#------------------------------------------------------------------------------
#$Date: 2018-07-20 15:02:54 +0300 (Fri, 20 Jul 2018) $
#$Revision: 1269 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500150.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500150
loop_
_publ_author_name
'El Mendili, Y.'
_publ_section_title
;
 Raman spectrum of commercial tungsten(IV) oxide
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2017
_chemical_compound_source        'commercial powder C STARCK BERLIN'
_chemical_formula_structural     'W O2'
_chemical_formula_sum            'O2 W'
_chemical_name_mineral           'Tungsten dioxide'
_chemical_name_systematic        'tungsten(IV) oxide'
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 120.678(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   5.5769(2)
_cell_length_b                   4.8986(1)
_cell_length_c                   5.6644(2)
_cell_volume                     133.089(7)
_cod_original_formula_sum        'W O2'
_raman_determination_method      experimental
_[local]_chemical_compound_color Black
_[local]_chemical_compound_state Solid
_raman_measurement_device.location ENSICAEN
_raman_measurement_device.company 'Thermo Scientific'
_raman_measurement_device.model  DXR
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 20
_raman_measurement_device.microscope_numerical_aperture 0.25
_raman_measurement_device.excitation_laser_type other
_raman_measurement_device.excitation_laser_wavelength 785
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 3
_raman_measurement_device.power_on_sample 1
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1.3
_raman_measurement_device.diffraction_grating 900
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 180
_raman_measurement.range_min     5.050586e+001
_raman_measurement.range_max     2.000186e+003
_rod_data_source.file            wo2.rod
_rod_data_source.block           1000005
_rod_database.code               3500150
_solsa_sample.id                 CN-AA00-0110
_raman_measurement.datetime_initiated 2017-10-10
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 neon_lamp
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1548686 COD http://www.crystallography.net/cod/1548686.html
;
 Entry contains the XRD analysis data of the same compound.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
5.050586e+001 4.985692e+001
5.147009e+001 6.630171e+001
5.243433e+001 8.470509e+001
5.339856e+001 1.015755e+002
5.436279e+001 1.152879e+002
5.532703e+001 1.258761e+002
5.629126e+001 1.332453e+002
5.725549e+001 1.355628e+002
5.821973e+001 1.349373e+002
5.918396e+001 1.348214e+002
6.014819e+001 1.339652e+002
6.111243e+001 1.346412e+002
6.207666e+001 1.404473e+002
6.304089e+001 1.520413e+002
6.400513e+001 1.683765e+002
6.496936e+001 1.911086e+002
6.593359e+001 2.207875e+002
6.689783e+001 2.457892e+002
6.786206e+001 2.606763e+002
6.882629e+001 2.653968e+002
6.979053e+001 2.589269e+002
7.075476e+001 2.336010e+002
7.171899e+001 1.980581e+002
7.268323e+001 1.659266e+002
7.364746e+001 1.383265e+002
7.461169e+001 1.154803e+002
7.557593e+001 9.837050e+001
7.654016e+001 8.793050e+001
7.750439e+001 8.136658e+001
7.846863e+001 7.698708e+001
7.943286e+001 7.477347e+001
8.039709e+001 7.349141e+001
8.136133e+001 7.248274e+001
8.232556e+001 7.177266e+001
8.328979e+001 7.171991e+001
8.425403e+001 7.244252e+001
8.521826e+001 7.401323e+001
8.618250e+001 7.638858e+001
8.714673e+001 8.152644e+001
8.811096e+001 8.666374e+001
8.907520e+001 8.874631e+001
9.003943e+001 8.762212e+001
9.100366e+001 8.362652e+001
9.196790e+001 7.613248e+001
9.293213e+001 6.534329e+001
9.389636e+001 5.376790e+001
9.486060e+001 4.132133e+001
9.582483e+001 2.870636e+001
9.678906e+001 1.816091e+001
9.775330e+001 1.069462e+001
9.871753e+001 5.999763e+000
9.968176e+001 2.322945e+000
1.006460e+002 -1.281509e-001
1.016102e+002 -1.667862e+000
1.025745e+002 -2.362053e+000
1.035387e+002 -2.161842e+000
1.045029e+002 -1.560707e+000
1.054672e+002 -1.003609e+000
1.064314e+002 -5.519028e-001
1.073956e+002 2.094612e-001
1.083599e+002 1.458282e+000
1.093241e+002 3.110859e+000
1.102883e+002 5.032024e+000
1.112526e+002 4.499683e+000
1.122168e+002 4.191574e+000
1.131810e+002 3.920021e+000
1.141453e+002 3.554981e+000
1.151095e+002 3.320332e+000
1.160737e+002 3.195705e+000
1.170380e+002 3.232071e+000
1.180022e+002 3.683624e+000
1.189664e+002 4.721191e+000
1.199307e+002 6.424511e+000
1.208949e+002 8.574810e+000
1.218591e+002 1.013647e+001
1.228234e+002 1.260335e+001
1.237876e+002 1.689756e+001
1.247518e+002 2.316224e+001
1.257161e+002 3.219586e+001
1.266803e+002 4.598708e+001
1.276445e+002 6.738297e+001
1.286088e+002 8.984681e+001
1.295730e+002 1.178451e+002
1.305372e+002 1.464370e+002
1.315015e+002 1.662253e+002
1.324657e+002 1.711403e+002
1.334299e+002 1.605950e+002
1.343942e+002 1.432415e+002
1.353584e+002 1.121171e+002
1.363226e+002 8.109132e+001
1.372869e+002 5.643096e+001
1.382511e+002 3.916526e+001
1.392153e+002 2.723996e+001
1.401796e+002 1.817010e+001
1.411438e+002 1.367284e+001
1.421080e+002 1.004119e+001
1.430723e+002 7.520790e+000
1.440365e+002 5.718834e+000
1.450007e+002 4.227535e+000
1.459650e+002 2.843731e+000
1.469292e+002 1.636497e+000
1.478934e+002 9.233131e-001
1.488577e+002 1.071228e+000
1.498219e+002 1.378567e+000
1.507861e+002 1.767975e+000
1.517504e+002 2.197067e+000
1.527146e+002 2.626556e+000
1.536788e+002 2.938698e+000
1.546431e+002 2.545410e+000
1.556073e+002 2.590778e+000
1.565715e+002 3.498577e+000
1.575358e+002 4.578266e+000
1.585000e+002 5.426350e+000
1.594642e+002 5.909966e+000
1.604285e+002 6.334175e+000
1.613927e+002 7.246441e+000
1.623569e+002 8.924152e+000
1.633212e+002 1.039764e+001
1.642854e+002 1.131850e+001
1.652496e+002 1.187408e+001
1.662139e+002 1.230489e+001
1.671781e+002 1.279195e+001
1.681423e+002 1.324678e+001
1.691066e+002 1.332531e+001
1.700708e+002 1.275523e+001
1.710350e+002 1.219527e+001
1.719993e+002 1.212011e+001
1.729635e+002 1.253072e+001
1.739277e+002 1.319486e+001
1.748920e+002 1.418454e+001
1.758562e+002 1.541401e+001
1.768204e+002 1.635202e+001
1.777847e+002 1.660629e+001
1.787489e+002 1.653397e+001
1.797132e+002 1.697607e+001
1.806774e+002 1.847421e+001
1.816416e+002 2.008659e+001
1.826059e+002 2.133224e+001
1.835701e+002 2.220265e+001
1.845343e+002 2.259465e+001
1.854986e+002 2.239213e+001
1.864628e+002 2.146722e+001
1.874270e+002 2.022898e+001
1.883913e+002 1.844659e+001
1.893555e+002 1.647689e+001
1.903197e+002 1.458577e+001
1.912840e+002 1.283807e+001
1.922482e+002 1.126804e+001
1.932124e+002 9.927952e+000
1.941767e+002 9.012424e+000
1.951409e+002 8.071205e+000
1.961051e+002 6.908913e+000
1.970694e+002 5.738155e+000
1.980336e+002 4.869209e+000
1.989978e+002 4.504463e+000
1.999621e+002 4.576744e+000
2.009263e+002 4.550125e+000
2.018905e+002 4.101158e+000
2.028548e+002 3.821114e+000
2.038190e+002 3.928886e+000
2.047832e+002 4.365841e+000
2.057475e+002 4.911251e+000
2.067117e+002 5.458717e+000
2.076759e+002 6.043007e+000
2.086402e+002 6.312283e+000
2.096044e+002 5.783470e+000
2.105686e+002 5.195847e+000
2.115329e+002 4.966862e+000
2.124971e+002 5.195145e+000
2.134613e+002 5.669205e+000
2.144256e+002 6.226006e+000
2.153898e+002 6.875191e+000
2.163540e+002 7.447372e+000
2.173183e+002 8.019630e+000
2.182825e+002 8.459011e+000
2.192467e+002 8.520462e+000
2.202110e+002 7.998867e+000
2.211752e+002 7.187691e+000
2.221394e+002 6.268456e+000
2.231037e+002 5.198776e+000
2.240679e+002 4.279537e+000
2.250321e+002 3.885208e+000
2.259964e+002 4.156948e+000
2.269606e+002 4.140060e+000
2.279248e+002 3.259384e+000
2.288891e+002 2.218685e+000
2.298533e+002 1.798714e+000
2.308175e+002 2.201576e+000
2.317818e+002 3.110592e+000
2.327460e+002 3.975430e+000
2.337102e+002 4.988945e+000
2.346745e+002 5.835434e+000
2.356387e+002 6.384941e+000
2.366029e+002 6.775787e+000
2.375672e+002 7.186378e+000
2.385314e+002 7.722267e+000
2.394956e+002 8.345806e+000
2.404599e+002 8.802277e+000
2.414241e+002 8.887383e+000
2.423883e+002 9.039242e+000
2.433526e+002 9.323956e+000
2.443168e+002 9.868000e+000
2.452810e+002 1.051409e+001
2.462453e+002 1.122712e+001
2.472095e+002 1.202164e+001
2.481737e+002 1.304175e+001
2.491380e+002 1.434422e+001
2.501022e+002 1.587466e+001
2.510664e+002 1.746072e+001
2.520307e+002 1.901151e+001
2.529949e+002 2.097626e+001
2.539591e+002 2.371331e+001
2.549234e+002 2.715793e+001
2.558876e+002 3.087106e+001
2.568518e+002 3.439719e+001
2.578160e+002 3.825171e+001
2.587803e+002 4.391152e+001
2.597445e+002 5.144453e+001
2.607087e+002 6.050228e+001
2.616730e+002 7.094765e+001
2.626372e+002 8.281476e+001
2.636014e+002 9.635753e+001
2.645657e+002 1.119536e+002
2.655299e+002 1.299999e+002
2.664941e+002 1.469439e+002
2.674584e+002 1.669646e+002
2.684226e+002 1.830567e+002
2.693868e+002 1.923552e+002
2.703511e+002 1.944574e+002
2.713153e+002 1.900916e+002
2.722795e+002 1.786960e+002
2.732438e+002 1.582682e+002
2.742080e+002 1.381614e+002
2.751722e+002 1.183473e+002
2.761365e+002 9.970891e+001
2.771007e+002 8.275089e+001
2.780649e+002 6.750658e+001
2.790292e+002 5.444481e+001
2.799934e+002 4.426031e+001
2.809576e+002 3.702138e+001
2.819219e+002 3.137587e+001
2.828861e+002 2.706557e+001
2.838503e+002 2.396644e+001
2.848146e+002 2.143761e+001
2.857788e+002 1.952472e+001
2.867430e+002 1.811601e+001
2.877073e+002 1.723822e+001
2.886715e+002 1.684679e+001
2.896357e+002 1.669153e+001
2.906000e+002 1.660366e+001
2.915642e+002 1.662466e+001
2.925284e+002 1.647535e+001
2.934927e+002 1.636079e+001
2.944569e+002 1.598156e+001
2.954211e+002 1.509354e+001
2.963854e+002 1.367827e+001
2.973496e+002 1.198947e+001
2.983138e+002 1.022839e+001
2.992781e+002 8.209942e+000
3.002423e+002 6.753479e+000
3.012065e+002 6.284035e+000
3.021708e+002 6.246902e+000
3.031350e+002 6.253342e+000
3.040992e+002 6.175310e+000
3.050635e+002 6.153364e+000
3.060277e+002 6.357092e+000
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3.098847e+002 8.755592e+000
3.108489e+002 9.725508e+000
3.118131e+002 1.082424e+001
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4.072722e+002 -1.450124e+000
4.082365e+002 -1.413391e+000
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