#------------------------------------------------------------------------------
#$Date: 2018-01-05 14:55:17 +0200 (Fri, 05 Jan 2018) $
#$Revision: 361 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500140.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500140
loop_
_publ_author_name
'El Mendili, Y'
_publ_section_title
;
 Raman spectrum of commercial PbO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial RP NORMAPUR AR 98%'
_chemical_formula_structural     'O2 Pb'
_chemical_formula_sum            'O2 Pb'
_chemical_name_mineral           Plattnerite
_chemical_name_systematic        'Lead(IV) oxide'
_space_group_IT_number           201
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  'P 2 2 3 -1n'
_symmetry_space_group_name_H-M   'P n -3 :1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   5.38
_cell_length_b                   5.38
_cell_length_c                   5.38
_raman_determination_method      experimental
_[local]_chemical_compound_color black
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 785
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 30
_raman_measurement.range_min     3.507813e+001
_raman_measurement.range_max     2.000186e+003
_rod_data_source.file            PbO2.rod
_rod_data_source.block           1000005
_rod_database.code               3500140
_solsa_sample.id                 CN-AA00-0148
_raman_measurement.datetime_initiated 2017-10-10
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1010382 COD http://www.crystallography.net/cod/1010382.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
3.507813e+001 6.082625e+001
3.604236e+001 6.107600e+001
3.700659e+001 6.358826e+001
3.797083e+001 6.889674e+001
3.893506e+001 7.681342e+001
3.989929e+001 8.591813e+001
4.086353e+001 8.640929e+001
4.182776e+001 7.775963e+001
4.279199e+001 7.615014e+001
4.375623e+001 8.192907e+001
4.472046e+001 9.380920e+001
4.568469e+001 1.098693e+002
4.664893e+001 1.376619e+002
4.761316e+001 1.669755e+002
4.857739e+001 1.831437e+002
4.954163e+001 1.836598e+002
5.050586e+001 1.741622e+002
5.147009e+001 1.562291e+002
5.243433e+001 1.288134e+002
5.339856e+001 1.057553e+002
5.436279e+001 9.416621e+001
5.532703e+001 9.382312e+001
5.629126e+001 1.028386e+002
5.725549e+001 1.280059e+002
5.821973e+001 1.604962e+002
5.918396e+001 1.866826e+002
6.014819e+001 2.076187e+002
6.111243e+001 2.201507e+002
6.207666e+001 2.167314e+002
6.304089e+001 1.918447e+002
6.400513e+001 1.614158e+002
6.496936e+001 1.377651e+002
6.593359e+001 1.206182e+002
6.689783e+001 1.067729e+002
6.786206e+001 9.456129e+001
6.882629e+001 8.391349e+001
6.979053e+001 7.541593e+001
7.075476e+001 6.976231e+001
7.171899e+001 6.655446e+001
7.268323e+001 6.494668e+001
7.364746e+001 6.563625e+001
7.461169e+001 6.746078e+001
7.557593e+001 6.879056e+001
7.654016e+001 6.947997e+001
7.750439e+001 6.967960e+001
7.846863e+001 6.985364e+001
7.943286e+001 7.015309e+001
8.039709e+001 7.000519e+001
8.136133e+001 6.932507e+001
8.232556e+001 6.803129e+001
8.328979e+001 6.549281e+001
8.425403e+001 6.053366e+001
8.521826e+001 5.446205e+001
8.618250e+001 4.962748e+001
8.714673e+001 4.686697e+001
8.811096e+001 4.523766e+001
8.907520e+001 4.332051e+001
9.003943e+001 4.065993e+001
9.100366e+001 3.905038e+001
9.196790e+001 4.065780e+001
9.293213e+001 4.513003e+001
9.389636e+001 5.000381e+001
9.486060e+001 5.373109e+001
9.582483e+001 5.694996e+001
9.678906e+001 6.174415e+001
9.775330e+001 6.874905e+001
9.871753e+001 7.816183e+001
9.968177e+001 8.922070e+001
1.006460e+002 1.007223e+002
1.016102e+002 1.146693e+002
1.025745e+002 1.315175e+002
1.035387e+002 1.510492e+002
1.045029e+002 1.762633e+002
1.054672e+002 2.087415e+002
1.064314e+002 2.474817e+002
1.073956e+002 2.986273e+002
1.083599e+002 3.672075e+002
1.093241e+002 4.486865e+002
1.102883e+002 5.393379e+002
1.112526e+002 6.429362e+002
1.122168e+002 7.484919e+002
1.131810e+002 8.292043e+002
1.141453e+002 8.942648e+002
1.151095e+002 9.316843e+002
1.160737e+002 9.313212e+002
1.170380e+002 8.957308e+002
1.180022e+002 8.377278e+002
1.189664e+002 7.620363e+002
1.199307e+002 6.636197e+002
1.208949e+002 5.730433e+002
1.218591e+002 4.880112e+002
1.228234e+002 4.121485e+002
1.237876e+002 3.498906e+002
1.247518e+002 3.027323e+002
1.257161e+002 2.677641e+002
1.266803e+002 2.398295e+002
1.276445e+002 2.197915e+002
1.286088e+002 2.049728e+002
1.295730e+002 1.962596e+002
1.305372e+002 1.926974e+002
1.315015e+002 1.926566e+002
1.324657e+002 1.953417e+002
1.334299e+002 2.008366e+002
1.343942e+002 2.081534e+002
1.353584e+002 2.187393e+002
1.363226e+002 2.295172e+002
1.372869e+002 2.394821e+002
1.382511e+002 2.482505e+002
1.392153e+002 2.554827e+002
1.401796e+002 2.610209e+002
1.411438e+002 2.673248e+002
1.421080e+002 2.676809e+002
1.430723e+002 2.610266e+002
1.440365e+002 2.496496e+002
1.450007e+002 2.352113e+002
1.459650e+002 2.182714e+002
1.469292e+002 1.992955e+002
1.478934e+002 1.804386e+002
1.488577e+002 1.597471e+002
1.498219e+002 1.409463e+002
1.507861e+002 1.249184e+002
1.517504e+002 1.114905e+002
1.527146e+002 1.000088e+002
1.536788e+002 9.024943e+001
1.546431e+002 8.261329e+001
1.556073e+002 7.505674e+001
1.565715e+002 6.628142e+001
1.575358e+002 5.839249e+001
1.585000e+002 5.289723e+001
1.594642e+002 5.033795e+001
1.604285e+002 4.915533e+001
1.613927e+002 4.690681e+001
1.623569e+002 4.302537e+001
1.633212e+002 3.938368e+001
1.642854e+002 3.675443e+001
1.652496e+002 3.468961e+001
1.662139e+002 3.258006e+001
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1.700708e+002 2.324525e+001
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1.729635e+002 1.777574e+001
1.739277e+002 1.544730e+001
1.748920e+002 1.392281e+001
1.758562e+002 1.310204e+001
1.768204e+002 1.229567e+001
1.777847e+002 1.099648e+001
1.787489e+002 9.717438e+000
1.797132e+002 9.483467e+000
1.806774e+002 1.180625e+001
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1.826059e+002 1.422647e+001
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1.845343e+002 1.023031e+001
1.854986e+002 8.775475e+000
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1.874270e+002 7.511047e+000
1.883913e+002 6.125397e+000
1.893555e+002 4.778336e+000
1.903197e+002 4.180046e+000
1.912840e+002 4.502052e+000
1.922482e+002 5.331230e+000
1.932124e+002 5.930634e+000
1.941767e+002 6.311417e+000
1.951409e+002 6.296356e+000
1.961051e+002 5.360756e+000
1.970694e+002 4.092972e+000
1.980336e+002 3.295792e+000
1.989978e+002 3.461296e+000
1.999621e+002 4.459236e+000
2.009263e+002 5.215057e+000
2.018905e+002 5.012711e+000
2.028548e+002 5.157127e+000
2.038190e+002 6.125969e+000
2.047832e+002 7.794144e+000
2.057475e+002 9.677383e+000
2.067117e+002 1.147325e+001
2.076759e+002 1.321425e+001
2.086402e+002 1.453721e+001
2.096044e+002 1.501457e+001
2.105686e+002 1.521719e+001
2.115329e+002 1.541366e+001
2.124971e+002 1.564561e+001
2.134613e+002 1.600710e+001
2.144256e+002 1.661356e+001
2.153898e+002 1.746558e+001
2.163540e+002 1.837280e+001
2.173183e+002 1.947527e+001
2.182825e+002 2.059483e+001
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2.202110e+002 2.192719e+001
2.211752e+002 2.213554e+001
2.221394e+002 2.165838e+001
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2.250321e+002 1.973114e+001
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2.337102e+002 1.800053e+001
2.346745e+002 1.778398e+001
2.356387e+002 1.672086e+001
2.366029e+002 1.530523e+001
2.375672e+002 1.412685e+001
2.385314e+002 1.350158e+001
2.394956e+002 1.337630e+001
2.404599e+002 1.339256e+001
2.414241e+002 1.369335e+001
2.423883e+002 1.404723e+001
2.433526e+002 1.453507e+001
2.443168e+002 1.497054e+001
2.452810e+002 1.499045e+001
2.462453e+002 1.403259e+001
2.472095e+002 1.220596e+001
2.481737e+002 1.098907e+001
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2.539591e+002 1.103953e+001
2.549234e+002 9.486954e+000
2.558876e+002 8.715630e+000
2.568518e+002 9.607910e+000
2.578160e+002 1.153642e+001
2.587803e+002 1.242117e+001
2.597445e+002 1.129552e+001
2.607087e+002 1.010823e+001
2.616730e+002 9.947090e+000
2.626372e+002 1.062375e+001
2.636014e+002 1.129172e+001
2.645657e+002 1.126787e+001
2.655299e+002 1.036367e+001
2.664941e+002 9.842842e+000
2.674584e+002 1.008112e+001
2.684226e+002 1.049266e+001
2.693868e+002 1.073920e+001
2.703511e+002 1.082819e+001
2.713153e+002 1.103719e+001
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2.751722e+002 1.463744e+001
2.761365e+002 1.505282e+001
2.771007e+002 1.544013e+001
2.780649e+002 1.589246e+001
2.790292e+002 1.643248e+001
2.799934e+002 1.704762e+001
2.809576e+002 1.774854e+001
2.819219e+002 1.861870e+001
2.828861e+002 1.974094e+001
2.838503e+002 2.097218e+001
2.848146e+002 2.195456e+001
2.857788e+002 2.219264e+001
2.867430e+002 2.252765e+001
2.877073e+002 2.376991e+001
2.886715e+002 2.583176e+001
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2.906000e+002 2.904075e+001
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2.934927e+002 3.073811e+001
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2.954212e+002 3.275231e+001
2.963854e+002 3.297441e+001
2.973496e+002 3.280505e+001
2.983139e+002 3.234776e+001
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