#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500090.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500090
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial Lithium metaborate
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa aesar 99.997% 10739'
_chemical_formula_structural     'B Li O2'
_chemical_formula_sum            'B4 Li4 O8'
_chemical_name_mineral           'Lithium metaborate'
_chemical_name_systematic        'B Li O2'
_space_group_IT_number           122
_symmetry_space_group_name_Hall  'I -4 2bw'
_symmetry_space_group_name_H-M   'I -4 2 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   4.1961
_cell_length_b                   4.1961
_cell_length_c                   6.5112
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_solsa_sample.id                 CN-AA00-0079
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     3.938696e+001
_raman_measurement.range_max     2.999583e+003
_rod_data_source.file            LiBO2.rod
_rod_data_source.block           1000005
_rod_database.code               3500090
_raman_measurement.datetime_initiated 2017-10-17
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009881 COD http://www.crystallography.net/cod/9009881.html
;
 The structure contains the XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
3.938696e+001 5.606036e+001
4.035120e+001 5.079158e+001
4.131543e+001 4.688573e+001
4.227966e+001 4.573125e+001
4.324390e+001 4.423673e+001
4.420813e+001 4.123261e+001
4.517236e+001 3.632193e+001
4.613660e+001 3.366665e+001
4.710083e+001 3.481446e+001
4.806506e+001 3.661174e+001
4.902930e+001 3.726454e+001
4.999353e+001 3.534279e+001
5.095776e+001 3.266188e+001
5.192200e+001 2.993928e+001
5.288623e+001 2.767029e+001
5.385046e+001 2.645051e+001
5.481470e+001 2.760992e+001
5.577893e+001 3.061938e+001
5.674316e+001 3.476767e+001
5.770740e+001 3.993678e+001
5.867163e+001 4.587348e+001
5.963586e+001 4.784518e+001
6.060010e+001 4.498564e+001
6.156433e+001 4.191659e+001
6.252856e+001 4.083451e+001
6.349280e+001 4.232015e+001
6.445703e+001 4.431369e+001
6.542126e+001 4.748144e+001
6.638550e+001 5.066602e+001
6.734973e+001 5.266016e+001
6.831396e+001 5.194320e+001
6.927820e+001 5.119942e+001
7.024243e+001 5.159260e+001
7.120667e+001 5.280034e+001
7.217090e+001 5.398179e+001
7.313513e+001 5.368860e+001
7.409937e+001 5.246705e+001
7.506360e+001 5.032069e+001
7.602783e+001 4.740427e+001
7.699207e+001 4.404770e+001
7.795630e+001 4.319661e+001
7.892053e+001 4.428339e+001
7.988477e+001 4.682369e+001
8.084900e+001 5.071154e+001
8.181323e+001 5.752216e+001
8.277747e+001 6.256230e+001
8.374170e+001 6.313964e+001
8.470593e+001 6.279344e+001
8.567017e+001 6.648248e+001
8.663440e+001 7.312109e+001
8.759863e+001 8.948814e+001
8.856287e+001 1.185016e+002
8.952710e+001 1.593717e+002
9.049133e+001 2.079634e+002
9.145557e+001 2.775479e+002
9.241980e+001 3.424070e+002
9.338403e+001 3.868653e+002
9.434827e+001 4.019708e+002
9.531250e+001 3.867851e+002
9.627673e+001 3.400247e+002
9.724097e+001 2.678990e+002
9.820520e+001 1.919706e+002
9.916943e+001 1.338759e+002
1.001337e+002 1.019593e+002
1.010979e+002 7.856017e+001
1.020621e+002 6.502897e+001
1.030264e+002 5.890226e+001
1.039906e+002 5.541838e+001
1.049548e+002 5.689211e+001
1.059191e+002 5.811664e+001
1.068833e+002 5.789247e+001
1.078475e+002 5.643743e+001
1.088118e+002 5.577046e+001
1.097760e+002 5.892607e+001
1.107402e+002 6.295730e+001
1.117045e+002 6.671165e+001
1.126687e+002 6.939233e+001
1.136329e+002 7.078433e+001
1.145972e+002 7.026958e+001
1.155614e+002 6.857949e+001
1.165256e+002 6.678419e+001
1.174899e+002 6.591994e+001
1.184541e+002 6.586436e+001
1.194183e+002 7.029463e+001
1.203826e+002 7.996349e+001
1.213468e+002 9.345306e+001
1.223110e+002 1.081374e+002
1.232753e+002 1.292575e+002
1.242395e+002 1.449875e+002
1.252037e+002 1.546096e+002
1.261680e+002 1.579285e+002
1.271322e+002 1.553773e+002
1.280964e+002 1.410350e+002
1.290607e+002 1.249626e+002
1.300249e+002 1.099149e+002
1.309891e+002 9.760245e+001
1.319534e+002 8.811470e+001
1.329176e+002 8.227888e+001
1.338818e+002 7.887193e+001
1.348461e+002 7.724295e+001
1.358103e+002 7.681377e+001
1.367745e+002 7.770727e+001
1.377388e+002 7.613245e+001
1.387030e+002 7.165026e+001
1.396672e+002 6.583466e+001
1.406315e+002 6.088119e+001
1.415957e+002 5.673366e+001
1.425599e+002 5.396782e+001
1.435242e+002 5.244227e+001
1.444884e+002 5.216537e+001
1.454526e+002 5.313023e+001
1.464169e+002 5.450982e+001
1.473811e+002 5.850718e+001
1.483453e+002 6.553959e+001
1.493096e+002 7.591943e+001
1.502738e+002 8.997410e+001
1.512380e+002 1.133425e+002
1.522023e+002 1.389514e+002
1.531665e+002 1.627816e+002
1.541307e+002 1.817873e+002
1.550950e+002 1.942648e+002
1.560592e+002 1.880861e+002
1.570234e+002 1.647623e+002
1.579877e+002 1.357420e+002
1.589519e+002 1.106688e+002
1.599161e+002 8.994806e+001
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1.618446e+002 6.401192e+001
1.628088e+002 5.741217e+001
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1.657015e+002 4.901889e+001
1.666658e+002 4.971529e+001
1.676300e+002 5.176641e+001
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1.782366e+002 5.878648e+001
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1.811293e+002 6.185283e+001
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1.936643e+002 1.879458e+002
1.946285e+002 1.633660e+002
1.955928e+002 1.383915e+002
1.965570e+002 1.139101e+002
1.975212e+002 9.408479e+001
1.984855e+002 8.051029e+001
1.994497e+002 6.953775e+001
2.004139e+002 6.072050e+001
2.013782e+002 5.398304e+001
2.023424e+002 4.924119e+001
2.033066e+002 4.815987e+001
2.042709e+002 4.749172e+001
2.052351e+002 4.569963e+001
2.061993e+002 4.207343e+001
2.071636e+002 3.849038e+001
2.081278e+002 3.697786e+001
2.090920e+002 3.637810e+001
2.100563e+002 3.582698e+001
2.110205e+002 3.460241e+001
2.119847e+002 3.289177e+001
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2.139132e+002 3.152839e+001
2.148774e+002 3.152748e+001
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2.187344e+002 3.028865e+001
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2.399475e+002 1.962605e+001
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2.438044e+002 1.956182e+001
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2.698387e+002 4.107651e+001
2.708030e+002 4.236045e+001
2.717672e+002 4.288165e+001
2.727314e+002 4.240775e+001
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2.833380e+002 3.046944e+001
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