#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500068.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500068
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial PbO
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Alfa Aesar 99.9%'
_chemical_formula_structural     'O Pb'
_chemical_formula_sum            'O Pb'
_chemical_name_mineral           Litharge
_chemical_name_systematic        'Plumbous oxide'
_space_group_IT_number           57
_symmetry_space_group_name_Hall  '-P 2a 2ab'
_symmetry_space_group_name_H-M   'P b m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.891
_cell_length_b                   4.775
_cell_length_c                   5.489
_raman_determination_method      experimental
_[local]_chemical_compound_color yelow
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2249.589
_rod_data_source.file            PbO.rod
_rod_data_source.block           1000005
_rod_database.code               3500068
_solsa_sample.id                 CN-AA00-0057
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008960 COD http://www.crystallography.net/cod/9008960.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 1.566038e+003
5.113732e+001 1.576546e+003
5.210155e+001 1.595384e+003
5.306579e+001 1.617516e+003
5.403002e+001 1.637408e+003
5.499426e+001 1.645787e+003
5.595849e+001 1.660159e+003
5.692272e+001 1.689955e+003
5.788696e+001 1.735966e+003
5.885119e+001 1.795848e+003
5.981542e+001 1.866702e+003
6.077965e+001 1.943547e+003
6.174389e+001 2.027146e+003
6.270812e+001 2.119048e+003
6.367235e+001 2.222939e+003
6.463658e+001 2.299791e+003
6.560081e+001 2.355493e+003
6.656505e+001 2.394582e+003
6.752928e+001 2.415724e+003
6.849352e+001 2.386485e+003
6.945775e+001 2.382624e+003
7.042198e+001 2.384591e+003
7.138622e+001 2.413874e+003
7.235045e+001 2.505132e+003
7.331468e+001 2.713175e+003
7.427892e+001 2.990545e+003
7.524315e+001 3.349232e+003
7.620738e+001 3.774894e+003
7.717162e+001 4.224675e+003
7.813585e+001 4.693286e+003
7.910008e+001 5.107261e+003
8.006432e+001 5.355398e+003
8.102855e+001 5.360192e+003
8.199278e+001 5.097683e+003
8.295702e+001 4.745032e+003
8.392125e+001 4.276443e+003
8.488548e+001 3.767681e+003
8.584972e+001 3.317428e+003
8.681395e+001 2.947762e+003
8.777818e+001 2.648936e+003
8.874242e+001 2.434801e+003
8.970665e+001 2.293121e+003
9.067088e+001 2.183646e+003
9.163512e+001 2.103585e+003
9.259935e+001 2.038800e+003
9.356358e+001 1.991325e+003
9.452782e+001 1.960638e+003
9.549205e+001 1.943119e+003
9.645628e+001 1.933522e+003
9.742052e+001 1.927517e+003
9.838475e+001 1.922703e+003
9.934898e+001 1.917050e+003
1.003132e+002 1.910698e+003
1.012775e+002 1.911613e+003
1.022417e+002 1.920979e+003
1.032059e+002 1.933669e+003
1.041701e+002 1.940975e+003
1.051344e+002 1.936664e+003
1.060986e+002 1.941760e+003
1.070628e+002 1.954718e+003
1.080271e+002 1.974217e+003
1.089913e+002 1.998998e+003
1.099555e+002 2.028228e+003
1.109198e+002 2.063743e+003
1.118840e+002 2.103620e+003
1.128482e+002 2.148795e+003
1.138125e+002 2.209628e+003
1.147767e+002 2.291442e+003
1.157409e+002 2.390612e+003
1.167052e+002 2.502480e+003
1.176694e+002 2.623756e+003
1.186336e+002 2.774240e+003
1.195979e+002 2.977913e+003
1.205621e+002 3.229011e+003
1.215263e+002 3.537505e+003
1.224906e+002 3.921037e+003
1.234548e+002 4.392124e+003
1.244190e+002 4.981836e+003
1.253833e+002 5.694600e+003
1.263475e+002 6.524540e+003
1.273117e+002 7.462276e+003
1.282760e+002 8.702781e+003
1.292402e+002 9.870827e+003
1.302044e+002 1.098670e+004
1.311687e+002 1.201840e+004
1.321329e+002 1.274186e+004
1.330971e+002 1.298070e+004
1.340614e+002 1.289969e+004
1.350256e+002 1.249430e+004
1.359898e+002 1.177353e+004
1.369541e+002 1.083762e+004
1.379183e+002 9.892474e+003
1.388825e+002 8.951389e+003
1.398468e+002 8.057208e+003
1.408110e+002 7.261903e+003
1.417752e+002 6.595047e+003
1.427395e+002 6.035040e+003
1.437037e+002 5.599896e+003
1.446679e+002 5.268111e+003
1.456322e+002 4.983982e+003
1.465964e+002 4.780052e+003
1.475606e+002 4.592320e+003
1.485249e+002 4.418331e+003
1.494891e+002 4.256402e+003
1.504533e+002 4.103033e+003
1.514176e+002 3.959830e+003
1.523818e+002 3.832631e+003
1.533460e+002 3.729441e+003
1.543103e+002 3.649456e+003
1.552745e+002 3.579136e+003
1.562387e+002 3.491463e+003
1.572030e+002 3.397789e+003
1.581672e+002 3.310153e+003
1.591314e+002 3.237835e+003
1.600957e+002 3.180426e+003
1.610599e+002 3.115583e+003
1.620241e+002 3.042932e+003
1.629884e+002 2.970301e+003
1.639526e+002 2.907091e+003
1.649168e+002 2.860820e+003
1.658811e+002 2.819332e+003
1.668453e+002 2.780538e+003
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1.687738e+002 2.703441e+003
1.697380e+002 2.659193e+003
1.707022e+002 2.619519e+003
1.716665e+002 2.588493e+003
1.726307e+002 2.564077e+003
1.735949e+002 2.539791e+003
1.745592e+002 2.507203e+003
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1.764876e+002 2.431692e+003
1.774519e+002 2.390326e+003
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1.793803e+002 2.321409e+003
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1.919154e+002 2.038034e+003
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2.025219e+002 1.981796e+003
2.034862e+002 1.980475e+003
2.044504e+002 1.986171e+003
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2.063788e+002 2.027946e+003
2.073431e+002 2.045475e+003
2.083073e+002 2.046268e+003
2.092715e+002 2.044619e+003
2.102358e+002 2.049534e+003
2.112000e+002 2.067003e+003
2.121642e+002 2.092680e+003
2.131285e+002 2.113970e+003
2.140927e+002 2.131953e+003
2.150569e+002 2.148974e+003
2.160212e+002 2.167793e+003
2.169854e+002 2.188739e+003
2.179496e+002 2.207677e+003
2.189139e+002 2.223638e+003
2.198781e+002 2.240615e+003
2.208423e+002 2.264469e+003
2.218066e+002 2.300078e+003
2.227708e+002 2.332958e+003
2.237350e+002 2.365285e+003
2.246993e+002 2.398683e+003
2.256635e+002 2.434599e+003
2.266277e+002 2.471307e+003
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2.314489e+002 2.636181e+003
2.324131e+002 2.682365e+003
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2.343416e+002 2.760727e+003
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2.497693e+002 3.692940e+003
2.507336e+002 3.737801e+003
2.516978e+002 3.762430e+003
2.526620e+002 3.777104e+003
2.536263e+002 3.794609e+003
2.545905e+002 3.828010e+003
2.555547e+002 3.876252e+003
2.565190e+002 3.911912e+003
2.574832e+002 3.935948e+003
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2.594117e+002 3.989781e+003
2.603759e+002 4.038898e+003
2.613401e+002 4.078541e+003
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2.632686e+002 4.144385e+003
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2.690540e+002 4.121295e+003
2.700182e+002 4.107362e+003
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2.729109e+002 3.928493e+003
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2.748394e+002 3.799050e+003
2.758036e+002 3.803765e+003
2.767679e+002 3.799548e+003
2.777321e+002 3.778029e+003
2.786964e+002 3.740237e+003
2.796606e+002 3.691947e+003
2.806248e+002 3.622569e+003
2.815891e+002 3.554952e+003
2.825533e+002 3.492650e+003
2.835175e+002 3.435567e+003
2.844818e+002 3.378148e+003
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2.864102e+002 3.262379e+003
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2.893029e+002 3.075949e+003
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2.912314e+002 2.964633e+003
2.921956e+002 2.916327e+003
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2.941241e+002 2.848698e+003
2.950883e+002 2.807259e+003
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2.970168e+002 2.696605e+003
2.979810e+002 2.652565e+003
2.989453e+002 2.622400e+003
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3.076234e+002 2.279776e+003
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_rod_maintainer_comment.date
_rod_maintainer_comment.text
1 elmendili 2017-10-06T16:07:05+0300 'Mineral name changed'