#------------------------------------------------------------------------------
#$Date: 2017-11-07 14:10:34 +0200 (Tue, 07 Nov 2017) $
#$Revision: 294 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500051.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500051
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial GeO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Alfa Aesar 99.99%'
_chemical_formula_structural     'Ge O2'
_chemical_formula_sum            'Ge O2'
_chemical_name_mineral           Argutite
_chemical_name_systematic        'Germanium dioxide'
_space_group_IT_number           199
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-P 4n 2n'
_symmetry_space_group_name_H-M   'P 42/m n m'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   4.40656(5)
_cell_length_b                   4.40656(5)
_cell_length_c                   2.86186(3)
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2999.762
_rod_data_source.file            GeO2.rod
_rod_data_source.block           1000005
_rod_database.code               3500051
_solsa_sample.id                 CN-AA00-0040
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 2101851 COD http://www.crystallography.net/cod/2101851.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 1.505518e+000
5.113732e+001 2.829639e+000
5.210155e+001 2.241748e+000
5.306579e+001 7.480469e-001
5.403002e+001 -6.402344e-001
5.499426e+001 -8.340820e-001
5.595849e+001 -2.347168e-001
5.692272e+001 1.408740e+000
5.788695e+001 3.802539e+000
5.885118e+001 6.332373e+000
5.981542e+001 6.517090e+000
6.077965e+001 4.779053e+000
6.174389e+001 2.394336e+000
6.270812e+001 -7.958984e-003
6.367235e+001 -2.211768e+000
6.463658e+001 -3.609180e+000
6.560081e+001 -3.940039e+000
6.656505e+001 -3.345020e+000
6.752928e+001 -2.111035e+000
6.849352e+001 -8.674805e-001
6.945775e+001 2.076172e-001
7.042198e+001 1.038867e+000
7.138622e+001 1.634863e+000
7.235045e+001 2.146484e+000
7.331468e+001 4.673340e+000
7.427892e+001 6.643945e+000
7.524315e+001 6.331103e+000
7.620738e+001 3.612549e+000
7.717162e+001 -7.280274e-002
7.813585e+001 -1.961133e+000
7.910008e+001 -2.937793e+000
8.006432e+001 -3.241943e+000
8.102855e+001 -2.928760e+000
8.199278e+001 -1.343359e+000
8.295702e+001 5.875977e-001
8.392125e+001 2.211279e+000
8.488548e+001 3.201074e+000
8.584972e+001 3.292236e+000
8.681395e+001 1.821045e+000
8.777818e+001 4.809570e-001
8.874242e+001 -5.292969e-001
8.970665e+001 -9.204590e-001
9.067088e+001 -2.805176e-001
9.163512e+001 2.193408e+000
9.259935e+001 4.343554e+000
9.356358e+001 5.542188e+000
9.452781e+001 5.782959e+000
9.549204e+001 6.286572e+000
9.645628e+001 9.023974e+000
9.742051e+001 1.202402e+001
9.838474e+001 1.344653e+001
9.934898e+001 1.178418e+001
1.003132e+002 7.180860e+000
1.012774e+002 4.471924e+000
1.022417e+002 3.656543e+000
1.032059e+002 5.066358e+000
1.041701e+002 9.242432e+000
1.051344e+002 2.215869e+001
1.060986e+002 3.117734e+001
1.070628e+002 3.296802e+001
1.080271e+002 2.933560e+001
1.089913e+002 2.849795e+001
1.099555e+002 3.173706e+001
1.109198e+002 3.924663e+001
1.118840e+002 4.759101e+001
1.128482e+002 5.710806e+001
1.138125e+002 8.065166e+001
1.147767e+002 9.637740e+001
1.157409e+002 1.437035e+002
1.167052e+002 2.594429e+002
1.176694e+002 4.719046e+002
1.186336e+002 7.780544e+002
1.195979e+002 1.155509e+003
1.205621e+002 1.584048e+003
1.215263e+002 1.964623e+003
1.224906e+002 2.153862e+003
1.234548e+002 2.060787e+003
1.244190e+002 1.860732e+003
1.253833e+002 1.473687e+003
1.263475e+002 9.646149e+002
1.273117e+002 5.646989e+002
1.282760e+002 3.662025e+002
1.292402e+002 2.262632e+002
1.302044e+002 1.394835e+002
1.311687e+002 9.752676e+001
1.321329e+002 7.470537e+001
1.330971e+002 5.961948e+001
1.340614e+002 4.789561e+001
1.350256e+002 3.781069e+001
1.359898e+002 2.829961e+001
1.369541e+002 2.114702e+001
1.379183e+002 1.880913e+001
1.388825e+002 1.963223e+001
1.398468e+002 2.189375e+001
1.408110e+002 2.373403e+001
1.417752e+002 2.473809e+001
1.427395e+002 2.532603e+001
1.437037e+002 2.557739e+001
1.446679e+002 2.612803e+001
1.456322e+002 2.802720e+001
1.465964e+002 3.381475e+001
1.475606e+002 3.754018e+001
1.485249e+002 3.679541e+001
1.494891e+002 3.260161e+001
1.504533e+002 3.007803e+001
1.514176e+002 3.390596e+001
1.523818e+002 4.074805e+001
1.533460e+002 4.857061e+001
1.543103e+002 5.688745e+001
1.552745e+002 6.830508e+001
1.562387e+002 7.595156e+001
1.572030e+002 9.121299e+001
1.581672e+002 1.213392e+002
1.591314e+002 1.722350e+002
1.600957e+002 2.514626e+002
1.610599e+002 4.754646e+002
1.620241e+002 8.652838e+002
1.629884e+002 1.314018e+003
1.639526e+002 1.712879e+003
1.649168e+002 2.157549e+003
1.658811e+002 2.349632e+003
1.668453e+002 2.205706e+003
1.678095e+002 1.835366e+003
1.687738e+002 1.422272e+003
1.697380e+002 9.548924e+002
1.707022e+002 5.660542e+002
1.716665e+002 3.081274e+002
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1.755234e+002 5.389561e+001
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1.784161e+002 2.727471e+001
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1.890226e+002 1.189653e+001
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1.919153e+002 8.203028e+000
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1.957723e+002 1.444775e+000
1.967365e+002 -1.566943e+000
1.977007e+002 -9.332520e-001
1.986650e+002 3.206982e+000
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2.005934e+002 6.585156e+000
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2.034861e+002 1.332070e+001
2.044504e+002 2.498770e+001
2.054146e+002 4.019653e+001
2.063788e+002 5.798730e+001
2.073431e+002 8.558018e+001
2.083073e+002 1.365233e+002
2.092715e+002 1.885769e+002
2.102358e+002 2.354446e+002
2.112000e+002 2.739443e+002
2.121642e+002 2.954257e+002
2.131285e+002 2.871742e+002
2.140927e+002 2.591264e+002
2.150569e+002 2.175902e+002
2.160212e+002 1.685280e+002
2.169854e+002 1.143215e+002
2.179496e+002 7.455083e+001
2.189139e+002 4.888828e+001
2.198781e+002 3.354775e+001
2.208423e+002 2.352949e+001
2.218066e+002 2.250933e+001
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2.304847e+002 1.039170e+001
2.314489e+002 9.926270e+000
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2.333774e+002 1.134478e+001
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2.459124e+002 2.368755e+002
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2.488051e+002 2.436353e+002
2.497693e+002 2.072726e+002
2.507336e+002 1.689141e+002
2.516978e+002 1.493070e+002
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2.536263e+002 1.530901e+002
2.545905e+002 1.718060e+002
2.555547e+002 2.031947e+002
2.565190e+002 2.477702e+002
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2.584474e+002 3.732913e+002
2.594117e+002 4.476613e+002
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2.700182e+002 2.404541e+002
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2.738752e+002 9.038545e+001
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2.767679e+002 4.758716e+001
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2.786963e+002 3.020273e+001
2.796606e+002 2.465049e+001
2.806248e+002 2.348237e+001
2.815890e+002 2.271577e+001
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2.883387e+002 1.233120e+001
2.893029e+002 9.449366e+000
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2.912314e+002 1.158115e+001
2.921956e+002 1.307129e+001
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2.950883e+002 1.391611e+001
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loop_
_rod_maintainer_comment.id
_rod_maintainer_comment.author
_rod_maintainer_comment.date
_rod_maintainer_comment.text
1 elmendili 2017-10-06T15:58:03+0300 'Mineral name changed'