#------------------------------------------------------------------------------
#$Date: 2017-11-22 18:04:19 +0200 (Wed, 22 Nov 2017) $
#$Revision: 347 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500149.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500149
loop_
_publ_author_name
'El Mendili, Y'
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder Alfa Aesar 99.9%'
_chemical_formula_structural     'O5 V2'
_chemical_formula_sum            'O5 V2'
_chemical_name_mineral           'Vanadium oxide'
_chemical_name_systematic        'Vanadium oxide'
_space_group_IT_number           31
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac -2'
_symmetry_space_group_name_H-M   'P m n 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.503
_cell_length_b                   4.369
_cell_length_c                   3.557
_raman_determination_method      experimental
_[local]_chemical_compound_color Brown
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.name   DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 785
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 180
_raman_measurement.range_min     5.050586e+001
_raman_measurement.range_max     2.000186e+003
_rod_data_source.file            Shcherbianite.rod
_rod_data_source.block           1000005
_rod_database.code               3500149
_solsa_sample.id                 CN-AA00-0109
_raman_measurement.datetime_initiated 2017-10-10
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1011291 COD http://www.crystallography.net/cod/1011291.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.050586e+001 9.871214e+001
5.147009e+001 9.790884e+001
5.243433e+001 9.731168e+001
5.339856e+001 9.701253e+001
5.436279e+001 9.723761e+001
5.532703e+001 9.795052e+001
5.629126e+001 9.860803e+001
5.725549e+001 9.914256e+001
5.821973e+001 9.945663e+001
5.918396e+001 9.947815e+001
6.014819e+001 9.861568e+001
6.111243e+001 9.771452e+001
6.207666e+001 9.831572e+001
6.304089e+001 1.011287e+002
6.400513e+001 1.043855e+002
6.496936e+001 1.065378e+002
6.593359e+001 1.075871e+002
6.689783e+001 1.081880e+002
6.786206e+001 1.084320e+002
6.882629e+001 1.083174e+002
6.979053e+001 1.084471e+002
7.075476e+001 1.092154e+002
7.171899e+001 1.104406e+002
7.268323e+001 1.116958e+002
7.364746e+001 1.124745e+002
7.461169e+001 1.132098e+002
7.557593e+001 1.146695e+002
7.654016e+001 1.170373e+002
7.750439e+001 1.195457e+002
7.846863e+001 1.216555e+002
7.943286e+001 1.234723e+002
8.039709e+001 1.255462e+002
8.136133e+001 1.280415e+002
8.232556e+001 1.309628e+002
8.328979e+001 1.343606e+002
8.425403e+001 1.377587e+002
8.521826e+001 1.419698e+002
8.618250e+001 1.481301e+002
8.714673e+001 1.561080e+002
8.811096e+001 1.662820e+002
8.907520e+001 1.773447e+002
9.003943e+001 1.875291e+002
9.100366e+001 2.042901e+002
9.196790e+001 2.316581e+002
9.293213e+001 2.673678e+002
9.389636e+001 3.215737e+002
9.486060e+001 4.112679e+002
9.582483e+001 5.261361e+002
9.678906e+001 6.363132e+002
9.775330e+001 7.476427e+002
9.871753e+001 8.351375e+002
9.968176e+001 8.620335e+002
1.006460e+002 7.898839e+002
1.016102e+002 6.824811e+002
1.025745e+002 5.796799e+002
1.035387e+002 4.807984e+002
1.045029e+002 3.970305e+002
1.054672e+002 3.425934e+002
1.064314e+002 3.165062e+002
1.073956e+002 3.002119e+002
1.083599e+002 2.936087e+002
1.093241e+002 2.941849e+002
1.102883e+002 2.979545e+002
1.112526e+002 3.042147e+002
1.122168e+002 3.126791e+002
1.131810e+002 3.222589e+002
1.141453e+002 3.313888e+002
1.151095e+002 3.427636e+002
1.160737e+002 3.576059e+002
1.170380e+002 3.758075e+002
1.180022e+002 3.967971e+002
1.189664e+002 4.197827e+002
1.199307e+002 4.447182e+002
1.208949e+002 4.745333e+002
1.218591e+002 5.081610e+002
1.228234e+002 5.470895e+002
1.237876e+002 5.914327e+002
1.247518e+002 6.409880e+002
1.257161e+002 6.985723e+002
1.266803e+002 7.710865e+002
1.276445e+002 8.508083e+002
1.286088e+002 9.517090e+002
1.295730e+002 1.064644e+003
1.305372e+002 1.199868e+003
1.315015e+002 1.373802e+003
1.324657e+002 1.593613e+003
1.334299e+002 1.858402e+003
1.343942e+002 2.207675e+003
1.353584e+002 2.641608e+003
1.363226e+002 3.137301e+003
1.372869e+002 3.747507e+003
1.382511e+002 4.451047e+003
1.392153e+002 5.125356e+003
1.401796e+002 5.610690e+003
1.411438e+002 5.859291e+003
1.421080e+002 5.950968e+003
1.430723e+002 5.907454e+003
1.440365e+002 5.719626e+003
1.450007e+002 5.350380e+003
1.459650e+002 4.765865e+003
1.469292e+002 4.014712e+003
1.478934e+002 3.342876e+003
1.488577e+002 2.759510e+003
1.498219e+002 2.257250e+003
1.507861e+002 1.848295e+003
1.517504e+002 1.523854e+003
1.527146e+002 1.261846e+003
1.536788e+002 1.049353e+003
1.546431e+002 8.927971e+002
1.556073e+002 7.595704e+002
1.565715e+002 6.569802e+002
1.575358e+002 5.723278e+002
1.585000e+002 5.013202e+002
1.594642e+002 4.432022e+002
1.604285e+002 3.950029e+002
1.613927e+002 3.531436e+002
1.623569e+002 3.184395e+002
1.633212e+002 2.879377e+002
1.642854e+002 2.605970e+002
1.652496e+002 2.363548e+002
1.662139e+002 2.154295e+002
1.671781e+002 1.985909e+002
1.681423e+002 1.852193e+002
1.691066e+002 1.733649e+002
1.700708e+002 1.632396e+002
1.710350e+002 1.544117e+002
1.719993e+002 1.461214e+002
1.729635e+002 1.382780e+002
1.739277e+002 1.319158e+002
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1.768204e+002 1.253577e+002
1.777847e+002 1.238840e+002
1.787489e+002 1.229682e+002
1.797132e+002 1.243298e+002
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1.854986e+002 1.702018e+002
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1.893555e+002 2.694938e+002
1.903197e+002 3.033896e+002
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1.922482e+002 3.719566e+002
1.932124e+002 3.952267e+002
1.941767e+002 4.072467e+002
1.951409e+002 4.093025e+002
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1.970694e+002 3.789812e+002
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1.989978e+002 3.180832e+002
1.999621e+002 2.788472e+002
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2.028548e+002 1.788779e+002
2.038190e+002 1.553285e+002
2.047832e+002 1.372009e+002
2.057475e+002 1.226565e+002
2.067117e+002 1.106013e+002
2.076759e+002 1.012212e+002
2.086402e+002 9.266876e+001
2.096044e+002 8.494444e+001
2.105686e+002 7.798373e+001
2.115329e+002 7.187089e+001
2.124971e+002 6.663794e+001
2.134613e+002 6.223799e+001
2.144256e+002 5.865259e+001
2.153898e+002 5.587514e+001
2.163540e+002 5.380624e+001
2.173183e+002 5.301909e+001
2.182825e+002 5.289119e+001
2.192467e+002 5.237022e+001
2.202110e+002 5.058557e+001
2.211752e+002 4.872434e+001
2.221394e+002 4.806689e+001
2.231037e+002 4.866471e+001
2.240679e+002 4.990511e+001
2.250321e+002 5.155311e+001
2.259964e+002 5.381753e+001
2.269606e+002 5.537943e+001
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2.317818e+002 5.522137e+001
2.327460e+002 5.478416e+001
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2.481737e+002 5.197253e+001
2.491380e+002 5.242318e+001
2.501022e+002 5.307062e+001
2.510664e+002 5.416724e+001
2.520307e+002 5.563902e+001
2.529949e+002 5.785646e+001
2.539591e+002 6.159016e+001
2.549234e+002 6.653064e+001
2.558876e+002 7.098314e+001
2.568518e+002 7.406096e+001
2.578160e+002 7.628595e+001
2.587803e+002 7.949056e+001
2.597445e+002 8.311443e+001
2.607087e+002 8.809145e+001
2.616730e+002 9.508470e+001
2.626372e+002 1.039392e+002
2.636014e+002 1.139845e+002
2.645657e+002 1.245868e+002
2.655299e+002 1.355487e+002
2.664941e+002 1.485136e+002
2.674584e+002 1.613596e+002
2.684226e+002 1.777718e+002
2.693868e+002 1.987720e+002
2.703511e+002 2.249139e+002
2.713153e+002 2.568983e+002
2.722795e+002 2.939512e+002
2.732438e+002 3.337480e+002
2.742080e+002 3.872578e+002
2.751722e+002 4.596558e+002
2.761365e+002 5.443525e+002
2.771007e+002 6.416012e+002
2.780649e+002 7.558088e+002
2.790292e+002 8.706313e+002
2.799934e+002 9.751463e+002
2.809576e+002 1.070231e+003
2.819219e+002 1.140658e+003
2.828861e+002 1.178563e+003
2.838503e+002 1.183228e+003
2.848146e+002 1.162843e+003
2.857788e+002 1.106913e+003
2.867430e+002 1.033666e+003
2.877073e+002 9.503962e+002
2.886715e+002 8.588575e+002
2.896357e+002 7.673648e+002
2.906000e+002 6.818240e+002
2.915642e+002 6.010629e+002
2.925284e+002 5.330407e+002
2.934927e+002 4.782704e+002
2.944569e+002 4.342589e+002
2.954211e+002 4.015527e+002
2.963854e+002 3.794322e+002
2.973496e+002 3.644359e+002
2.983138e+002 3.528784e+002
2.992781e+002 3.456230e+002
3.002423e+002 3.392754e+002
3.012065e+002 3.358525e+002
3.021708e+002 3.318932e+002
3.031350e+002 3.245944e+002
3.040992e+002 3.128405e+002
3.050635e+002 2.983153e+002
3.060277e+002 2.822268e+002
3.069920e+002 2.646557e+002
3.079562e+002 2.472822e+002
3.089204e+002 2.307623e+002
3.098847e+002 2.151054e+002
3.108489e+002 2.000573e+002
3.118131e+002 1.852767e+002
3.127774e+002 1.713955e+002
3.137416e+002 1.588945e+002
3.147058e+002 1.477890e+002
3.156701e+002 1.377695e+002
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3.185628e+002 1.122976e+002
3.195270e+002 1.050435e+002
3.204912e+002 9.834053e+001
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3.224197e+002 8.667372e+001
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