.9545 32.30699 993.9188 32.46873 994.883 31.6247 995.8472 30.85221 996.8115 30.86502 997.7757 31.17537 998.7399 30.71799 999.7042 29.84138 1000.668 29.52038 1001.633 30.10616 1002.597 30.94032 1003.561 30.90803 1004.525 29.84557 1005.49 28.83296 1006.454 27.51958 1007.418 26.38461 1008.382 25.83487 1009.346 25.60263 1010.311 25.18427 1011.275 24.40862 1012.239 23.48325 1013.203 22.61966 1014.168 21.89466 1015.132 21.15462 1016.096 20.35835 1017.06 19.68244 1018.025 19.3355 1018.989 19.27977 1019.953 19.04928 1020.917 18.53084 1021.882 17.97042 1022.846 17.38437 1023.81 16.84026 1024.774 16.36148 1025.738 15.93917 1026.703 15.60319 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1461.572 17.79672 1462.536 17.09507 1463.5 17.13179 1464.465 17.71278 1465.429 17.91571 1466.393 17.58127 1467.357 17.00831 1468.322 15.89468 1469.286 15.00412 1470.25 15.96545 1471.214 17.9822 1472.178 18.83548 1473.143 18.13088 1474.107 17.52489 1475.071 18.42637 1476.035 19.92478 1477 20.24729 1477.964 19.39195 1478.928 18.35506 1479.892 17.11673 1480.857 16.19204 1481.821 15.85395 1482.785 15.9877 1483.749 16.79761 1484.714 17.80302 1485.678 18.13086 1486.642 17.59709 1487.606 16.87114 1488.57 16.58329 1489.535 16.66415 1490.499 16.77263 1491.463 16.83125 1492.427 16.86669 1493.392 17.28865 1494.356 17.51682 1495.32 16.96009 1496.284 16.4671 1497.249 16.82993 1498.213 17.50812 1499.177 17.38581 1500.141 16.31467 1501.105 15.38344 1502.07 15.57717 1503.034 16.57135 1503.998 17.37136 1504.962 17.98047 1505.927 18.0446 1506.891 17.01306 1507.855 16.16089 1508.819 15.72704 1509.784 15.76291 1510.748 16.62329 1511.712 17.83051 1512.676 18.40024 1513.641 18.11736 1514.605 17.5324 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