#------------------------------------------------------------------------------ #$Date: 2017-11-22 18:06:21 +0200 (Wed, 22 Nov 2017) $ #$Revision: 354 $ #$URL: svn://172.16.1.111/rod/cif/3/50/01/3500156.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500156 loop_ _publ_author_name 'El Mendili, Y' _journal_name_full 'Personal communication to ROD' _journal_year 2017 _chemical_compound_source 'commercial powder Alfa Aesar 99%' _chemical_formula_structural 'Cr2 O3' _chemical_formula_sum 'Cr2 O3' _chemical_name_mineral Eskolaite _chemical_name_systematic 'Cr2 O3' _space_group_IT_number 167 _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 4.785 _cell_length_b 4.785 _cell_length_c 13.162 _raman_determination_method experimental _[local]_chemical_compound_color black _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.name DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 785 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 3 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 600 _raman_measurement.range_min 5.147009e+001 _raman_measurement.range_max 2.000186e+003 _rod_data_source.file Cr2O3.rod _rod_data_source.block 1000005 _rod_database.code 3500156 _solsa_sample.id CN-AA00-0097 _raman_measurement.datetime_initiated 2017-10-10 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 9014203 COD http://www.crystallography.net/cod/9014203.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 5.050586e+001 1.119354e+000 5.147009e+001 6.907806e-001 5.243433e+001 1.147232e-001 5.339856e+001 -3.955841e-001 5.436279e+001 -7.435913e-001 5.532703e+001 -9.283295e-001 5.629126e+001 -8.976593e-001 5.725549e+001 -3.825760e-001 5.821973e+001 3.135986e-001 5.918396e+001 7.615967e-001 6.014819e+001 9.035416e-001 6.111243e+001 8.218307e-001 6.207666e+001 5.570221e-001 6.304089e+001 1.430511e-002 6.400513e+001 -3.812637e-001 6.496936e+001 -2.844162e-001 6.593359e+001 2.977142e-001 6.689783e+001 8.773727e-001 6.786206e+001 1.057823e+000 6.882629e+001 8.460693e-001 6.979053e+001 7.258606e-001 7.075476e+001 9.588928e-001 7.171899e+001 1.436768e+000 7.268323e+001 1.908630e+000 7.364746e+001 2.370094e+000 7.461169e+001 2.698708e+000 7.557593e+001 2.651382e+000 7.654016e+001 2.031631e+000 7.750439e+001 1.315842e+000 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