#------------------------------------------------------------------------------ #$Date: 2018-02-06 16:24:32 +0200 (Tue, 06 Feb 2018) $ #$Revision: 414 $ #$URL: svn://172.16.1.111/rod/cif/3/50/01/3500199.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500199 loop_ _publ_author_name 'El Mendili, Y' 'Secchi, M' 'Zannatta, M' _publ_section_title ; Raman spectrum of commercial Nahcolite ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder Alfa aesar 99.7% 14707' _chemical_formula_structural 'Na H C O3' _chemical_formula_sum 'C H Na O3' _chemical_name_mineral Nahcolite _chemical_name_systematic 'Na H C O3' _space_group_IT_number 14 _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90 _cell_angle_beta 93.32 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.51(4) _cell_length_b 9.70(4) _cell_length_c 3.53(3) _raman_determination_method experimental _[local]_chemical_compound_color white _[local]_chemical_compound_state Solid _raman_measurement_device.location 'University of Trento' _raman_measurement_device.company Horiba _raman_measurement_device.model Aramis _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 50 _raman_measurement_device.microscope_numerical_aperture 0.50 _raman_measurement_device.excitation_laser_type helium-neon _raman_measurement_device.excitation_laser_wavelength 633 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 2 _raman_measurement_device.power_on_sample 12 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1 _raman_measurement_device.diffraction_grating 600 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.integration_time 10 _raman_measurement.datetime_initiated 2018-01-15 _rod_data_source.file NaHCO3.rod _rod_data_source.block 3500020 _rod_database.code 3500199 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 silicon_wafer loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 1011016 COD http://www.crystallography.net/cod/1011016.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 102.279 1189 104.522 1333 106.766 1909 109.007 3585 111.248 7418 113.489 11691 115.728 12248 117.967 8601 120.207 4486 122.445 2543 124.682 1995 126.919 1696 129.155 1379 131.39 1136 133.624 1144 135.858 1358 138.09 1978 140.323 3598 142.555 6605 144.786 9133 147.017 8816 149.247 6355 151.475 4133 153.704 3065 155.932 2372 158.158 1742 160.385 1355 162.612 1309 164.836 1483 167.061 1522 169.284 1353 171.508 960 173.729 729 175.952 572 178.172 596 180.394 651 182.613 739 184.833 686 187.051 595 189.268 524 191.486 468 193.702 505 195.917 512 198.134 593 200.348 780 202.561 1044 204.774 1310 206.986 1395 209.198 1414 211.409 1336 213.621 1170 215.83 973 218.039 884 220.248 872 222.456 1052 224.663 1294 226.868 1599 229.074 1686 231.279 1580 233.484 1366 235.688 1061 237.892 827 240.093 693 242.295 587 244.497 545 246.698 462 248.897 432 251.096 386 253.295 356 255.492 359 257.69 351 259.886 315 262.083 312 264.277 305 266.473 300 268.666 288 270.86 291 273.052 253 275.245 270 277.436 262 279.626 246 281.816 264 284.006 248 286.194 228 288.382 223 290.569 244 292.757 237 294.943 235 297.128 236 299.313 233 301.497 238 303.68 221 305.863 241 308.045 217 310.227 232 312.408 239 314.588 229 316.768 243 318.947 246 321.125 237 323.302 256 325.479 274 327.656 262 329.832 259 332.007 264 334.181 245 336.355 221 338.528 215 340.7 223 342.872 208 345.043 217 347.214 233 349.383 212 351.553 227 353.721 216 355.889 189 358.056 197 360.224 196 362.389 190 364.554 199 366.72 199 368.883 200 371.046 192 373.209 197 375.372 187 377.533 195 379.694 193 381.854 193 384.013 205 386.172 207 388.33 197 390.487 209 392.644 201 394.801 189 396.957 200 399.112 199 401.266 188 403.42 182 405.574 191 407.726 204 409.878 195 412.029 192 414.179 183 416.33 182 418.48 194 420.627 195 422.776 189 424.922 176 427.07 170 429.216 177 431.361 176 433.507 197 435.65 194 437.794 168 439.937 186 442.078 179 444.221 164 446.361 171 448.503 185 450.642 184 452.781 174 454.919 169 457.058 165 459.195 170 461.331 176 463.467 188 465.602 196 467.737 182 469.871 164 472.004 172 474.137 176 476.269 167 478.401 159 480.532 179 482.662 177 484.792 185 486.921 194 489.05 191 491.178 184 493.304 185 495.431 177 497.557 188 499.682 173 501.806 173 503.931 185 506.054 188 508.176 183 510.299 192 512.42 160 514.541 184 516.661 168 518.781 183 520.9 171 523.019 172 525.136 197 527.253 186 529.37 171 531.485 170 533.6 168 535.714 173 537.83 170 539.943 182 542.055 182 544.167 185 546.278 170 548.389 173 550.499 192 552.609 182 554.718 170 556.826 172 558.934 182 561.041 176 563.148 161 565.254 170 567.359 176 569.464 154 571.569 175 573.671 174 575.774 187 577.877 189 579.977 177 582.079 193 584.18 193 586.279 183 588.378 198 590.476 185 592.574 201 594.671 184 596.768 176 598.864 189 600.96 172 603.054 171 605.148 185 607.242 185 609.335 188 611.427 189 613.519 189 615.61 201 617.7 184 619.79 193 621.879 208 623.968 202 626.055 193 628.144 188 630.231 207 632.317 205 634.403 210 636.486 213 638.571 208 640.655 213 642.738 209 644.821 278 646.903 395 648.984 556 651.064 558 653.144 443 655.224 301 657.302 304 659.381 439 661.459 685 663.535 752 665.612 593 667.687 375 669.763 303 671.837 317 673.912 293 675.985 303 678.058 362 680.13 435 682.201 631 684.273 946 686.343 1485 688.412 2034 690.481 2039 692.551 1613 694.618 1094 696.686 732 698.752 739 700.818 848 702.883 778 704.948 572 707.013 364 709.076 295 711.139 240 713.202 244 715.264 222 717.326 231 719.385 216 721.445 211 723.505 191 725.564 195 727.623 197 729.68 203 731.737 199 733.794 204 735.849 193 737.905 179 739.959 184 742.014 196 744.067 191 746.12 199 748.172 183 750.224 206 752.275 187 754.325 208 756.376 194 758.424 188 760.473 192 762.521 179 764.569 186 766.616 199 768.662 196 770.707 196 772.752 198 774.797 199 776.841 188 778.884 192 780.927 199 782.969 189 785.01 195 787.051 204 789.092 185 791.132 201 793.171 204 795.209 201 797.247 195 799.285 198 801.322 204 803.357 189 805.393 208 807.428 200 809.463 203 811.497 211 813.529 214 815.563 198 817.594 201 819.625 214 821.657 193 823.687 213 825.717 211 827.746 215 829.774 212 831.801 241 833.83 247 835.856 284 837.882 294 839.908 293 841.932 276 843.957 236 845.982 212 848.005 185 850.027 216 852.05 212 854.07 192 856.091 193 858.111 205 860.131 196 862.15 216 864.169 195 866.187 206 868.204 205 870.221 195 872.238 220 874.252 213 876.268 195 878.283 189 880.296 195 882.31 194 884.322 194 886.335 202 888.345 202 890.356 219 892.367 217 894.376 206 896.386 198 898.395 196 900.402 208 902.409 208 904.417 207 906.423 193 908.429 211 910.434 207 912.438 212 914.442 194 916.445 204 918.448 205 920.451 219 922.452 215 924.453 216 926.454 211 928.454 209 930.454 207 932.451 212 934.45 218 936.448 222 938.445 215 940.441 218 942.437 218 944.433 209 946.427 211 948.422 218 950.415 212 952.408 212 954.4 237 956.393 216 958.383 216 960.374 209 962.365 220 964.354 224 966.342 227 968.332 214 970.319 229 972.306 222 974.293 234 976.279 230 978.265 233 980.25 227 982.234 254 984.218 263 986.202 282 988.184 298 990.166 343 992.147 388 994.128 412 996.109 435 998.089 429 1000.07 394 1002.05 374 1004.02 373 1006 352 1007.98 330 1009.96 327 1011.93 293 1013.91 312 1015.88 309 1017.86 329 1019.83 322 1021.8 340 1023.77 338 1025.75 392 1027.72 407 1029.69 377 1031.66 449 1033.63 477 1035.6 542 1037.57 702 1039.53 908 1041.5 1177 1043.47 1995 1045.43 4264 1047.4 9105 1049.36 13585 1051.33 13398 1053.29 8847 1055.26 4419 1057.22 2060 1059.18 1195 1061.14 808 1063.11 622 1065.06 527 1067.03 473 1068.98 472 1070.94 393 1072.9 390 1074.86 353 1076.82 330 1078.77 313 1080.73 311 1082.69 288 1084.64 304 1086.59 288 1088.55 281 1090.5 276 1092.45 291 1094.41 251 1096.36 270 1098.31 267 1100.26 273 1102.21 261 1104.16 262 1106.11 265 1108.06 261 1110 265 1111.95 267 1113.9 276 1115.84 259 1117.79 279 1119.73 276 1121.68 253 1123.62 263 1125.57 249 1127.51 291 1129.45 277 1131.39 250 1133.33 267 1135.27 261 1137.21 279 1139.15 269 1141.09 257 1143.03 273 1144.97 218 1146.9 268 1148.84 262 1150.78 269 1152.71 257 1154.65 269 1156.58 264 1158.52 270 1160.45 257 1162.38 246 1164.31 257 1166.25 270 1168.18 256 1170.11 260 1172.04 257 1173.97 272 1175.9 264 1177.83 278 1179.75 243 1181.68 254 1183.61 280 1185.53 256 1187.46 266 1189.38 271 1191.31 284 1193.23 307 1195.16 268 1197.08 317 1199 299 1200.92 316 1202.84 317 1204.76 309 1206.68 294 1208.6 342 1210.52 335 1212.44 353 1214.36 337 1216.28 350 1218.19 346 1220.11 367 1222.03 386 1223.94 395 1225.86 399 1227.77 417 1229.68 449 1231.6 451 1233.51 465 1235.42 489 1237.33 479 1239.24 538 1241.15 599 1243.06 626 1244.97 661 1246.88 750 1248.79 811 1250.7 900 1252.6 964 1254.51 1064 1256.42 1181 1258.32 1259 1260.23 1382 1262.13 1584 1264.04 1732 1265.94 1960 1267.84 2223 1269.74 2349 1271.64 2501 1273.55 2466 1275.45 2406 1277.35 2201 1279.25 1962 1281.14 1680 1283.04 1408 1284.94 1198 1286.84 1073 1288.74 903 1290.63 818 1292.53 712 1294.42 636 1296.32 559 1298.21 531 1300.11 485 1302 473 1303.89 432 1305.78 416 1307.67 376 1309.57 394 1311.46 373 1313.34 332 1315.23 331 1317.12 338 1319.01 323 1320.9 309 1322.79 309 1324.67 310 1326.56 291 1328.45 285 1330.33 288 1332.21 262 1334.1 244 1335.98 247 1337.86 267 1339.75 256 1341.63 274 1343.51 263 1345.39 249 1347.27 270 1349.15 251 1351.03 266 1352.91 257 1354.79 246 1356.66 239 1358.54 251 1360.42 267 1362.29 246 1364.17 245 1366.04 248 1367.92 237 1369.79 232 1371.67 243 1373.54 249 1375.41 242 1377.28 248 1379.15 225 1381.03 254 1382.9 244 1384.76 228 1386.63 250 1388.5 245 1390.37 235 1392.24 224 1394.11 248 1395.97 250 1397.84 234 1399.7 253 1401.57 238 1403.43 240 1405.3 243 1407.16 228 1409.02 234 1410.89 250 1412.75 255 1414.61 246 1416.47 256 1418.33 266 1420.19 261 1422.05 270 1423.91 281 1425.77 284 1427.62 282 1429.48 311 1431.34 346 1433.19 409 1435.05 550 1436.9 737 1438.76 938 1440.61 985 1442.47 860 1444.32 685 1446.17 521 1448.02 466 1449.87 449 1451.73 458 1453.58 509 1455.42 573 1457.27 662 1459.12 740 1460.97 786 1462.82 823 1464.67 788 1466.51 684 1468.36 606 1470.2 485 1472.05 439 1473.89 377 1475.74 351 1477.58 329 1479.42 288 1481.27 303 1483.11 267 1484.95 272 1486.79 254 1488.63 235 1490.47 258 1492.31 252 1494.15 230 1495.99 244 1497.83 249 1499.66 265 1501.5 228 1503.34 243 1505.17 216 1507.01 225 1508.84 207 1510.68 239 1512.51 216 1514.35 237 1516.18 221 1518.01 233 1519.84 229 1521.67 212 1523.5 225 1525.33 210 1527.16 216 1528.99 221 1530.82 210 1532.65 231 1534.48 226 1536.3 217 1538.13 232 1539.96 215 1541.78 222 1543.61 209 1545.43 209 1547.26 226 1549.08 218 1550.9 219 1552.73 216 1554.55 208 1556.37 216 1558.19 220 1560.01 231 1561.83 208 1563.65 217 1565.47 209 1567.29 224 1569.11 222 1570.92 224 1572.74 219 1574.56 220 1576.37 222 1578.19 229 1580 219 1581.82 230 1583.63 215 1585.45 222 1587.26 222 1589.07 239 1590.88 231 1592.69 232 1594.51 224 1596.32 217 1598.13 219 1599.94 230 1601.74 231 1603.55 256 1605.36 247 1607.17 244 1608.97 264 1610.78 268 1612.59 255 1614.39 291 1616.2 310 1618 311 1619.81 340 1621.61 396 1623.41 437 1625.21 462 1627.02 473 1628.82 440 1630.62 438 1632.42 382 1634.22 366 1636.02 309 1637.82 289 1639.61 278 1641.41 254 1643.21 263 1645.01 249 1646.8 242 1648.6 211 1650.39 217 1652.19 230 1653.98 226 1655.78 217 1657.57 231 1659.36 229 1661.16 235 1662.95 229 1664.74 235 1666.53 234 1668.32 245 1670.11 265 1671.9 278 1673.69 292 1675.48 302 1677.26 306 1679.05 303 1680.84 299 1682.63 322 1684.41 310 1686.2 323 1687.98 316 1689.77 284 1691.55 320 1693.33 304 1695.12 297 1696.9 307 1698.68 305 1700.46 275 1702.24 271 1704.02 251 1705.8 249 1707.58 231 1709.36 228 1711.14 236 1712.92 210 1714.7 240 1716.47 224 1718.25 224 1720.03 228 1721.8 228 1723.58 234 1725.35 244 1727.13 230 1728.9 237 1730.67 233 1732.44 221 1734.22 213 1735.99 227 1737.76 226 1739.53 234 1741.3 228 1743.07 212 1744.84 199 1746.61 210 1748.38 217 1750.14 211 1751.91 211 1753.68 218 1755.44 206 1757.21 214 1758.98 211 1760.74 221 1762.5 217 1764.27 219 1766.03 213 1767.79 203 1769.56 208 1771.32 216 1773.08 222 1774.84 224 1776.6 196 1778.36 210 1780.12 209 1781.88 214 1783.64 210 1785.4 213 1787.15 214 1788.91 209 1790.67 215 1792.42 214 1794.18 212 1795.93 206 1797.69 217 1799.44 210 1801.2 223 1802.95 215 1804.7 228 1806.46 232 1808.21 231 1809.96 221 1811.71 213 1813.46 215 1815.21 227 1816.96 235 1818.71 218 1820.46 229 1822.2 239 1823.95 213 1825.7 239 1827.44 247 1829.19 241 1830.94 230 1832.68 233 1834.42 260 1836.17 237 1837.91 258 1839.66 252 1841.4 246 1843.14 243 1844.88 226 1846.62 237 1848.36 252 1850.1 258 1851.84 245 1853.58 245 1855.32 245 1857.06 250 1858.8 251 1860.54 230 1862.27 244 1864.01 240 1865.74 248 1867.48 250 1869.22 215 1870.95 219 1872.68 227 1874.42 237 1876.15 232 1877.88 235 1879.61 239 1881.35 235 1883.08 240 1884.81 237 1886.54 248 1888.27 245 1890 245 1891.73 276 1893.45 243 1895.18 245 1896.91 259 1898.64 262 1900.36 260 1902.09 271 1903.81 269 1905.54 279 1907.26 297 1908.99 281 1910.71 304 1912.43 304 1914.16 291 1915.88 284 1917.6 305 1919.32 307 1921.04 301 1922.76 311 1924.48 280 1926.2 276 1927.92 288 1929.64 290 1931.36 284 1933.08 280 1934.79 255 1936.51 274 1938.23 296 1939.94 248 1941.66 253 1943.37 240 1945.08 255 1946.8 238 1948.51 221 1950.22 254 1951.94 249 1953.65 230 1955.36 247 1957.07 234 1958.78 238 1960.49 250 1962.2 227 1963.91 231 1965.62 229 1967.33 225 1969.03 233 1970.74 210 1972.45 233 1974.15 231 1975.86 227 1977.56 229 1979.27 225 1980.97 209 1982.68 239 1984.38 232 1986.08 229 1987.79 242 1989.49 247 1991.19 232 1992.89 223 1994.59 238 1996.29 227 1997.99 224 1999.69 241