#------------------------------------------------------------------------------ #$Date: 2018-02-01 15:36:29 +0200 (Thu, 01 Feb 2018) $ #$Revision: 373 $ #$URL: svn://172.16.1.111/rod/cif/3/50/01/3500149.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500149 loop_ _publ_author_name 'El Mendili, Y' _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder Alfa Aesar 99.9%' _chemical_formula_structural 'O5 V2' _chemical_formula_sum 'O5 V2' _chemical_name_mineral Shcherbianite _chemical_name_systematic 'Vanadium oxide' _space_group_IT_number 31 _symmetry_cell_setting orthorhombic _symmetry_space_group_name_Hall 'P 2ac -2' _symmetry_space_group_name_H-M 'P m n 21' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 11.503 _cell_length_b 4.369 _cell_length_c 3.557 _raman_determination_method experimental _[local]_chemical_compound_color Brown _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 785 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 3 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 180 _raman_measurement.range_min 5.050586e+001 _raman_measurement.range_max 2.000186e+003 _rod_data_source.file 3500149.rod _rod_data_source.block 3500149 _rod_database.code 3500149 _solsa_sample.id CN-AA00-0109 _raman_measurement.datetime_initiated 2017-10-10 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1011291 COD http://www.crystallography.net/cod/1011291.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 5.050586e+001 9.871214e+001 5.147009e+001 9.790884e+001 5.243433e+001 9.731168e+001 5.339856e+001 9.701253e+001 5.436279e+001 9.723761e+001 5.532703e+001 9.795052e+001 5.629126e+001 9.860803e+001 5.725549e+001 9.914256e+001 5.821973e+001 9.945663e+001 5.918396e+001 9.947815e+001 6.014819e+001 9.861568e+001 6.111243e+001 9.771452e+001 6.207666e+001 9.831572e+001 6.304089e+001 1.011287e+002 6.400513e+001 1.043855e+002 6.496936e+001 1.065378e+002 6.593359e+001 1.075871e+002 6.689783e+001 1.081880e+002 6.786206e+001 1.084320e+002 6.882629e+001 1.083174e+002 6.979053e+001 1.084471e+002 7.075476e+001 1.092154e+002 7.171899e+001 1.104406e+002 7.268323e+001 1.116958e+002 7.364746e+001 1.124745e+002 7.461169e+001 1.132098e+002 7.557593e+001 1.146695e+002 7.654016e+001 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1.979937e+003 9.581470e+000 1.980901e+003 1.035544e+001 1.981865e+003 1.111235e+001 1.982830e+003 1.035464e+001 1.983794e+003 9.062195e+000 1.984758e+003 9.490149e+000 1.985722e+003 1.091626e+001 1.986687e+003 1.131025e+001 1.987651e+003 1.076127e+001 1.988615e+003 1.004681e+001 1.989579e+003 9.457739e+000 1.990544e+003 1.009188e+001 1.991508e+003 1.196359e+001 1.992472e+003 1.247479e+001 1.993436e+003 1.197230e+001 1.994401e+003 1.210220e+001 1.995365e+003 1.298104e+001 1.996329e+003 1.287375e+001 1.997293e+003 1.172908e+001 1.998257e+003 1.115298e+001 1.999222e+003 1.124550e+001 2.000186e+003 1.155973e+001 loop_ _rod_maintainer_comment.id _rod_maintainer_comment.author _rod_maintainer_comment.date _rod_maintainer_comment.text 1 elmendili 2018-02-01T15:36:28+0200 '_chemical_name_mineral was changed'