#------------------------------------------------------------------------------ #$Date: 2017-11-22 18:04:39 +0200 (Wed, 22 Nov 2017) $ #$Revision: 352 $ #$URL: svn://172.16.1.111/rod/cif/3/50/01/3500154.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500154 loop_ _publ_author_name 'El Mendili, Y' _publ_section_title ; SOLSA communication to ROD ; _journal_name_full 'Personal communication to ROD' _journal_year 2017 _chemical_compound_source 'commercial powder RP Normapur >99%' _chemical_formula_structural 'C Ca O3' _chemical_formula_sum 'C Ca O3' _chemical_name_mineral calcite _chemical_name_systematic 'C Ca O3' _space_group_IT_number 167 _symmetry_cell_setting trigonal _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 4.991 _cell_length_b 4.991 _cell_length_c 17.062 _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.name DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 785 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 3 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 600 _raman_measurement.range_min 5.036682e+001 _raman_measurement.range_max 2.500483e+003 _rod_data_source.file CaCO3-duplicate.rod _rod_data_source.block CaCO3 _rod_database.code 3500154 _solsa_sample.id CN-AA00-0112 _raman_measurement.datetime_initiated 2017-10-10 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 2100992 COD http://www.crystallography.net/cod/2100992.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 5.036682e+001 1.462114e+001 5.133105e+001 1.287329e+001 5.229529e+001 1.082952e+001 5.325952e+001 8.938910e+000 5.422375e+001 7.489385e+000 5.518799e+001 6.516413e+000 5.615222e+001 5.935029e+000 5.711646e+001 5.742502e+000 5.808069e+001 6.134254e+000 5.904492e+001 6.414882e+000 6.000916e+001 6.549282e+000 6.097339e+001 6.497612e+000 6.193762e+001 6.107254e+000 6.290186e+001 5.177423e+000 6.386609e+001 3.832752e+000 6.483032e+001 3.031768e+000 6.579456e+001 3.069043e+000 6.675879e+001 3.389549e+000 6.772302e+001 3.670234e+000 6.868726e+001 3.871628e+000 6.965149e+001 4.001526e+000 7.061572e+001 4.047592e+000 7.157996e+001 3.952021e+000 7.254419e+001 3.910047e+000 7.350842e+001 4.079759e+000 7.447266e+001 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