#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500065.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500065
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial NbO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Alfa Aesar 99%'
_chemical_formula_structural     'Nb O2'
_chemical_formula_sum            'Nb O2'
_chemical_name_mineral           'Niobium dioxide'
_chemical_name_systematic        'Niobium dioxide'
_space_group_IT_number           88
_symmetry_space_group_name_Hall  '-I 4ad'
_symmetry_space_group_name_H-M   'I 41/a :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            32
_cell_length_a                   13.698
_cell_length_b                   13.698
_cell_length_c                   5.976
_raman_determination_method      experimental
_[local]_chemical_compound_color black
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2248.589
_rod_data_source.file            NbO2.rod
_rod_data_source.block           1000005
_rod_database.code               3500065
_solsa_sample.id                 CN-AA00-0054
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1520791 COD http://www.crystallography.net/cod/1520791.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 1.561054e+004
5.113732e+001 1.569288e+004
5.210155e+001 1.574293e+004
5.306579e+001 1.577082e+004
5.403002e+001 1.579092e+004
5.499426e+001 1.582911e+004
5.595849e+001 1.585725e+004
5.692272e+001 1.585954e+004
5.788696e+001 1.583919e+004
5.885119e+001 1.580646e+004
5.981542e+001 1.577737e+004
6.077965e+001 1.572982e+004
6.174389e+001 1.564334e+004
6.270812e+001 1.550977e+004
6.367235e+001 1.533001e+004
6.463658e+001 1.516967e+004
6.560081e+001 1.503680e+004
6.656505e+001 1.492841e+004
6.752928e+001 1.483663e+004
6.849352e+001 1.474205e+004
6.945775e+001 1.463666e+004
7.042198e+001 1.451967e+004
7.138622e+001 1.439153e+004
7.235045e+001 1.425360e+004
7.331468e+001 1.412482e+004
7.427892e+001 1.401066e+004
7.524315e+001 1.390552e+004
7.620738e+001 1.380738e+004
7.717162e+001 1.371669e+004
7.813585e+001 1.364960e+004
7.910008e+001 1.358368e+004
8.006432e+001 1.349832e+004
8.102855e+001 1.338239e+004
8.199278e+001 1.325057e+004
8.295702e+001 1.317379e+004
8.392125e+001 1.313528e+004
8.488548e+001 1.310765e+004
8.584972e+001 1.305874e+004
8.681395e+001 1.297513e+004
8.777818e+001 1.289361e+004
8.874242e+001 1.282609e+004
8.970665e+001 1.277477e+004
9.067088e+001 1.273386e+004
9.163512e+001 1.268117e+004
9.259935e+001 1.262943e+004
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9.549205e+001 1.256080e+004
9.645628e+001 1.254306e+004
9.742052e+001 1.252012e+004
9.838475e+001 1.249989e+004
9.934898e+001 1.248901e+004
1.003132e+002 1.248295e+004
1.012775e+002 1.247889e+004
1.022417e+002 1.248338e+004
1.032059e+002 1.249622e+004
1.041701e+002 1.251417e+004
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1.070628e+002 1.271001e+004
1.080271e+002 1.283258e+004
1.089913e+002 1.296781e+004
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1.138125e+002 1.379058e+004
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1.157409e+002 1.412113e+004
1.167052e+002 1.426438e+004
1.176694e+002 1.439096e+004
1.186336e+002 1.450213e+004
1.195979e+002 1.459334e+004
1.205621e+002 1.465928e+004
1.215263e+002 1.469603e+004
1.224906e+002 1.470183e+004
1.234548e+002 1.468485e+004
1.244190e+002 1.462910e+004
1.253833e+002 1.453382e+004
1.263475e+002 1.440344e+004
1.273117e+002 1.424771e+004
1.282760e+002 1.402974e+004
1.292402e+002 1.379648e+004
1.302044e+002 1.354513e+004
1.311687e+002 1.327759e+004
1.321329e+002 1.301255e+004
1.330971e+002 1.276313e+004
1.340614e+002 1.252665e+004
1.350256e+002 1.230964e+004
1.359898e+002 1.211713e+004
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1.388825e+002 1.170134e+004
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1.408110e+002 1.145384e+004
1.417752e+002 1.131896e+004
1.427395e+002 1.118271e+004
1.437037e+002 1.105517e+004
1.446679e+002 1.093960e+004
1.456322e+002 1.083392e+004
1.465964e+002 1.072968e+004
1.475606e+002 1.063084e+004
1.485249e+002 1.053903e+004
1.494891e+002 1.045199e+004
1.504533e+002 1.036121e+004
1.514176e+002 1.026634e+004
1.523818e+002 1.018469e+004
1.533460e+002 1.012296e+004
1.543103e+002 1.007958e+004
1.552745e+002 1.004018e+004
1.562387e+002 9.983873e+003
1.572030e+002 9.919802e+003
1.581672e+002 9.852521e+003
1.591314e+002 9.784660e+003
1.600957e+002 9.711412e+003
1.610599e+002 9.643094e+003
1.620241e+002 9.582323e+003
1.629884e+002 9.531659e+003
1.639526e+002 9.494783e+003
1.649168e+002 9.487323e+003
1.658811e+002 9.487938e+003
1.668453e+002 9.489313e+003
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1.687738e+002 9.483325e+003
1.697380e+002 9.479576e+003
1.707022e+002 9.474260e+003
1.716665e+002 9.457575e+003
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1.784161e+002 9.443440e+003
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2.121642e+002 1.100270e+004
2.131285e+002 1.106234e+004
2.140927e+002 1.112280e+004
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2.160212e+002 1.126098e+004
2.169854e+002 1.134241e+004
2.179496e+002 1.139390e+004
2.189139e+002 1.141332e+004
2.198781e+002 1.141798e+004
2.208423e+002 1.143201e+004
2.218066e+002 1.145656e+004
2.227708e+002 1.147590e+004
2.237350e+002 1.150080e+004
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2.536263e+002 1.135690e+004
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2.758036e+002 9.957177e+003
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2.777321e+002 9.832610e+003
2.786964e+002 9.756458e+003
2.796606e+002 9.682340e+003
2.806248e+002 9.601300e+003
2.815891e+002 9.533855e+003
2.825533e+002 9.491095e+003
2.835175e+002 9.469282e+003
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2.950883e+002 8.907632e+003
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