#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/00/3500096.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500096
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial Lead nitrate
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Merck 99% 7397'
_chemical_formula_structural     'Pb (N O3)2'
_chemical_formula_sum            'N2 O6 Pb'
_chemical_name_mineral           'Lead nitrate'
_chemical_name_systematic        'Pb (N O3)2'
_space_group_IT_number           205
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-P 2ac 2ab 3'
_symmetry_space_group_name_H-M   'P a -3'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   7.84
_cell_length_b                   7.84
_cell_length_c                   7.84
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_solsa_sample.id                 CN-AA00-0085
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 532
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     9.916943e+001
_raman_measurement.range_max     3.500020e+003
_rod_data_source.file            PbNO32.rod
_rod_data_source.block           1000005
_rod_database.code               3500096
_raman_measurement.datetime_initiated 2017-10-17
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 5910007 COD http://www.crystallography.net/cod/5910007.html
;
 The structure contains the XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
9.916943e+001 1.554520e+004
1.001337e+002 1.536875e+004
1.010979e+002 1.468811e+004
1.020621e+002 1.321909e+004
1.030264e+002 1.132578e+004
1.039906e+002 9.745677e+003
1.049548e+002 8.762814e+003
1.059191e+002 8.007892e+003
1.068833e+002 7.478934e+003
1.078475e+002 7.152030e+003
1.088118e+002 6.966762e+003
1.097760e+002 6.909627e+003
1.107402e+002 6.940995e+003
1.117045e+002 7.054436e+003
1.126687e+002 7.241849e+003
1.136329e+002 7.504625e+003
1.145972e+002 7.847712e+003
1.155614e+002 8.250482e+003
1.165256e+002 8.689737e+003
1.174899e+002 9.144801e+003
1.184541e+002 9.636995e+003
1.194183e+002 1.009218e+004
1.203826e+002 1.054796e+004
1.213468e+002 1.096197e+004
1.223110e+002 1.125430e+004
1.232753e+002 1.138885e+004
1.242395e+002 1.137675e+004
1.252037e+002 1.119128e+004
1.261680e+002 1.085336e+004
1.271322e+002 1.044009e+004
1.280964e+002 9.920674e+003
1.290607e+002 9.401781e+003
1.300249e+002 8.900295e+003
1.309891e+002 8.436521e+003
1.319534e+002 8.039868e+003
1.329176e+002 7.766689e+003
1.338818e+002 7.595201e+003
1.348461e+002 7.528569e+003
1.358103e+002 7.567611e+003
1.367745e+002 7.729146e+003
1.377388e+002 7.986456e+003
1.387030e+002 8.359089e+003
1.396672e+002 8.789584e+003
1.406315e+002 9.199456e+003
1.415957e+002 9.635033e+003
1.425599e+002 9.962823e+003
1.435242e+002 1.016250e+004
1.444884e+002 1.025006e+004
1.454526e+002 1.027259e+004
1.464169e+002 1.019058e+004
1.473811e+002 1.010526e+004
1.483453e+002 1.002097e+004
1.493096e+002 9.950700e+003
1.502738e+002 9.920314e+003
1.512380e+002 9.976166e+003
1.522023e+002 1.009862e+004
1.531665e+002 1.029900e+004
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1.550950e+002 1.091816e+004
1.560592e+002 1.122743e+004
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1.599161e+002 1.216288e+004
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1.628088e+002 1.117518e+004
1.637731e+002 1.045742e+004
1.647373e+002 9.498207e+003
1.657015e+002 8.548306e+003
1.666658e+002 7.633310e+003
1.676300e+002 6.776835e+003
1.685942e+002 5.994871e+003
1.695585e+002 5.349021e+003
1.705227e+002 4.793571e+003
1.714869e+002 4.311526e+003
1.724512e+002 3.892630e+003
1.734154e+002 3.532852e+003
1.743796e+002 3.222005e+003
1.753439e+002 2.950504e+003
1.763081e+002 2.708207e+003
1.772723e+002 2.490973e+003
1.782366e+002 2.302255e+003
1.792008e+002 2.136789e+003
1.801650e+002 1.991174e+003
1.811293e+002 1.861405e+003
1.820935e+002 1.746293e+003
1.830577e+002 1.649045e+003
1.840220e+002 1.565003e+003
1.849862e+002 1.490062e+003
1.859504e+002 1.422007e+003
1.869147e+002 1.359531e+003
1.878789e+002 1.302556e+003
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1.898074e+002 1.201379e+003
1.907716e+002 1.156361e+003
1.917358e+002 1.115385e+003
1.927000e+002 1.078558e+003
1.936643e+002 1.043756e+003
1.946285e+002 1.010093e+003
1.955927e+002 9.788109e+002
1.965570e+002 9.502861e+002
1.975212e+002 9.211354e+002
1.984854e+002 8.872723e+002
1.994497e+002 8.583962e+002
2.004139e+002 8.377347e+002
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2.023424e+002 8.107502e+002
2.033066e+002 7.944291e+002
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2.052351e+002 7.526791e+002
2.061993e+002 7.243903e+002
2.071635e+002 6.979131e+002
2.081278e+002 6.806223e+002
2.090920e+002 6.671115e+002
2.100562e+002 6.538585e+002
2.110205e+002 6.378798e+002
2.119847e+002 6.195417e+002
2.129489e+002 6.012206e+002
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loop_
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_rod_maintainer_comment.text
1 elmendili 2017-10-18T18:59:49+0300 'Chemical name changed'