#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500139.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500139
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial PbO
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial Alfa Aesar 99.9%'
_chemical_formula_structural     'O Pb'
_chemical_formula_sum            'O Pb'
_chemical_name_mineral           Litharge
_chemical_name_systematic        'Plumbous oxide'
_space_group_IT_number           57
_symmetry_space_group_name_Hall  '-P 2a 2ab'
_symmetry_space_group_name_H-M   'P b m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   5.891
_cell_length_b                   4.775
_cell_length_c                   5.489
_raman_determination_method      experimental
_[local]_chemical_compound_color yelow
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 785
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     5.050586e+001
_raman_measurement.range_max     2.000186e+003
_rod_data_source.file            PbO.rod
_rod_data_source.block           1000005
_rod_database.code               3500139
_solsa_sample.id                 CN-AA00-0147
_raman_measurement.datetime_initiated 2017-10-10
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9008960 COD http://www.crystallography.net/cod/9008960.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.050586e+001 5.194025e+002
5.147009e+001 5.368922e+002
5.243433e+001 5.404546e+002
5.339856e+001 5.382562e+002
5.436279e+001 5.316529e+002
5.532703e+001 5.211439e+002
5.629126e+001 5.145704e+002
5.725549e+001 5.160032e+002
5.821973e+001 5.234223e+002
5.918396e+001 5.337618e+002
6.014819e+001 5.448854e+002
6.111243e+001 5.593055e+002
6.207666e+001 5.722688e+002
6.304089e+001 5.669431e+002
6.400513e+001 5.961530e+002
6.496936e+001 6.923204e+002
6.593359e+001 8.499799e+002
6.689783e+001 1.073109e+003
6.786206e+001 1.442421e+003
6.882629e+001 1.943482e+003
6.979053e+001 2.312252e+003
7.075476e+001 2.419523e+003
7.171899e+001 2.327709e+003
7.268323e+001 2.141037e+003
7.364746e+001 1.749371e+003
7.461169e+001 1.305606e+003
7.557593e+001 1.037153e+003
7.654016e+001 9.696061e+002
7.750439e+001 1.039945e+003
7.846863e+001 1.204937e+003
7.943286e+001 1.459373e+003
8.039709e+001 1.762932e+003
8.136133e+001 2.076961e+003
8.232556e+001 2.410372e+003
8.328979e+001 2.853726e+003
8.425403e+001 3.622628e+003
8.521826e+001 4.451261e+003
8.618250e+001 4.891820e+003
8.714673e+001 4.761196e+003
8.811096e+001 4.274496e+003
8.907520e+001 3.584765e+003
9.003943e+001 2.615954e+003
9.100366e+001 1.688755e+003
9.196790e+001 1.122436e+003
9.293213e+001 8.840150e+002
9.389636e+001 7.516424e+002
9.486060e+001 6.724972e+002
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9.678906e+001 6.192001e+002
9.775330e+001 6.115093e+002
9.871753e+001 6.132101e+002
9.968176e+001 6.170580e+002
1.006460e+002 6.247052e+002
1.016102e+002 6.335814e+002
1.025745e+002 6.416686e+002
1.035387e+002 6.489573e+002
1.045029e+002 6.565593e+002
1.054672e+002 6.658652e+002
1.064314e+002 6.767100e+002
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1.141453e+002 6.904990e+002
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1.160737e+002 6.917874e+002
1.170380e+002 6.922533e+002
1.180022e+002 6.963507e+002
1.189664e+002 7.068605e+002
1.199307e+002 7.249264e+002
1.208949e+002 7.445237e+002
1.218591e+002 7.638608e+002
1.228234e+002 7.854905e+002
1.237876e+002 8.106766e+002
1.247518e+002 8.395859e+002
1.257161e+002 8.745096e+002
1.266803e+002 9.208016e+002
1.276445e+002 9.613838e+002
1.286088e+002 1.030121e+003
1.295730e+002 1.105936e+003
1.305372e+002 1.212653e+003
1.315015e+002 1.374550e+003
1.324657e+002 1.579836e+003
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1.343942e+002 2.440604e+003
1.353584e+002 3.465757e+003
1.363226e+002 4.768899e+003
1.372869e+002 6.540068e+003
1.382511e+002 8.696060e+003
1.392153e+002 1.075788e+004
1.401796e+002 1.206723e+004
1.411438e+002 1.205452e+004
1.421080e+002 1.204020e+004
1.430723e+002 1.215469e+004
1.440365e+002 1.222825e+004
1.450007e+002 1.212750e+004
1.459650e+002 1.180273e+004
1.469292e+002 1.122638e+004
1.478934e+002 1.024556e+004
1.488577e+002 8.200595e+003
1.498219e+002 6.344370e+003
1.507861e+002 4.927892e+003
1.517504e+002 3.928243e+003
1.527146e+002 3.205189e+003
1.536788e+002 2.673607e+003
1.546431e+002 2.366814e+003
1.556073e+002 2.108803e+003
1.565715e+002 1.916359e+003
1.575358e+002 1.760304e+003
1.585000e+002 1.630178e+003
1.594642e+002 1.523911e+003
1.604285e+002 1.436229e+003
1.613927e+002 1.360553e+003
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1.633212e+002 1.244564e+003
1.642854e+002 1.202489e+003
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1.662139e+002 1.135986e+003
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1.691066e+002 1.046941e+003
1.700708e+002 1.013240e+003
1.710350e+002 9.784338e+002
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1.729635e+002 9.100824e+002
1.739277e+002 8.758915e+002
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2.144256e+002 5.932083e+002
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2.163540e+002 5.877605e+002
2.173183e+002 5.859014e+002
2.182825e+002 5.838953e+002
2.192467e+002 5.796732e+002
2.202110e+002 5.735260e+002
2.211752e+002 5.649138e+002
2.221394e+002 5.514069e+002
2.231037e+002 5.321827e+002
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2.713153e+002 1.077734e+003
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2.780649e+002 1.921773e+003
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2.809576e+002 2.622374e+003
2.819219e+002 2.919250e+003
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2.838503e+002 3.620616e+003
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2.915642e+002 4.022248e+003
2.925284e+002 3.685995e+003
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2.963854e+002 2.381209e+003
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3.069920e+002 9.758544e+002
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3.118131e+002 7.479595e+002
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