#------------------------------------------------------------------------------
#$Date: 2018-02-05 18:53:39 +0200 (Mon, 05 Feb 2018) $
#$Revision: 387 $
#$URL: svn://172.16.1.111/rod/cif/3/50/01/3500172.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500172
loop_
_publ_author_name
'El Mendili, Y'
'Secchi, M'
'Zannatta, M'
_publ_section_title
;
 Raman spectrum of commercial Lithium metaborate
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2018
_chemical_compound_source        'commercial powder Alfa aesar 99.997% 10739'
_chemical_formula_structural     'B Li O2'
_chemical_formula_sum            'B4 Li4 O8'
_chemical_name_mineral           'Lithium metaborate'
_chemical_name_systematic        'B Li O2'
_space_group_IT_number           122
_symmetry_space_group_name_Hall  'I -4 2bw'
_symmetry_space_group_name_H-M   'I -4 2 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_length_a                   4.1961
_cell_length_b                   4.1961
_cell_length_c                   6.5112
_raman_determination_method      experimental
_[local]_chemical_compound_color white
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'University of Trento'
_raman_measurement_device.company Horiba
_raman_measurement_device.model  Aramis
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 100
_raman_measurement_device.microscope_numerical_aperture 0.80
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 633
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 2
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 600
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 50
_raman_measurement.datetime_initiated 2018-01-18
_rod_data_source.file            LiBO2.rod
_rod_data_source.block           3500090
_rod_database.code               3500172
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 silicon_wafer
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 9009881 COD http://www.crystallography.net/cod/9009881.html
;
 The structure contains the XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
102.305 2225
104.549 1810.25
106.791 1564
109.033 1491.5
111.274 1542.75
113.514 1671.75
115.755 2017.25
117.994 2578.5
120.233 3583.75
122.471 4689.75
124.708 4645.25
126.944 3727.25
129.18 2897.5
131.415 2404.75
133.65 1905
135.884 1558
138.117 1502.75
140.35 1576.5
142.58 1762
144.812 1932.5
147.043 1945.25
149.273 1874.75
151.502 1855.5
153.73 2317.5
155.958 3704.25
158.185 4803
160.411 4863
162.637 4324.5
164.863 4349.5
167.086 4497.25
169.311 4129.5
171.533 3455.25
173.756 3108.75
175.977 3039
178.199 2915.75
180.419 2752.75
182.639 2497.25
184.858 2223.75
187.076 1975.5
189.295 1767.5
191.511 1630.75
193.727 1545.75
195.943 1474
198.159 1431
200.373 1507.75
202.586 1669.5
204.799 1897.25
207.011 1977.25
209.225 1892.5
211.435 1623.75
213.646 1365.25
215.856 1207.25
218.065 1147.5
220.273 1127.5
222.481 1127.5
224.688 1124.25
226.895 1142.25
229.101 1183.75
231.304 1255
233.509 1309.75
235.713 1376
237.917 1447.25
240.12 1491.5
242.32 1521
244.522 1652.75
246.723 2014.5
248.923 2752
251.121 3284.75
253.321 3249.75
255.518 2847.5
257.715 2449
259.913 2188.25
262.108 1899
264.304 1675.25
266.498 1461.25
268.692 1273.25
270.885 1184.5
273.077 1081
275.27 1056.75
277.461 1006.5
279.651 999
281.842 971
284.031 961.25
286.219 951.5
288.407 946.5
290.596 1017
292.782 1002.75
294.968 1061
297.153 1153.5
299.338 1233.5
301.522 1349.5
303.705 1502.5
305.888 1674.75
308.07 1866.5
310.252 1981
312.433 1892.5
314.613 1798.25
316.793 1642.5
318.972 1488
321.15 1373
323.328 1264.25
325.504 1262.75
327.681 1306
329.857 1358
332.032 1427.5
334.205 1403
336.38 1340.25
338.553 1295.75
340.725 1331.25
342.897 1373.5
345.069 1477.25
347.239 1487
349.409 1480
351.578 1388.75
353.747 1348.75
355.914 1296.25
358.081 1273.5
360.248 1246.25
362.414 1196.75
364.58 1144.5
366.744 1087.75
368.908 1058.75
371.071 1031.5
373.235 1068
375.397 1119.5
377.558 1180.75
379.718 1322.25
381.878 1473.5
384.038 1665.75
386.198 1760.25
388.356 1830.25
390.514 1883.5
392.671 1878
394.827 1861
396.983 1876.75
399.138 1914
401.291 1932.75
403.445 1973
405.598 1915.75
407.751 1787.75
409.903 1666.75
412.055 1582.25
414.204 1528
416.354 1417.5
418.504 1387.5
420.652 1335.25
422.8 1287.75
424.948 1227.5
427.094 1200.25
429.241 1178.5
431.386 1209
433.531 1231
435.675 1323.25
437.819 1475.75
439.961 1738.25
442.104 2319.25
444.245 3111.75
446.386 3867.25
448.527 4036.5
450.667 3483.5
452.805 2682.5
454.945 2070.5
457.082 1658
459.219 1449.5
461.356 1299
463.491 1186
465.627 1161.75
467.763 1146
469.896 1146
472.03 1139
474.163 1110
476.295 1170.25
478.426 1201
480.557 1265
482.686 1361.75
484.816 1393
486.945 1451.5
489.074 1452.25
491.202 1507.5
493.329 1536
495.455 1563.75
497.581 1525.5
499.707 1465
501.83 1395.5
503.955 1336
506.079 1323
508.201 1347.75
510.323 1353.25
512.444 1307
514.566 1255.25
516.685 1229.5
518.805 1179.5
520.924 1164.75
523.043 1157.5
525.16 1205.75
527.277 1271.75
529.394 1351.75
531.51 1457.75
533.624 1572.5
535.74 1826
537.854 2184.5
539.967 2791.25
542.079 3413.5
544.191 3686.5
546.303 3520
548.415 3020.75
550.525 2355
552.634 1948.75
554.743 1670
556.852 1481.25
558.96 1375
561.065 1321.25
563.172 1315
565.278 1320
567.384 1252
569.489 1200.5
571.593 1111.25
573.695 1057.25
575.798 1024.5
577.901 992.5
580.003 975
582.103 979.75
584.204 963.25
586.303 941.25
588.402 923.5
590.501 953.25
592.598 927
594.696 928.5
596.792 930.75
598.888 931.25
600.984 927.75
603.078 961.25
605.173 934.75
607.266 948
609.359 983.5
611.452 1009.25
613.543 1097.75
615.634 1131.25
617.724 1204.5
619.814 1209.5
621.903 1174.25
623.993 1141.25
626.081 1080.5
628.168 1052.75
630.255 1037.25
632.341 1008.75
634.427 1011.75
636.512 999
638.596 1021
640.679 1004
642.762 999.75
644.845 1025.75
646.927 975.75
649.008 963.5
651.088 954.5
653.168 945
655.248 944.5
657.327 962.25
659.405 965.5
661.483 989.25
663.559 1005.75
665.636 1046
667.713 1012.25
669.787 1051.5
671.861 1024.5
673.936 1001
676.008 986
678.082 1013.25
680.154 1037.5
682.225 1035
684.297 1096.5
686.367 1150
688.436 1150.5
690.505 1169.75
692.574 1145.25
694.642 1143
696.709 1122.5
698.776 1135.5
700.842 1111.25
702.907 1138.5
704.972 1137.5
707.036 1207.75
709.1 1260.5
711.163 1380.75
713.226 1438.75
715.288 1531.75
717.349 1681
719.41 1873.75
721.469 2245.25
723.529 2549.75
725.588 2640
727.647 2399.75
729.703 2029.5
731.761 1685.5
733.818 1439.5
735.873 1326.25
737.929 1266.25
739.983 1192.25
742.037 1204.5
744.09 1198
746.144 1182
748.195 1190.25
750.248 1194.25
752.298 1214.25
754.348 1258.25
756.399 1268.75
758.448 1302
760.496 1353
762.545 1407
764.593 1507.75
766.639 1705.75
768.685 1884.75
770.731 2090.25
772.776 2330.25
774.82 2475.5
776.864 2557.25
778.907 2528
780.95 2481
782.992 2297.25
785.034 2177
787.075 1942.25
789.115 1699.25
791.155 1546.75
793.195 1362.25
795.234 1258
797.27 1161.5
799.308 1112.5
801.345 1079.25
803.381 1054.5
805.417 988.5
807.452 989.5
809.486 957.75
811.52 932
813.553 938
815.586 947.25
817.618 915.75
819.65 910.5
821.68 917.25
823.71 918.25
825.74 904.25
827.769 890.75
829.797 899.75
831.826 911
833.853 931
835.88 965.75
837.905 979.5
839.931 1059.25
841.957 1139.5
843.981 1176.75
846.005 1196
848.028 1145.5
850.051 1097.25
852.073 1053.25
854.094 997.25
856.115 968.25
858.134 974.5
860.154 991.25
862.174 955
864.192 946.5
866.211 956.25
868.227 949.5
870.244 976.75
872.261 1014.25
874.275 1037.25
876.291 1096.5
878.306 1125
880.319 1146.5
882.333 1149
884.345 1151.5
886.358 1177.75
888.369 1219.75
890.38 1234.75
892.39 1292
894.399 1347.25
896.409 1368.75
898.418 1402.75
900.425 1408
902.432 1411.25
904.44 1371.5
906.446 1339.75
908.452 1291
910.457 1269
912.461 1234.5
914.465 1196
916.468 1221.25
918.471 1213.25
920.474 1196.5
922.475 1188.5
924.476 1226.75
926.477 1235
928.477 1298.5
930.477 1291
932.476 1321
934.473 1355.25
936.471 1386.25
938.468 1443.5
940.464 1439.25
942.46 1465.25
944.456 1421.75
946.45 1370.5
948.445 1349.25
950.437 1306.5
952.431 1286.75
954.423 1249.5
956.415 1263.75
958.406 1248.25
960.398 1261.5
962.387 1265.75
964.377 1284.75
966.366 1301.5
968.354 1314.5
970.342 1320.5
972.329 1279.75
974.315 1221.25
976.303 1176.75
978.288 1093.75
980.273 1061
982.257 1035.25
984.241 999.25
986.224 974.75
988.207 983.25
990.189 975.5
992.171 967.5
994.151 984
996.131 956.75
998.111 978.25
1000.09 1000.75
1002.07 1017.75
1004.05 1049.75
1006.03 1068.25
1008 1102.75
1009.98 1143.5
1011.95 1203
1013.93 1252.25
1015.9 1303
1017.88 1423
1019.85 1582.5
1021.82 1845
1023.8 2094
1025.77 2488.5
1027.74 2853
1029.71 3170
1031.68 3244
1033.65 3188.75
1035.62 2816
1037.59 2414.75
1039.56 2051.5
1041.52 1767.5
1043.49 1536.75
1045.46 1403.25
1047.42 1276.75
1049.39 1183.25
1051.35 1119
1053.32 1111.25
1055.28 1048.5
1057.24 1039.5
1059.2 1025
1061.17 990.5
1063.13 966.5
1065.09 1002.25
1067.05 974
1069.01 957
1070.97 957.25
1072.92 964.25
1074.88 966
1076.84 985.5
1078.8 1002
1080.75 984
1082.71 983.75
1084.66 1003.5
1086.62 1022.25
1088.57 1048.75
1090.52 1095.75
1092.48 1137.5
1094.43 1200.75
1096.38 1246
1098.33 1263.75
1100.28 1251.75
1102.23 1252.25
1104.18 1155.5
1106.13 1117
1108.08 1024
1110.03 988.75
1111.97 957.75
1113.92 960.75
1115.87 933.75
1117.81 927.25
1119.76 912.75
1121.7 895.5
1123.65 876
1125.59 907.25
1127.53 903.75
1129.47 891.5
1131.42 883.5
1133.36 902.25
1135.3 895.5
1137.24 909.5
1139.18 891.75
1141.11 927.25
1143.05 926.75
1144.99 922.75
1146.93 901
1148.86 917.5
1150.8 951
1152.74 937.25
1154.67 939.25
1156.6 958
1158.54 962
1160.47 960.5
1162.4 972.5
1164.34 991.5
1166.27 984
1168.2 992
1170.13 969.25
1172.06 961
1173.99 957.75
1175.92 931.75
1177.85 916
1179.78 913.25
1181.7 883.75
1183.63 885
1185.55 864.5
1187.48 856.75
1189.41 866.25
1191.33 872.75
1193.25 868.25
1195.18 861.25
1197.1 873
1199.02 875.25
1200.94 872.75
1202.86 869.5
1204.79 865
1206.71 860.25
1208.63 858.25
1210.54 855.75
1212.46 877.25
1214.38 872.5
1216.3 880.5
1218.22 885.5
1220.13 885.5
1222.05 910.75
1223.96 901
1225.88 910
1227.79 913.25
1229.71 941
1231.62 944
1233.53 986.5
1235.44 996.25
1237.35 981
1239.26 1014.75
1241.18 998.5
1243.08 967.25
1244.99 958
1246.9 952.75
1248.81 943.75
1250.72 898
1252.63 925
1254.53 933.25
1256.44 919.25
1258.34 935.5
1260.25 945.5
1262.15 927.75
1264.06 947.25
1265.96 945.75
1267.86 932.75
1269.76 923.75
1271.67 920.25
1273.57 918.25
1275.47 870.75
1277.37 871.5
1279.27 855.25
1281.17 849.25
1283.06 880.75
1284.96 854.5
1286.86 861.25
1288.76 865
1290.65 874.25
1292.55 844.75
1294.44 840
1296.34 868.25
1298.23 837.5
1300.13 862
1302.02 863.5
1303.91 856
1305.8 848.25
1307.7 853.25
1309.59 844.5
1311.48 880.5
1313.37 865.75
1315.26 870.75
1317.15 860.25
1319.03 884
1320.92 884.75
1322.81 877.75
1324.7 894.25
1326.58 878
1328.47 924.5
1330.35 915.75
1332.24 926.25
1334.12 951
1336 1002.5
1337.89 1012.75
1339.77 1065
1341.65 1139.25
1343.53 1199.75
1345.41 1243.25
1347.29 1315
1349.17 1369.75
1351.05 1403.5
1352.93 1435.25
1354.81 1415.25
1356.69 1403.25
1358.56 1378
1360.44 1311
1362.32 1314.25
1364.19 1204.5
1366.07 1181
1367.94 1170
1369.81 1110.5
1371.69 1090.25
1373.56 1059.75
1375.43 1043
1377.31 1031.5
1379.18 1023.5
1381.05 1040.75
1382.92 1023.5
1384.79 1039.25
1386.66 1026.5
1388.52 1042
1390.39 1038.25
1392.26 1022.5
1394.13 1020.25
1395.99 1029
1397.86 1008.25
1399.73 1010
1401.59 975
1403.45 959.5
1405.32 956.5
1407.18 949
1409.04 923
1410.91 943
1412.77 917
1414.63 921.75
1416.49 915.25
1418.35 901
1420.21 917.5
1422.07 906.5
1423.93 940.75
1425.79 909.25
1427.64 916.5
1429.5 905.75
1431.36 909
1433.21 908.25
1435.07 882
1436.93 905.25
1438.78 909.5
1440.63 911
1442.49 872.5
1444.34 889
1446.19 908
1448.04 904
1449.89 882.75
1451.75 880
1453.6 881.75
1455.45 880.75
1457.3 879.5
1459.14 882.5
1460.99 895.25
1462.84 878.25
1464.69 882.25
1466.53 875.75
1468.38 873
1470.23 881.75
1472.07 874.25
1473.92 888.5
1475.76 879.5
1477.6 899.5
1479.45 872.75
1481.29 869.5
1483.13 858.5
1484.97 865.25
1486.81 879.5
1488.65 860.5
1490.49 867.5
1492.33 881
1494.17 884
1496.01 857.25
1497.85 844.75
1499.69 849.5
1501.52 868
1503.36 876.5
1505.19 859.75
1507.03 872.75
1508.87 843.25
1510.7 849.25
1512.53 851.75
1514.37 852.5
1516.2 851
1518.03 850.75
1519.86 849.25
1521.69 874.25
1523.53 858.5
1525.36 860.5
1527.19 845
1529.02 837
1530.84 858.75
1532.67 841
1534.5 867.25
1536.33 836.25
1538.15 852
1539.98 844.5
1541.8 837.25
1543.63 845.75
1545.45 852.25
1547.28 836.5
1549.1 838.75
1550.93 853
1552.75 848
1554.57 856
1556.39 832.25
1558.21 859.5
1560.03 848.25
1561.85 848.5
1563.67 851.25
1565.49 845
1567.31 867.75
1569.13 841.75
1570.95 843
1572.76 839.5
1574.58 844.25
1576.39 834.25
1578.21 841.5
1580.03 835
1581.84 835.75
1583.65 829
1585.47 838.75
1587.28 833.25
1589.09 841.5
1590.9 820.5
1592.72 853.5
1594.53 825.75
1596.34 828
1598.15 834.75
1599.96 814
1601.76 834.25
1603.57 842.75
1605.38 864.25
1607.19 835
1609 844.5
1610.8 832.75
1612.61 839
1614.41 842.5
1616.22 818
1618.02 850.5
1619.83 836.25
1621.63 842
1623.43 876.75
1625.23 841.75
1627.04 840.5
1628.84 841.5
1630.64 848.75
1632.44 863.25
1634.24 850.75
1636.04 841
1637.84 842.5
1639.63 855.25
1641.43 852
1643.23 848.5
1645.03 834.25
1646.82 849
1648.62 846.75
1650.42 868.75
1652.21 848
1654 832.5
1655.8 852.25
1657.59 841.75
1659.38 848.75
1661.18 834
1662.97 868
1664.76 865.25
1666.55 872
1668.34 850.75
1670.13 863.5
1671.92 862.75
1673.71 855.25
1675.5 858
1677.29 858.25
1679.07 891.5
1680.86 865
1682.65 852.75
1684.43 863.5
1686.22 885.5
1688 854
1689.79 860
1691.57 860
1693.35 859.75
1695.14 875.75
1696.92 853.75
1698.7 876.5
1700.48 866.5
1702.26 854
1704.04 836.5
1705.83 849.25
1707.6 854.75
1709.38 866.5
1711.16 865.25
1712.94 863
1714.72 853
1716.49 862.25
1718.27 849.25
1720.05 854.25
1721.82 843.75
1723.6 855
1725.37 866
1727.15 850.25
1728.92 863.75
1730.69 847.5
1732.47 818.25
1734.24 831.25
1736.01 825.75
1737.78 829.75
1739.55 829.25
1741.32 814.75
1743.09 835.75
1744.86 845.75
1746.63 822.75
1748.4 828.5
1750.16 823.5
1751.93 819.75
1753.7 816.5
1755.46 815.75
1757.23 827.25
1759 821.75
1760.76 812.5
1762.52 812.75
1764.29 820.5
1766.05 788
1767.82 802.75
1769.58 811.25
1771.34 794
1773.1 807
1774.86 791.25
1776.62 806.5
1778.38 803.5
1780.14 807
1781.9 788.5
1783.66 814.25
1785.42 786
1787.17 805.25
1788.93 796.25
1790.69 782.5
1792.44 819.5
1794.2 804
1795.95 784.75
1797.71 805.5
1799.46 799.25
1801.22 790.25
1802.97 804.5
1804.72 802.25
1806.48 789.5
1808.23 785.75
1809.98 790
1811.73 790
1813.48 795.75
1815.23 790.25
1816.98 786.25
1818.73 791
1820.48 776.5
1822.22 794.5
1823.97 785.75
1825.72 782
1827.46 803
1829.21 786.25
1830.96 783.25
1832.7 799.25
1834.44 796.5
1836.19 795.5
1837.93 783.5
1839.68 792.25
1841.42 778.75
1843.16 775
1844.9 787.5
1846.64 779
1848.38 784.5
1850.12 768
1851.86 777
1853.6 774.25
1855.34 788.25
1857.08 780.5
1858.82 787.5
1860.56 776.5
1862.29 779.5
1864.03 776
1865.77 775.75
1867.5 770.5
1869.24 783.25
1870.97 765.25
1872.7 773.25
1874.44 784.25
1876.17 746
1877.9 777.25
1879.63 785.25
1881.37 777.75
1883.1 759.75
1884.83 764.25
1886.56 786.5
1888.29 765
1890.02 765
1891.75 775.25
1893.47 781
1895.2 781.5
1896.93 776.5
1898.66 760.75
1900.38 775.25
1902.11 780.25
1903.83 767.25
1905.56 762.5
1907.28 765.75
1909.01 775
1910.73 758
1912.45 752
1914.18 785.75
1915.9 740.75
1917.62 770.5
1919.34 769
1921.06 750.25
1922.78 773.25
1924.5 787.75
1926.22 752.5
1927.94 761
1929.66 758.25
1931.38 741.75
1933.1 751.75
1934.81 754
1936.53 754
1938.24 745.25
1939.96 747.5
1941.68 767
1943.39 778.5
1945.1 748.5
1946.82 745
1948.53 738.25
1950.24 753
1951.96 765.5
1953.67 762.5
1955.38 736.25
1957.09 752.5
1958.8 751.25
1960.51 732.75
1962.22 731
1963.93 754
1965.64 757.75
1967.35 752.5
1969.05 740.75
1970.76 739
1972.47 731
1974.17 751.75
1975.88 761.75
1977.58 738.25
1979.29 755.5
1980.99 742.5
1982.7 758.75
1984.4 730.5
1986.1 752.25
1987.81 752.75
1989.51 750
1991.21 727.75
1992.91 761.25
1994.61 763.5
1996.31 763
1998.01 746
1999.71 756