#------------------------------------------------------------------------------
#$Date: 2018-01-29 12:24:48 +0200 (Mon, 29 Jan 2018) $
#$Revision: 366 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500096.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500096
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial Lead nitrate
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Merck 99% 7397'
_chemical_formula_structural     'Pb (N O3)2'
_chemical_formula_sum            'N2 O6 Pb'
_chemical_name_mineral           'Lead nitrate'
_chemical_name_systematic        'Pb (N O3)2'
_space_group_crystal_system      cubic
_space_group_IT_number           205
_space_group_name_Hall           '-P 2ac 2ab 3'
_space_group_name_H-M_alt        'P a -3'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.8586(2)
_cell_length_b                   7.8586(2)
_cell_length_c                   7.8586(2)
_cell_volume                     485.33(2)
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_solsa_sample.id                 CN-AA00-0085
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     9.916943e+001
_raman_measurement.range_max     3.500020e+003
_rod_data_source.file            PbNO32.rod
_rod_data_source.block           1000005
_rod_database.code               3500096
_raman_measurement.datetime_initiated 2017-10-17
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 2020897 COD http://www.crystallography.net/cod/2020897.html
;
 Entry contains the XRD analysis data of the same compound.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
9.916943e+001 1.554520e+004
1.001337e+002 1.536875e+004
1.010979e+002 1.468811e+004
1.020621e+002 1.321909e+004
1.030264e+002 1.132578e+004
1.039906e+002 9.745677e+003
1.049548e+002 8.762814e+003
1.059191e+002 8.007892e+003
1.068833e+002 7.478934e+003
1.078475e+002 7.152030e+003
1.088118e+002 6.966762e+003
1.097760e+002 6.909627e+003
1.107402e+002 6.940995e+003
1.117045e+002 7.054436e+003
1.126687e+002 7.241849e+003
1.136329e+002 7.504625e+003
1.145972e+002 7.847712e+003
1.155614e+002 8.250482e+003
1.165256e+002 8.689737e+003
1.174899e+002 9.144801e+003
1.184541e+002 9.636995e+003
1.194183e+002 1.009218e+004
1.203826e+002 1.054796e+004
1.213468e+002 1.096197e+004
1.223110e+002 1.125430e+004
1.232753e+002 1.138885e+004
1.242395e+002 1.137675e+004
1.252037e+002 1.119128e+004
1.261680e+002 1.085336e+004
1.271322e+002 1.044009e+004
1.280964e+002 9.920674e+003
1.290607e+002 9.401781e+003
1.300249e+002 8.900295e+003
1.309891e+002 8.436521e+003
1.319534e+002 8.039868e+003
1.329176e+002 7.766689e+003
1.338818e+002 7.595201e+003
1.348461e+002 7.528569e+003
1.358103e+002 7.567611e+003
1.367745e+002 7.729146e+003
1.377388e+002 7.986456e+003
1.387030e+002 8.359089e+003
1.396672e+002 8.789584e+003
1.406315e+002 9.199456e+003
1.415957e+002 9.635033e+003
1.425599e+002 9.962823e+003
1.435242e+002 1.016250e+004
1.444884e+002 1.025006e+004
1.454526e+002 1.027259e+004
1.464169e+002 1.019058e+004
1.473811e+002 1.010526e+004
1.483453e+002 1.002097e+004
1.493096e+002 9.950700e+003
1.502738e+002 9.920314e+003
1.512380e+002 9.976166e+003
1.522023e+002 1.009862e+004
1.531665e+002 1.029900e+004
1.541307e+002 1.057688e+004
1.550950e+002 1.091816e+004
1.560592e+002 1.122743e+004
1.570234e+002 1.153633e+004
1.579877e+002 1.179901e+004
1.589519e+002 1.198926e+004
1.599161e+002 1.216288e+004
1.608804e+002 1.209005e+004
1.618446e+002 1.174197e+004
1.628088e+002 1.117518e+004
1.637731e+002 1.045742e+004
1.647373e+002 9.498207e+003
1.657015e+002 8.548306e+003
1.666658e+002 7.633310e+003
1.676300e+002 6.776835e+003
1.685942e+002 5.994871e+003
1.695585e+002 5.349021e+003
1.705227e+002 4.793571e+003
1.714869e+002 4.311526e+003
1.724512e+002 3.892630e+003
1.734154e+002 3.532852e+003
1.743796e+002 3.222005e+003
1.753439e+002 2.950504e+003
1.763081e+002 2.708207e+003
1.772723e+002 2.490973e+003
1.782366e+002 2.302255e+003
1.792008e+002 2.136789e+003
1.801650e+002 1.991174e+003
1.811293e+002 1.861405e+003
1.820935e+002 1.746293e+003
1.830577e+002 1.649045e+003
1.840220e+002 1.565003e+003
1.849862e+002 1.490062e+003
1.859504e+002 1.422007e+003
1.869147e+002 1.359531e+003
1.878789e+002 1.302556e+003
1.888431e+002 1.250156e+003
1.898074e+002 1.201379e+003
1.907716e+002 1.156361e+003
1.917358e+002 1.115385e+003
1.927000e+002 1.078558e+003
1.936643e+002 1.043756e+003
1.946285e+002 1.010093e+003
1.955927e+002 9.788109e+002
1.965570e+002 9.502861e+002
1.975212e+002 9.211354e+002
1.984854e+002 8.872723e+002
1.994497e+002 8.583962e+002
2.004139e+002 8.377347e+002
2.013781e+002 8.249835e+002
2.023424e+002 8.107502e+002
2.033066e+002 7.944291e+002
2.042708e+002 7.757347e+002
2.052351e+002 7.526791e+002
2.061993e+002 7.243903e+002
2.071635e+002 6.979131e+002
2.081278e+002 6.806223e+002
2.090920e+002 6.671115e+002
2.100562e+002 6.538585e+002
2.110205e+002 6.378798e+002
2.119847e+002 6.195417e+002
2.129489e+002 6.012206e+002
2.139132e+002 5.837272e+002
2.148774e+002 5.676890e+002
2.158416e+002 5.535996e+002
2.168059e+002 5.413600e+002
2.177701e+002 5.305741e+002
2.187343e+002 5.214901e+002
2.196986e+002 5.125094e+002
2.206628e+002 5.014421e+002
2.216270e+002 4.867257e+002
2.225913e+002 4.724049e+002
2.235555e+002 4.593618e+002
2.245197e+002 4.479080e+002
2.254840e+002 4.378808e+002
2.264482e+002 4.286689e+002
2.274124e+002 4.202000e+002
2.283767e+002 4.137406e+002
2.293409e+002 4.091939e+002
2.303051e+002 4.055459e+002
2.312694e+002 3.985975e+002
2.322336e+002 3.889976e+002
2.331978e+002 3.808519e+002
2.341621e+002 3.759368e+002
2.351263e+002 3.744701e+002
2.360905e+002 3.721097e+002
2.370548e+002 3.684854e+002
2.380190e+002 3.645966e+002
2.389832e+002 3.607453e+002
2.399475e+002 3.568581e+002
2.409117e+002 3.525304e+002
2.418759e+002 3.477000e+002
2.428402e+002 3.432129e+002
2.438044e+002 3.394448e+002
2.447686e+002 3.364581e+002
2.457329e+002 3.329491e+002
2.466971e+002 3.282971e+002
2.476613e+002 3.233887e+002
2.486256e+002 3.190422e+002
2.495898e+002 3.159331e+002
2.505540e+002 3.139620e+002
2.515183e+002 3.112834e+002
2.524825e+002 3.077197e+002
2.534467e+002 3.037865e+002
2.544110e+002 3.004150e+002
2.553752e+002 2.990906e+002
2.563394e+002 2.952592e+002
2.573037e+002 2.875791e+002
2.582679e+002 2.782149e+002
2.592321e+002 2.705438e+002
2.601964e+002 2.665859e+002
2.611606e+002 2.627145e+002
2.621248e+002 2.577767e+002
2.630891e+002 2.519149e+002
2.640533e+002 2.456878e+002
2.650175e+002 2.398504e+002
2.659818e+002 2.347205e+002
2.669460e+002 2.305684e+002
2.679102e+002 2.270467e+002
2.688745e+002 2.234260e+002
2.698387e+002 2.178897e+002
2.708029e+002 2.108139e+002
2.717672e+002 2.050104e+002
2.727314e+002 2.014049e+002
2.736956e+002 1.997093e+002
2.746599e+002 1.966779e+002
2.756241e+002 1.897164e+002
2.765883e+002 1.837719e+002
2.775526e+002 1.806660e+002
2.785168e+002 1.803764e+002
2.794810e+002 1.793176e+002
2.804453e+002 1.753416e+002
2.814095e+002 1.712452e+002
2.823737e+002 1.679505e+002
2.833380e+002 1.656341e+002
2.843022e+002 1.633645e+002
2.852664e+002 1.599897e+002
2.862307e+002 1.563859e+002
2.871949e+002 1.532644e+002
2.881591e+002 1.510324e+002
2.891234e+002 1.496777e+002
2.900876e+002 1.482035e+002
2.910518e+002 1.463319e+002
2.920161e+002 1.438866e+002
2.929803e+002 1.406003e+002
2.939445e+002 1.360480e+002
2.949088e+002 1.332118e+002
2.958730e+002 1.332730e+002
2.968372e+002 1.334412e+002
2.978015e+002 1.316865e+002
2.987657e+002 1.268292e+002
2.997299e+002 1.226278e+002
3.006942e+002 1.209828e+002
3.016584e+002 1.202483e+002
3.026227e+002 1.191718e+002
3.035869e+002 1.168858e+002
3.045511e+002 1.142086e+002
3.055154e+002 1.127917e+002
3.064796e+002 1.123969e+002
3.074438e+002 1.124470e+002
3.084081e+002 1.122543e+002
3.093723e+002 1.114387e+002
3.103365e+002 1.107859e+002
3.113008e+002 1.106300e+002
3.122650e+002 1.101355e+002
3.132292e+002 1.082982e+002
3.141935e+002 1.043701e+002
3.151577e+002 1.016769e+002
3.161219e+002 1.007671e+002
3.170862e+002 1.003232e+002
3.180504e+002 9.879462e+001
3.190146e+002 9.470197e+001
3.199789e+002 9.175352e+001
3.209431e+002 9.267175e+001
3.219073e+002 9.540306e+001
3.228716e+002 9.738173e+001
3.238358e+002 9.590078e+001
3.248000e+002 9.158411e+001
3.257643e+002 8.774260e+001
3.267285e+002 8.455687e+001
3.276927e+002 8.205638e+001
3.286570e+002 8.014046e+001
3.296212e+002 7.876624e+001
3.305854e+002 7.756840e+001
3.315497e+002 7.665231e+001
3.325139e+002 7.592046e+001
3.334781e+002 7.529372e+001
3.344424e+002 7.543778e+001
3.354066e+002 7.488446e+001
3.363708e+002 7.251987e+001
3.373351e+002 6.931590e+001
3.382993e+002 6.680331e+001
3.392635e+002 6.655746e+001
3.402278e+002 6.686719e+001
3.411920e+002 6.651416e+001
3.421562e+002 6.561951e+001
3.431205e+002 6.452567e+001
3.440847e+002 6.366163e+001
3.450489e+002 6.282835e+001
3.460132e+002 6.170232e+001
3.469774e+002 6.031010e+001
3.479416e+002 5.880799e+001
3.489059e+002 5.748755e+001
3.498701e+002 5.685371e+001
3.508343e+002 5.620182e+001
3.517986e+002 5.486305e+001
3.527628e+002 5.339636e+001
3.537270e+002 5.298489e+001
3.546913e+002 5.490797e+001
3.556555e+002 5.574035e+001
3.566197e+002 5.455833e+001
3.575840e+002 5.236230e+001
3.585482e+002 5.076636e+001
3.595124e+002 5.165946e+001
3.604767e+002 5.274662e+001
3.614409e+002 5.111152e+001
3.624051e+002 4.733162e+001
3.633694e+002 4.316786e+001
3.643336e+002 4.130412e+001
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3.681905e+002 4.149304e+001
3.691548e+002 4.130715e+001
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3.710832e+002 4.286769e+001
3.720475e+002 4.284869e+001
3.730117e+002 4.239591e+001
3.739759e+002 4.167611e+001
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3.816898e+002 3.343298e+001
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3.865110e+002 2.837684e+001
3.874752e+002 2.702024e+001
3.884394e+002 2.624471e+001
3.894037e+002 2.591866e+001
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3.913321e+002 2.699810e+001
3.922964e+002 2.937979e+001
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4.511146e+002 1.012434e+001
4.520788e+002 9.824841e+000
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4.540073e+002 9.785254e+000
4.549715e+002 1.022527e+001
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4.569000e+002 1.151669e+001
4.578642e+002 1.200749e+001
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4.626854e+002 1.044991e+001
4.636496e+002 8.516199e+000
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loop_
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_rod_maintainer_comment.text
1 elmendili 2017-10-18T18:59:49+0300 'Chemical name changed'
