#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500061.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500061
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial NaBH4
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Prolabo 99%'
_chemical_formula_structural     'Na (B H4)'
_chemical_formula_sum            'B H4 Na'
_chemical_name_mineral           'Sodium borohydride'
_chemical_name_systematic        'Sodium borohydride'
_space_group_IT_number           225
_symmetry_space_group_name_Hall  '-F 4 2 3'
_symmetry_space_group_name_H-M   'F m -3 m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.1635
_cell_length_b                   6.1635
_cell_length_c                   6.1635
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     21.24609
_raman_measurement.range_max     2999.762
_rod_data_source.file            NaBH4.rod
_rod_data_source.block           1000005
_rod_database.code               3500061
_solsa_sample.id                 CN-AA00-0050
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1541413 COD http://www.crystallography.net/cod/1541413.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
2.124609e+001 2.202749e+002
2.221033e+001 2.191894e+002
2.317456e+001 2.179846e+002
2.413879e+001 2.160712e+002
2.510303e+001 2.185828e+002
2.606726e+001 2.265529e+002
2.703149e+001 2.387798e+002
2.799573e+001 2.514206e+002
2.895996e+001 2.581016e+002
2.992419e+001 2.719577e+002
3.088842e+001 2.981424e+002
3.185266e+001 3.377044e+002
3.281689e+001 3.783349e+002
3.378112e+001 4.111802e+002
3.474536e+001 4.434761e+002
3.570959e+001 4.803289e+002
3.667382e+001 5.262281e+002
3.763805e+001 5.010176e+002
3.860229e+001 4.724211e+002
3.956652e+001 4.434739e+002
4.053075e+001 4.189889e+002
4.149499e+001 4.103166e+002
4.245922e+001 4.166915e+002
4.342345e+001 4.223509e+002
4.438769e+001 4.241953e+002
4.535192e+001 4.225984e+002
4.631615e+001 4.340392e+002
4.728039e+001 4.565622e+002
4.824462e+001 4.852206e+002
4.920885e+001 5.175662e+002
5.017309e+001 5.526490e+002
5.113732e+001 5.945917e+002
5.210155e+001 6.361992e+002
5.306579e+001 6.840993e+002
5.403002e+001 7.462909e+002
5.499425e+001 8.375410e+002
5.595848e+001 9.381914e+002
5.692272e+001 1.044586e+003
5.788695e+001 1.150615e+003
5.885118e+001 1.248341e+003
5.981542e+001 1.314522e+003
6.077965e+001 1.352074e+003
6.174389e+001 1.355179e+003
6.270812e+001 1.319359e+003
6.367235e+001 1.240117e+003
6.463658e+001 1.163857e+003
6.560081e+001 1.092115e+003
6.656505e+001 1.022480e+003
6.752928e+001 9.518019e+002
6.849352e+001 8.748000e+002
6.945775e+001 7.993156e+002
7.042198e+001 7.217413e+002
7.138622e+001 6.464855e+002
7.235045e+001 5.800548e+002
7.331468e+001 5.332374e+002
7.427892e+001 4.965452e+002
7.524315e+001 4.677126e+002
7.620738e+001 4.456384e+002
7.717162e+001 4.300340e+002
7.813585e+001 4.232255e+002
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8.006432e+001 4.222795e+002
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8.681394e+001 4.153680e+002
8.777818e+001 4.042176e+002
8.874241e+001 3.897801e+002
8.970664e+001 3.738397e+002
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9.645628e+001 3.376325e+002
9.742051e+001 3.409915e+002
9.838474e+001 3.438645e+002
9.934898e+001 3.443268e+002
1.003132e+002 3.425959e+002
1.012774e+002 3.444436e+002
1.022417e+002 3.502095e+002
1.032059e+002 3.573560e+002
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1.051344e+002 3.636517e+002
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1.080271e+002 3.500285e+002
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1.118840e+002 3.215007e+002
1.128482e+002 3.194404e+002
1.138125e+002 3.176474e+002
1.147767e+002 3.126037e+002
1.157409e+002 3.065221e+002
1.167052e+002 3.012381e+002
1.176694e+002 2.982757e+002
1.186336e+002 2.971505e+002
1.195979e+002 2.937874e+002
1.205621e+002 2.883419e+002
1.215263e+002 2.825146e+002
1.224906e+002 2.789204e+002
1.234548e+002 2.790976e+002
1.244190e+002 2.811525e+002
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1.263475e+002 2.931790e+002
1.273117e+002 2.998255e+002
1.282760e+002 3.049983e+002
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1.302044e+002 3.127751e+002
1.311687e+002 3.149367e+002
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1.350256e+002 3.356393e+002
1.359898e+002 3.318942e+002
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1.832373e+002 2.764831e+002
1.842015e+002 2.736346e+002
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1.861300e+002 2.682005e+002
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1.880584e+002 2.730943e+002
1.890227e+002 2.767602e+002
1.899869e+002 2.782937e+002
1.909511e+002 2.778678e+002
1.919154e+002 2.752265e+002
1.928796e+002 2.683421e+002
1.938438e+002 2.612120e+002
1.948080e+002 2.602648e+002
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