#------------------------------------------------------------------------------
#$Date: 2017-10-17 18:40:30 +0300 (Tue, 17 Oct 2017) $
#$Revision: 269 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500084.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500084
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial cobalt (II) dicobalt (III) oxide
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa aesar 99.7% 40184A4'
_chemical_formula_structural     'Co3 O4'
_chemical_formula_sum            'Co3 O4'
_chemical_name_mineral           'cobalt (II) dicobalt (III) oxide'
_chemical_name_systematic        'Co Co2 O4'
_space_group_IT_number           216
_symmetry_space_group_name_Hall  'F -4 2 3'
_symmetry_space_group_name_H-M   'F -4 3 m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   8.065
_cell_length_b                   8.065
_cell_length_c                   8.065
_raman_determination_method      experimental
_[local]_chemical_compound_color gray
_[local]_chemical_compound_state Solid
_solsa_sample.id                 CN-AA00-0073
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     3.938696e+001
_raman_measurement.range_max     2.999583e+003
_rod_data_source.file            Co3O4.rod
_rod_data_source.block           1000005
_rod_database.code               3500084
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1526734 COD http://www.crystallography.net/cod/1526734.html
;
 The structure contains the XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
3.938696e+001 1.720004e+001
4.035120e+001 1.417574e+001
4.131543e+001 1.176798e+001
4.227966e+001 1.050031e+001
4.324390e+001 9.266647e+000
4.420813e+001 7.659395e+000
4.517236e+001 5.532425e+000
4.613660e+001 4.250057e+000
4.710083e+001 4.113497e+000
4.806506e+001 4.263790e+000
4.902930e+001 4.236677e+000
4.999353e+001 3.698122e+000
5.095776e+001 2.943819e+000
5.192200e+001 2.113293e+000
5.288623e+001 1.314692e+000
5.385046e+001 6.687317e-001
5.481470e+001 3.877583e-001
5.577893e+001 4.109535e-001
5.674316e+001 7.017212e-001
5.770740e+001 1.259869e+000
5.867163e+001 2.052656e+000
5.963586e+001 2.522831e+000
6.060010e+001 2.789249e+000
6.156433e+001 2.864641e+000
6.252856e+001 2.653156e+000
6.349280e+001 1.902143e+000
6.445703e+001 1.272051e+000
6.542126e+001 8.175240e-001
6.638550e+001 4.999218e-001
6.734973e+001 2.575245e-001
6.831396e+001 -2.120972e-002
6.927820e+001 7.880402e-002
7.024243e+001 9.649086e-001
7.120667e+001 2.322739e+000
7.217090e+001 3.552086e+000
7.313513e+001 3.328453e+000
7.409937e+001 2.448851e+000
7.506360e+001 1.512848e+000
7.602783e+001 7.946148e-001
7.699207e+001 3.247013e-001
7.795630e+001 -7.205200e-002
7.892053e+001 -5.015583e-001
7.988477e+001 -7.225800e-001
8.084900e+001 -4.492455e-001
8.181323e+001 8.726978e-001
8.277747e+001 1.608402e+000
8.374170e+001 1.630686e+000
8.470593e+001 1.216908e+000
8.567017e+001 7.557182e-001
8.663440e+001 1.130486e-001
8.759863e+001 -2.357502e-001
8.856287e+001 2.742958e-002
8.952710e+001 7.869301e-001
9.049133e+001 1.546314e+000
9.145557e+001 1.434498e+000
9.241980e+001 1.025526e+000
9.338403e+001 6.274128e-001
9.434827e+001 4.237843e-001
9.531250e+001 3.891106e-001
9.627673e+001 2.397137e-001
9.724097e+001 -3.276253e-002
9.820520e+001 -3.699360e-001
9.916943e+001 -7.120762e-001
1.001337e+002 -1.065783e+000
1.010979e+002 -1.262117e+000
1.020621e+002 -1.329073e+000
1.030264e+002 -1.250328e+000
1.039906e+002 -9.867229e-001
1.049548e+002 -1.020432e-001
1.059191e+002 4.407120e-001
1.068833e+002 3.704872e-001
1.078475e+002 -2.307987e-001
1.088118e+002 -8.212852e-001
1.097760e+002 -8.754215e-001
1.107402e+002 -7.346611e-001
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1.126687e+002 -3.863468e-001
1.136329e+002 -3.324146e-001
1.145972e+002 -4.079666e-001
1.155614e+002 -5.637836e-001
1.165256e+002 -7.343693e-001
1.174899e+002 -8.494377e-001
1.184541e+002 -8.476982e-001
1.194183e+002 -7.370796e-001
1.203826e+002 -4.912415e-001
1.213468e+002 -1.787510e-001
1.223110e+002 7.911491e-002
1.232753e+002 3.881416e-001
1.242395e+002 4.218006e-001
1.252037e+002 -1.065350e-001
1.261680e+002 -1.029898e+000
1.271322e+002 -1.644182e+000
1.280964e+002 -1.055532e+000
1.290607e+002 -2.464485e-001
1.300249e+002 5.508900e-001
1.309891e+002 1.166611e+000
1.319534e+002 1.473894e+000
1.329176e+002 9.732399e-001
1.338818e+002 1.214066e-001
1.348461e+002 -5.254269e-001
1.358103e+002 -4.951286e-001
1.367745e+002 3.108597e-001
1.377388e+002 8.890209e-001
1.387030e+002 1.310101e+000
1.396672e+002 1.527149e+000
1.406315e+002 1.444645e+000
1.415957e+002 6.756573e-001
1.425599e+002 8.016396e-002
1.435242e+002 -3.752651e-001
1.444884e+002 -6.599770e-001
1.454526e+002 -7.101440e-001
1.464169e+002 -7.893372e-002
1.473811e+002 5.463409e-001
1.483453e+002 8.833408e-001
1.493096e+002 9.472790e-001
1.502738e+002 9.095459e-001
1.512380e+002 1.138702e+000
1.522023e+002 1.425396e+000
1.531665e+002 1.544857e+000
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1.550950e+002 8.622475e-001
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1.570234e+002 2.505569e-001
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1.936643e+002 9.087269e+000
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2.033066e+002 1.971157e+000
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2.071636e+002 1.297226e-001
2.081278e+002 -1.299839e-001
2.090920e+002 5.352249e-001
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loop_
_rod_maintainer_comment.id
_rod_maintainer_comment.author
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_rod_maintainer_comment.text
1 elmendili 2017-10-17T18:40:30+0300 'Solsa sample id changed'