#------------------------------------------------------------------------------
#$Date: 2017-11-07 14:10:34 +0200 (Tue, 07 Nov 2017) $
#$Revision: 294 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500069.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500069
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial PbO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial RP NORMAPUR AR 98%'
_chemical_formula_structural     'O2 Pb'
_chemical_formula_sum            'O2 Pb'
_chemical_name_mineral           Plattnerite
_chemical_name_systematic        'Lead(IV) oxide'
_space_group_IT_number           201
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  'P 2 2 3 -1n'
_symmetry_space_group_name_H-M   'P n -3 :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   5.38
_cell_length_b                   5.38
_cell_length_c                   5.38
_raman_determination_method      experimental
_[local]_chemical_compound_color black
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     21.24609
_raman_measurement.range_max     2999.762
_rod_data_source.file            PbO2.rod
_rod_data_source.block           1000005
_rod_database.code               3500069
_solsa_sample.id                 CN-AA00-0058
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1010382 COD http://www.crystallography.net/cod/1010382.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
2.124609e+001 2.431921e+002
2.221033e+001 2.516029e+002
2.317456e+001 2.599084e+002
2.413879e+001 2.674555e+002
2.510303e+001 2.796566e+002
2.606726e+001 2.937283e+002
2.703149e+001 3.117532e+002
2.799573e+001 3.416841e+002
2.895996e+001 3.843824e+002
2.992419e+001 4.399659e+002
3.088842e+001 5.110570e+002
3.185266e+001 5.977155e+002
3.281689e+001 6.962325e+002
3.378112e+001 8.136146e+002
3.474536e+001 9.330902e+002
3.570959e+001 1.044252e+003
3.667382e+001 1.135669e+003
3.763805e+001 1.090462e+003
3.860229e+001 1.065613e+003
3.956652e+001 1.054450e+003
4.053075e+001 1.050505e+003
4.149499e+001 1.046031e+003
4.245922e+001 1.045458e+003
4.342345e+001 1.047255e+003
4.438769e+001 1.052554e+003
4.535192e+001 1.062218e+003
4.631615e+001 1.070740e+003
4.728039e+001 1.069473e+003
4.824462e+001 1.069710e+003
4.920885e+001 1.076918e+003
5.017309e+001 1.094237e+003
5.113732e+001 1.107295e+003
5.210155e+001 1.108919e+003
5.306579e+001 1.105931e+003
5.403002e+001 1.104601e+003
5.499425e+001 1.109873e+003
5.595848e+001 1.122458e+003
5.692272e+001 1.141869e+003
5.788695e+001 1.168255e+003
5.885118e+001 1.201522e+003
5.981542e+001 1.241810e+003
6.077965e+001 1.286630e+003
6.174389e+001 1.337062e+003
6.270812e+001 1.393919e+003
6.367235e+001 1.458457e+003
6.463658e+001 1.531709e+003
6.560081e+001 1.627076e+003
6.656505e+001 1.720816e+003
6.752928e+001 1.792206e+003
6.849352e+001 1.829407e+003
6.945775e+001 1.845434e+003
7.042198e+001 1.818900e+003
7.138622e+001 1.775798e+003
7.235045e+001 1.758353e+003
7.331468e+001 1.787006e+003
7.427892e+001 1.875907e+003
7.524315e+001 2.032272e+003
7.620738e+001 2.256630e+003
7.717162e+001 2.545609e+003
7.813585e+001 2.950346e+003
7.910008e+001 3.393837e+003
8.006432e+001 3.825833e+003
8.102855e+001 4.209834e+003
8.199278e+001 4.532796e+003
8.295702e+001 4.577909e+003
8.392125e+001 4.335710e+003
8.488548e+001 3.916570e+003
8.584971e+001 3.458585e+003
8.681394e+001 2.862646e+003
8.777818e+001 2.383171e+003
8.874241e+001 2.048924e+003
8.970664e+001 1.838927e+003
9.067088e+001 1.680775e+003
9.163511e+001 1.571093e+003
9.259934e+001 1.485825e+003
9.356358e+001 1.429030e+003
9.452781e+001 1.398859e+003
9.549204e+001 1.383115e+003
9.645628e+001 1.363191e+003
9.742051e+001 1.342574e+003
9.838474e+001 1.324833e+003
9.934898e+001 1.312911e+003
1.003132e+002 1.306956e+003
1.012774e+002 1.305896e+003
1.022417e+002 1.310626e+003
1.032059e+002 1.317523e+003
1.041701e+002 1.320455e+003
1.051344e+002 1.316807e+003
1.060986e+002 1.316653e+003
1.070628e+002 1.317110e+003
1.080271e+002 1.318465e+003
1.089913e+002 1.324940e+003
1.099555e+002 1.339867e+003
1.109198e+002 1.358600e+003
1.118840e+002 1.378987e+003
1.128482e+002 1.401130e+003
1.138125e+002 1.431421e+003
1.147767e+002 1.473601e+003
1.157409e+002 1.524926e+003
1.167052e+002 1.582829e+003
1.176694e+002 1.645529e+003
1.186336e+002 1.722823e+003
1.195979e+002 1.824521e+003
1.205621e+002 1.948049e+003
1.215263e+002 2.100237e+003
1.224906e+002 2.292506e+003
1.234548e+002 2.525338e+003
1.244190e+002 2.841148e+003
1.253833e+002 3.238769e+003
1.263475e+002 3.717323e+003
1.273117e+002 4.281166e+003
1.282760e+002 4.951866e+003
1.292402e+002 5.704009e+003
1.302044e+002 6.599808e+003
1.311687e+002 7.628703e+003
1.321329e+002 8.599576e+003
1.330971e+002 9.512829e+003
1.340614e+002 1.023959e+004
1.350256e+002 1.068953e+004
1.359898e+002 1.081093e+004
1.369541e+002 1.059785e+004
1.379183e+002 1.004772e+004
1.388825e+002 9.253177e+003
1.398468e+002 8.343149e+003
1.408110e+002 7.464122e+003
1.417752e+002 6.619235e+003
1.427395e+002 5.885694e+003
1.437037e+002 5.271530e+003
1.446679e+002 4.766882e+003
1.456322e+002 4.339529e+003
1.465964e+002 4.022728e+003
1.475606e+002 3.763271e+003
1.485249e+002 3.579992e+003
1.494891e+002 3.459579e+003
1.504533e+002 3.347529e+003
1.514176e+002 3.209652e+003
1.523818e+002 3.077723e+003
1.533460e+002 2.962878e+003
1.543103e+002 2.868323e+003
1.552745e+002 2.788609e+003
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1.591314e+002 2.534785e+003
1.600957e+002 2.473862e+003
1.610599e+002 2.413688e+003
1.620241e+002 2.355116e+003
1.629884e+002 2.299053e+003
1.639526e+002 2.246726e+003
1.649168e+002 2.201527e+003
1.658811e+002 2.159253e+003
1.668453e+002 2.116841e+003
1.678095e+002 2.074736e+003
1.687738e+002 2.034385e+003
1.697380e+002 1.998190e+003
1.707022e+002 1.964928e+003
1.716665e+002 1.934689e+003
1.726307e+002 1.906130e+003
1.735949e+002 1.876340e+003
1.745592e+002 1.839323e+003
1.755234e+002 1.801546e+003
1.764876e+002 1.767691e+003
1.774519e+002 1.739772e+003
1.784161e+002 1.717382e+003
1.793803e+002 1.698966e+003
1.803446e+002 1.683633e+003
1.813088e+002 1.668895e+003
1.822730e+002 1.654269e+003
1.832373e+002 1.641727e+003
1.842015e+002 1.622248e+003
1.851657e+002 1.590323e+003
1.861300e+002 1.559242e+003
1.870942e+002 1.540645e+003
1.880584e+002 1.544299e+003
1.890227e+002 1.544600e+003
1.899869e+002 1.530740e+003
1.909511e+002 1.509184e+003
1.919154e+002 1.487728e+003
1.928796e+002 1.475083e+003
1.938438e+002 1.462511e+003
1.948080e+002 1.441290e+003
1.957723e+002 1.414021e+003
1.967365e+002 1.387028e+003
1.977007e+002 1.374230e+003
1.986650e+002 1.375220e+003
1.996292e+002 1.375845e+003
2.005934e+002 1.373321e+003
2.015577e+002 1.367786e+003
2.025219e+002 1.363658e+003
2.034861e+002 1.363505e+003
2.044504e+002 1.366013e+003
2.054146e+002 1.368582e+003
2.063788e+002 1.368953e+003
2.073431e+002 1.368682e+003
2.083073e+002 1.371910e+003
2.092715e+002 1.375141e+003
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2.112000e+002 1.374971e+003
2.121642e+002 1.379472e+003
2.131285e+002 1.399200e+003
2.140927e+002 1.424893e+003
2.150569e+002 1.447474e+003
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2.169854e+002 1.459154e+003
2.179496e+002 1.464190e+003
2.189139e+002 1.473744e+003
2.198781e+002 1.485909e+003
2.208423e+002 1.497817e+003
2.218066e+002 1.506430e+003
2.227708e+002 1.517439e+003
2.237350e+002 1.531803e+003
2.246993e+002 1.550750e+003
2.256635e+002 1.575621e+003
2.266277e+002 1.608628e+003
2.275920e+002 1.641313e+003
2.285562e+002 1.674590e+003
2.295204e+002 1.706923e+003
2.304847e+002 1.735734e+003
2.314489e+002 1.751898e+003
2.324131e+002 1.766642e+003
2.333774e+002 1.790568e+003
2.343416e+002 1.825219e+003
2.353058e+002 1.866021e+003
2.362701e+002 1.893264e+003
2.372343e+002 1.907580e+003
2.381985e+002 1.928906e+003
2.391628e+002 1.966384e+003
2.401270e+002 2.021315e+003
2.410912e+002 2.064456e+003
2.420555e+002 2.093577e+003
2.430197e+002 2.125239e+003
2.439839e+002 2.164866e+003
2.449482e+002 2.212465e+003
2.459124e+002 2.265732e+003
2.468766e+002 2.326071e+003
2.478409e+002 2.386393e+003
2.488051e+002 2.442031e+003
2.497693e+002 2.490156e+003
2.507336e+002 2.537681e+003
2.516978e+002 2.592086e+003
2.526620e+002 2.650684e+003
2.536263e+002 2.710232e+003
2.545905e+002 2.768386e+003
2.555547e+002 2.824067e+003
2.565190e+002 2.878690e+003
2.574832e+002 2.933470e+003
2.584474e+002 2.990840e+003
2.594117e+002 3.055104e+003
2.603759e+002 3.142854e+003
2.613401e+002 3.200001e+003
2.623044e+002 3.206522e+003
2.632686e+002 3.191713e+003
2.642328e+002 3.201071e+003
2.651971e+002 3.277477e+003
2.661613e+002 3.346894e+003
2.671255e+002 3.382544e+003
2.680898e+002 3.388402e+003
2.690540e+002 3.377790e+003
2.700182e+002 3.361747e+003
2.709825e+002 3.347665e+003
2.719467e+002 3.344893e+003
2.729109e+002 3.352448e+003
2.738752e+002 3.363152e+003
2.748394e+002 3.356217e+003
2.758036e+002 3.327673e+003
2.767679e+002 3.290587e+003
2.777321e+002 3.245804e+003
2.786963e+002 3.194169e+003
2.796606e+002 3.142078e+003
2.806248e+002 3.093734e+003
2.815890e+002 3.040930e+003
2.825533e+002 2.978828e+003
2.835175e+002 2.907730e+003
2.844817e+002 2.835337e+003
2.854460e+002 2.763979e+003
2.864102e+002 2.695616e+003
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2.902671e+002 2.489211e+003
2.912314e+002 2.458531e+003
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2.950883e+002 2.281690e+003
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3.105160e+002 1.626131e+003
3.114803e+002 1.597122e+003
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3.134087e+002 1.544012e+003
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3.780123e+002 1.118842e+003
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3.809050e+002 1.075536e+003
3.818693e+002 1.056621e+003
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3.847620e+002 9.985601e+002
3.857262e+002 9.852865e+002
3.866904e+002 9.686242e+002
3.876547e+002 9.486957e+002
3.886189e+002 9.297881e+002
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3.944043e+002 8.666076e+002
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3.963328e+002 8.455845e+002
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3.982612e+002 8.199196e+002
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4.011539e+002 8.026024e+002
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loop_
_rod_maintainer_comment.id
_rod_maintainer_comment.author
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_rod_maintainer_comment.text
1 elmendili 2017-10-06T16:09:58+0300 'Mineral name changed'