#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500124.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500124
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial H3BO3
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Prolabo 99%'
_chemical_formula_structural     'B H3 O3'
_chemical_formula_sum            'B H3 O3'
_chemical_name_mineral           'Boric acid'
_chemical_name_systematic        'orthoboric acid'
_space_group_IT_number           145
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  'P 32'
_symmetry_space_group_name_H-M   'P 32'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   7.0453(4)
_cell_length_b                   7.0453(4)
_cell_length_c                   9.5608(7)
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 785
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     5.050586e+001
_raman_measurement.range_max     2.000186e+003
_rod_data_source.file            H3BO3.rod
_rod_data_source.block           1000005
_rod_database.code               3500124
_solsa_sample.id                 CN-AA00-0131
_raman_measurement.datetime_initiated 2017-10-10
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 2013259 COD http://www.crystallography.net/cod/2013259.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.050586e+001 4.309940e+000
5.147009e+001 3.368736e+000
5.243433e+001 2.380753e+000
5.339856e+001 1.548309e+000
5.436279e+001 9.995270e-001
5.532703e+001 7.263527e-001
5.629126e+001 6.510391e-001
5.725549e+001 9.659882e-001
5.821973e+001 1.412750e+000
5.918396e+001 1.609810e+000
6.014819e+001 1.386005e+000
6.111243e+001 9.328613e-001
6.207666e+001 4.896011e-001
6.304089e+001 -2.647400e-003
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6.496936e+001 -1.411629e-001
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6.786206e+001 1.441696e+000
6.882629e+001 1.605591e+000
6.979053e+001 1.826187e+000
7.075476e+001 2.213074e+000
7.171899e+001 2.757767e+000
7.268323e+001 3.404079e+000
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9.968176e+001 4.387210e+001
1.006460e+002 4.928205e+001
1.016102e+002 5.379480e+001
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1.295730e+002 9.485840e+001
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