#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500089.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500089
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial lithiophosphate
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa aesar 99.99% 10743'
_chemical_formula_structural     'Li3 O4 P'
_chemical_formula_sum            'Li6 O8 P2'
_chemical_name_mineral           lithiophosphate
_chemical_name_systematic        'Li3 O4 P'
_space_group_IT_number           31
_symmetry_space_group_name_Hall  'P 2ac -2'
_symmetry_space_group_name_H-M   'P m n 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   6.115
_cell_length_b                   5.2394
_cell_length_c                   4.8554
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_solsa_sample.id                 CN-AA00-0078
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     9.916943e+001
_raman_measurement.range_max     3.500020e+003
_rod_data_source.file            Li3PO4.rod
_rod_data_source.block           1000005
_rod_database.code               3500089
_raman_measurement.datetime_initiated 2017-10-17
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9012500 COD http://www.crystallography.net/cod/9012500.html
;
 The structure contains the XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
9.916943e+001 2.313797e+000
1.001337e+002 -9.928436e-001
1.010979e+002 -2.789795e+000
1.020621e+002 -2.402924e+000
1.030264e+002 -6.540070e-001
1.039906e+002 7.637177e-001
1.049548e+002 9.255219e-001
1.059191e+002 1.617432e-003
1.068833e+002 -1.946518e+000
1.078475e+002 -4.380264e+000
1.088118e+002 -6.001205e+000
1.097760e+002 -5.867294e+000
1.107402e+002 -4.426208e+000
1.117045e+002 -1.627686e+000
1.126687e+002 2.151917e+000
1.136329e+002 5.409821e+000
1.145972e+002 5.367233e+000
1.155614e+002 3.106995e+000
1.165256e+002 -4.447937e-002
1.174899e+002 -2.670029e+000
1.184541e+002 -3.891281e+000
1.194183e+002 -3.896591e+000
1.203826e+002 -2.320267e+000
1.213468e+002 -1.199493e-001
1.223110e+002 9.192657e-001
1.232753e+002 -1.675812e+000
1.242395e+002 -3.697144e+000
1.252037e+002 -4.018311e+000
1.261680e+002 -2.802841e+000
1.271322e+002 -1.669250e+000
1.280964e+002 -2.455887e+000
1.290607e+002 -3.195740e+000
1.300249e+002 -2.949097e+000
1.309891e+002 -1.504166e+000
1.319534e+002 -6.253052e-002
1.329176e+002 -1.362366e+000
1.338818e+002 -3.688156e+000
1.348461e+002 -5.207687e+000
1.358103e+002 -4.436905e+000
1.367745e+002 -1.315414e+000
1.377388e+002 8.820038e-001
1.387030e+002 2.668015e+000
1.396672e+002 3.801605e+000
1.406315e+002 3.727859e+000
1.415957e+002 4.575500e-001
1.425599e+002 -1.470581e+000
1.435242e+002 -1.585648e+000
1.444884e+002 -5.172882e-001
1.454526e+002 2.973175e-001
1.464169e+002 3.895874e-001
1.473811e+002 7.607574e-001
1.483453e+002 1.347473e+000
1.493096e+002 2.195908e+000
1.502738e+002 3.494339e+000
1.512380e+002 5.400909e+000
1.522023e+002 8.205048e+000
1.531665e+002 1.255669e+001
1.541307e+002 1.853412e+001
1.550950e+002 2.528864e+001
1.560592e+002 2.981927e+001
1.570234e+002 3.383130e+001
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1.599161e+002 3.373865e+001
1.608804e+002 3.046201e+001
1.618446e+002 2.474904e+001
1.628088e+002 1.784099e+001
1.637731e+002 1.189825e+001
1.647373e+002 9.849503e+000
1.657015e+002 8.677628e+000
1.666658e+002 7.265289e+000
1.676300e+002 5.680283e+000
1.685942e+002 4.410049e+000
1.695585e+002 4.222855e+000
1.705227e+002 4.864731e+000
1.714869e+002 6.355515e+000
1.724512e+002 8.518250e+000
1.734154e+002 1.093404e+001
1.743796e+002 1.166739e+001
1.753439e+002 1.091122e+001
1.763081e+002 1.019872e+001
1.772723e+002 1.031622e+001
1.782366e+002 1.149248e+001
1.792008e+002 1.319919e+001
1.801650e+002 1.529677e+001
1.811293e+002 1.763348e+001
1.820935e+002 2.031184e+001
1.830577e+002 2.379770e+001
1.840220e+002 2.755708e+001
1.849862e+002 3.224075e+001
1.859504e+002 3.610887e+001
1.869147e+002 3.736357e+001
1.878789e+002 3.390685e+001
1.888431e+002 2.804419e+001
1.898074e+002 2.198795e+001
1.907716e+002 1.656615e+001
1.917358e+002 1.257536e+001
1.927000e+002 1.116263e+001
1.936643e+002 1.074879e+001
1.946285e+002 9.583405e+000
1.955927e+002 8.011383e+000
1.965570e+002 6.527161e+000
1.975212e+002 5.249817e+000
1.984854e+002 4.369659e+000
1.994497e+002 4.214966e+000
2.004139e+002 4.289581e+000
2.013781e+002 4.152786e+000
2.023424e+002 4.293488e+000
2.033066e+002 6.193405e+000
2.042708e+002 8.153488e+000
2.052351e+002 9.464035e+000
2.061993e+002 9.853714e+000
2.071635e+002 1.023810e+001
2.081278e+002 1.125208e+001
2.090920e+002 1.177138e+001
2.100562e+002 1.068224e+001
2.110205e+002 7.160675e+000
2.119847e+002 2.008408e+000
2.129489e+002 8.551025e-002
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