#------------------------------------------------------------------------------ #$Date: 2017-12-07 14:21:12 +0200 (Thu, 07 Dec 2017) $ #$Revision: 359 $ #$URL: svn://172.16.1.111/rod/cif/3/50/01/3500159.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500159 loop_ _publ_author_name 'El Mendili, Y' _publ_section_title ; Raman spectrum of commercial H6TeO6 ; _journal_name_full 'Personal communication to ROD' _journal_year 2017 _chemical_compound_source 'commercial powder Alpha aesar +99% 'ref 014197' _chemical_formula_structural 'H6 O6 Te' _chemical_formula_sum 'H6 O6 Te3' _chemical_name_mineral 'Telluric acid dihydrate' _chemical_name_systematic 'Telluric acid dihydrate' _space_group_IT_number 225 _symmetry_cell_setting cubic _symmetry_space_group_name_Hall '-F 4 2 3' _symmetry_space_group_name_H-M 'F m -3 m' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.83 _cell_length_b 7.83 _cell_length_c 7.83 _cell_volume 480.0 _raman_determination_method experimental _solsa_sample_id CN-AA00-0100 _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.name DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 532 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 3 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.datetime_initiated 2017-12-06 _raman_measurement.integration_time 20 _raman_measurement.range_min 9.904980e+001 _raman_measurement.range_max 3.500865e+003 _rod_data_source.file RODH6O6Te _rod_data_source.block 3500158 _rod_database.code 3500159 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1010256 COD http://www.crystallography.net/cod/1010256.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 9.904980e+001 1.186237e+002 1.000140e+002 1.039115e+002 1.009783e+002 9.523438e+001 1.019425e+002 8.959238e+001 1.029067e+002 8.748977e+001 1.038710e+002 9.053489e+001 1.048352e+002 9.029097e+001 1.057994e+002 8.063489e+001 1.067637e+002 6.838411e+001 1.077279e+002 5.879170e+001 1.086921e+002 5.697534e+001 1.096564e+002 6.108445e+001 1.106206e+002 6.679763e+001 1.115848e+002 7.438296e+001 1.125491e+002 8.482507e+001 1.135133e+002 1.010560e+002 1.144775e+002 1.233457e+002 1.154418e+002 1.452427e+002 1.164060e+002 1.677195e+002 1.173702e+002 1.910976e+002 1.183345e+002 1.981684e+002 1.192987e+002 1.837657e+002 1.202629e+002 1.626637e+002 1.212272e+002 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