#------------------------------------------------------------------------------
#$Date: 2017-11-07 14:10:34 +0200 (Tue, 07 Nov 2017) $
#$Revision: 294 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500075.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500075
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial (NH4)10(H2W12O42)4H2O
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Alfa aesar 99.9%'
_chemical_formula_structural     'H50 N6 O52 W12'
_chemical_formula_sum            'H50 N6 O52 W12'
_chemical_name_mineral           'Ammonium paratungstate'
_chemical_name_systematic        'Ammonium paratungstate'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                102.46(5)
_cell_angle_beta                 97.31(5)
_cell_angle_gamma                88.61(5)
_cell_formula_units_Z            2
_cell_length_a                   11.94(2)
_cell_length_b                   13.21(1)
_cell_length_c                   16.63(1)
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     50.17309
_raman_measurement.range_max     2500.290
_rod_data_source.file            Ammoniumparatungstate.rod
_rod_data_source.block           1000005
_rod_database.code               3500075
_solsa_sample.id                 CN-AA00-0064
_raman_measurement.datetime_initiated 2017-09-20
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1007039 COD http://www.crystallography.net/cod/1007039.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.017309e+001 8.903177e+002
5.113732e+001 8.901553e+002
5.210155e+001 8.854247e+002
5.306579e+001 8.788796e+002
5.403002e+001 8.730892e+002
5.499426e+001 8.706514e+002
5.595849e+001 8.710048e+002
5.692272e+001 8.722137e+002
5.788696e+001 8.752023e+002
5.885119e+001 8.817721e+002
5.981542e+001 8.968834e+002
6.077965e+001 9.178646e+002
6.174389e+001 9.452123e+002
6.270812e+001 9.797207e+002
6.367235e+001 1.022987e+003
6.463658e+001 1.064420e+003
6.560081e+001 1.106377e+003
6.656505e+001 1.147347e+003
6.752928e+001 1.185884e+003
6.849352e+001 1.220115e+003
6.945775e+001 1.248142e+003
7.042198e+001 1.272121e+003
7.138622e+001 1.290296e+003
7.235045e+001 1.300011e+003
7.331468e+001 1.294082e+003
7.427892e+001 1.286143e+003
7.524315e+001 1.277016e+003
7.620738e+001 1.268537e+003
7.717162e+001 1.264216e+003
7.813585e+001 1.271686e+003
7.910008e+001 1.286908e+003
8.006432e+001 1.310899e+003
8.102855e+001 1.344631e+003
8.199278e+001 1.390431e+003
8.295702e+001 1.428504e+003
8.392125e+001 1.461037e+003
8.488548e+001 1.480564e+003
8.584972e+001 1.476848e+003
8.681395e+001 1.429968e+003
8.777818e+001 1.380962e+003
8.874242e+001 1.327174e+003
8.970665e+001 1.273004e+003
9.067088e+001 1.228814e+003
9.163512e+001 1.200116e+003
9.259935e+001 1.180931e+003
9.356358e+001 1.174394e+003
9.452782e+001 1.180367e+003
9.549205e+001 1.192440e+003
9.645628e+001 1.201425e+003
9.742052e+001 1.208174e+003
9.838475e+001 1.213333e+003
9.934898e+001 1.217486e+003
1.003132e+002 1.219620e+003
1.012775e+002 1.219316e+003
1.022417e+002 1.217513e+003
1.032059e+002 1.214827e+003
1.041701e+002 1.211887e+003
1.051344e+002 1.209743e+003
1.060986e+002 1.209811e+003
1.070628e+002 1.210391e+003
1.080271e+002 1.211293e+003
1.089913e+002 1.214096e+003
1.099555e+002 1.217907e+003
1.109198e+002 1.225060e+003
1.118840e+002 1.238373e+003
1.128482e+002 1.258356e+003
1.138125e+002 1.279141e+003
1.147767e+002 1.291938e+003
1.157409e+002 1.302663e+003
1.167052e+002 1.316863e+003
1.176694e+002 1.339036e+003
1.186336e+002 1.366220e+003
1.195979e+002 1.383441e+003
1.205621e+002 1.391431e+003
1.215263e+002 1.393523e+003
1.224906e+002 1.394996e+003
1.234548e+002 1.397291e+003
1.244190e+002 1.399001e+003
1.253833e+002 1.400811e+003
1.263475e+002 1.402505e+003
1.273117e+002 1.402854e+003
1.282760e+002 1.397368e+003
1.292402e+002 1.392370e+003
1.302044e+002 1.388843e+003
1.311687e+002 1.386934e+003
1.321329e+002 1.385524e+003
1.330971e+002 1.382443e+003
1.340614e+002 1.380856e+003
1.350256e+002 1.384308e+003
1.359898e+002 1.395225e+003
1.369541e+002 1.411643e+003
1.379183e+002 1.421595e+003
1.388825e+002 1.427092e+003
1.398468e+002 1.434168e+003
1.408110e+002 1.450112e+003
1.417752e+002 1.477828e+003
1.427395e+002 1.501615e+003
1.437037e+002 1.521877e+003
1.446679e+002 1.540567e+003
1.456322e+002 1.561028e+003
1.465964e+002 1.584825e+003
1.475606e+002 1.606672e+003
1.485249e+002 1.626111e+003
1.494891e+002 1.642734e+003
1.504533e+002 1.656339e+003
1.514176e+002 1.668027e+003
1.523818e+002 1.679207e+003
1.533460e+002 1.689719e+003
1.543103e+002 1.698989e+003
1.552745e+002 1.705048e+003
1.562387e+002 1.703374e+003
1.572030e+002 1.698297e+003
1.581672e+002 1.693350e+003
1.591314e+002 1.691103e+003
1.600957e+002 1.691026e+003
1.610599e+002 1.693347e+003
1.620241e+002 1.699351e+003
1.629884e+002 1.706950e+003
1.639526e+002 1.713422e+003
1.649168e+002 1.717160e+003
1.658811e+002 1.725844e+003
1.668453e+002 1.741086e+003
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1.687738e+002 1.773269e+003
1.697380e+002 1.780034e+003
1.707022e+002 1.785155e+003
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1.726307e+002 1.792123e+003
1.735949e+002 1.794069e+003
1.745592e+002 1.796753e+003
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1.803446e+002 1.783319e+003
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2.025219e+002 2.002853e+003
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2.044504e+002 2.081007e+003
2.054146e+002 2.119999e+003
2.063788e+002 2.156236e+003
2.073431e+002 2.179625e+003
2.083073e+002 2.190540e+003
2.092715e+002 2.191354e+003
2.102358e+002 2.181961e+003
2.112000e+002 2.163369e+003
2.121642e+002 2.143161e+003
2.131285e+002 2.124930e+003
2.140927e+002 2.106690e+003
2.150569e+002 2.087407e+003
2.160212e+002 2.066512e+003
2.169854e+002 2.045475e+003
2.179496e+002 2.030173e+003
2.189139e+002 2.020117e+003
2.198781e+002 2.014868e+003
2.208423e+002 2.013870e+003
2.218066e+002 2.018167e+003
2.227708e+002 2.023821e+003
2.237350e+002 2.033250e+003
2.246993e+002 2.046565e+003
2.256635e+002 2.062769e+003
2.266277e+002 2.080926e+003
2.275920e+002 2.096902e+003
2.285562e+002 2.111784e+003
2.295204e+002 2.125045e+003
2.304847e+002 2.135519e+003
2.314489e+002 2.138897e+003
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2.488051e+002 1.902588e+003
2.497693e+002 1.851218e+003
2.507336e+002 1.800501e+003
2.516978e+002 1.751080e+003
2.526620e+002 1.701379e+003
2.536263e+002 1.649718e+003
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2.555547e+002 1.532950e+003
2.565190e+002 1.474221e+003
2.574832e+002 1.418558e+003
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2.594117e+002 1.311887e+003
2.603759e+002 1.256608e+003
2.613401e+002 1.203279e+003
2.623044e+002 1.151073e+003
2.632686e+002 1.101382e+003
2.642328e+002 1.056780e+003
2.651971e+002 1.020799e+003
2.661613e+002 9.874715e+002
2.671255e+002 9.536422e+002
2.680898e+002 9.193918e+002
2.690540e+002 8.856849e+002
2.700182e+002 8.552414e+002
2.709825e+002 8.272214e+002
2.719467e+002 8.001281e+002
2.729109e+002 7.738528e+002
2.738752e+002 7.482494e+002
2.748394e+002 7.221146e+002
2.758036e+002 6.946401e+002
2.767679e+002 6.700631e+002
2.777321e+002 6.498664e+002
2.786964e+002 6.337444e+002
2.796606e+002 6.187841e+002
2.806248e+002 6.055029e+002
2.815891e+002 5.929648e+002
2.825533e+002 5.801354e+002
2.835175e+002 5.671472e+002
2.844818e+002 5.562567e+002
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2.893029e+002 5.476161e+002
2.902672e+002 5.517702e+002
2.912314e+002 5.568298e+002
2.921956e+002 5.652225e+002
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2.941241e+002 5.960817e+002
2.950883e+002 6.128539e+002
2.960526e+002 6.270443e+002
2.970168e+002 6.448766e+002
2.979810e+002 6.700547e+002
2.989453e+002 7.037247e+002
2.999095e+002 7.386087e+002
3.008737e+002 7.754446e+002
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3.037664e+002 8.930117e+002
3.047307e+002 9.338654e+002
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3.076234e+002 1.063008e+003
3.085876e+002 1.113218e+003
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