#------------------------------------------------------------------------------
#$Date: 2018-02-06 16:24:47 +0200 (Tue, 06 Feb 2018) $
#$Revision: 419 $
#$URL: svn://172.16.1.111/rod/cif/3/50/02/3500203.rod $
#------------------------------------------------------------------------------
#
# This file is available in the Raman Open Database (ROD),
# http://solsa.crystallography.net/rod/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_3500203
loop_
_publ_author_name
'El Mendili, Y'
'Secchi, M'
'Zannatta, M'
_publ_section_title
;
 Raman spectrum of commercial NbO2
;
_journal_name_full               'Personal communication to ROD'
_journal_year                    2018
_chemical_compound_source        'commercial Alfa Aesar 99%'
_chemical_formula_structural     'Nb O2'
_chemical_formula_sum            'Nb O2'
_chemical_name_mineral           'Niobium dioxide'
_chemical_name_systematic        'Niobium dioxide'
_space_group_IT_number           88
_symmetry_space_group_name_Hall  '-I 4ad'
_symmetry_space_group_name_H-M   'I 41/a :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            32
_cell_length_a                   13.698
_cell_length_b                   13.698
_cell_length_c                   5.976
_raman_determination_method      experimental
_[local]_chemical_compound_color black
_[local]_chemical_compound_state Solid
_raman_measurement_device.location 'University of Trento'
_raman_measurement_device.company Horiba
_raman_measurement_device.model  Aramis
_raman_measurement_device.optics_type microscope
_raman_measurement_device.microscope_system dispersive
_raman_measurement_device.microscope_objective_magnification 50
_raman_measurement_device.microscope_numerical_aperture 0.50
_raman_measurement_device.excitation_laser_type helium-neon
_raman_measurement_device.excitation_laser_wavelength 633
_raman_measurement_device.configuration simple
_raman_measurement_device.resolution 2
_raman_measurement_device.power_on_sample 12
_raman_measurement_device.direction_polarization unoriented
_raman_measurement_device.spot_size 1
_raman_measurement_device.diffraction_grating 600
_raman_measurement.environment   Air
_raman_measurement.environment_details
;
 The sample was measured in air.
;
_raman_measurement.temperature   300
_raman_measurement.pressure      100
_raman_measurement.background_subtraction no
_raman_measurement.background_subtraction_details
;
 No background subtraction method was applied.
;
_raman_measurement.baseline_correction no
_raman_measurement.baseline_correction_details
;
 No baseline correction method was applied.
;
_raman_measurement.integration_time 300
_raman_measurement.datetime_initiated 2018-01-15
_rod_data_source.file            NbO2.rod
_rod_data_source.block           3500020
_rod_database.code               3500203
loop_
_raman_complementary.id
_raman_complementary.method
1 EDX
loop_
_raman_measurement_device_calibration.id
_raman_measurement_device_calibration.standard
1 silicon_wafer
loop_
_rod_related_entry.id
_rod_related_entry.code
_rod_related_entry.database
_rod_related_entry.uri
_rod_related_entry.description
1 1520791 COD http://www.crystallography.net/cod/1520791.html
;
no XRD analysis data.
;
loop_
_raman_spectrum.raman_shift
_raman_spectrum.intensity
102.279 95.75
104.522 115.25
106.766 117.25
109.007 124.75
111.248 110
113.489 110
115.728 114.5
117.967 121.5
120.207 110
122.445 116.75
124.682 113.25
126.919 115
129.155 113.25
131.39 132.5
133.624 128.75
135.858 124.5
138.09 122.5
140.323 131.5
142.555 153.5
144.786 169.75
147.017 249.5
149.247 393
151.475 506.5
153.704 372.25
155.932 233.25
158.158 170
160.385 162
162.612 147.25
164.836 152.25
167.061 173
169.284 182.25
171.508 209.5
173.729 258
175.952 375
178.172 502
180.394 628.5
182.613 666.5
184.833 547.5
187.051 334.5
189.268 207.75
191.486 145
193.702 136
195.917 130.5
198.134 117.25
200.348 120.25
202.561 109
204.774 117.75
206.986 103.5
209.198 108.75
211.409 101.5
213.621 105
215.83 109.5
218.039 109
220.248 126
222.456 118.25
224.663 136
226.868 138.25
229.074 125.75
231.279 133.25
233.484 134.25
235.688 149.5
237.892 147.75
240.093 160.25
242.295 143.5
244.497 132.75
246.698 125.5
248.897 123.25
251.096 132.5
253.295 137.25
255.492 152
257.69 173
259.886 196.25
262.083 170.5
264.277 153.5
266.473 141.5
268.666 135.25
270.86 142
273.052 161.25
275.245 191.25
277.436 213
279.626 200
281.816 191
284.006 170.5
286.194 168.5
288.382 162.75
290.569 156.5
292.757 152
294.943 160.25
297.128 162.75
299.313 154.5
301.497 166
303.68 158.25
305.863 162.5
308.045 165.25
310.227 163
312.408 163.75
314.588 156.5
316.768 171.5
318.947 181
321.125 185
323.302 189.75
325.479 202
327.656 214
329.832 239.75
332.007 263.25
334.181 304.5
336.355 381
338.528 478.5
340.7 624.25
342.872 730
345.043 779
347.214 675.75
349.383 570.5
351.553 517
353.721 558.75
355.889 585.5
358.056 559.25
360.224 513
362.389 451.75
364.554 346.75
366.72 281.5
368.883 232.25
371.046 207
373.209 191
375.372 171
377.533 180.25
379.694 185.75
381.854 180
384.013 187
386.172 197.25
388.33 207.75
390.487 232
392.644 244
394.801 272
396.957 295.25
399.112 347.75
401.266 393.25
403.42 436.25
405.574 458
407.726 543.75
409.878 644
412.029 807.5
414.179 990
416.33 1146.25
418.48 1126.5
420.627 942
422.776 745
424.922 554.5
427.07 452.25
429.216 371.5
431.361 319.5
433.507 274
435.65 237
437.794 232.5
439.937 233.25
442.078 219.75
444.221 236.25
446.361 240.5
448.503 234.25
450.642 232
452.781 204.75
454.919 198.75
457.058 193
459.195 170.25
461.331 161.25
463.467 158.75
465.602 160.5
467.737 176.5
469.871 173
472.004 170
474.137 191
476.269 157.5
478.401 153.25
480.532 146.5
482.662 144.75
484.792 129.5
486.921 125
489.05 125.25
491.178 129.25
493.304 127.25
495.431 134.25
497.557 123.75
499.682 132.25
501.806 120
503.931 115
506.054 117
508.176 129
510.299 124
512.42 125
514.541 129.75
516.661 118.25
518.781 112.5
520.9 122.25
523.019 122
525.136 119.5
527.253 121
529.37 120.25
531.485 125
533.6 126.5
535.714 121.75
537.83 126
539.943 125.5
542.055 137
544.167 138
546.278 131.25
548.389 134
550.499 133.25
552.609 145.5
554.718 137.5
556.826 143.75
558.934 131
561.041 152.75
563.148 150
565.254 152.5
567.359 159.5
569.464 165.5
571.569 184.75
573.671 201.25
575.774 207.5
577.877 214
579.977 233.5
582.079 240.75
584.18 250.75
586.279 283
588.378 322
590.476 355
592.574 354.25
594.671 342.75
596.768 314.5
598.864 271.75
600.96 233.75
603.054 214.25
605.148 191.5
607.242 182.5
609.335 173.75
611.427 166
613.519 165.75
615.61 160.25
617.7 166.25
619.79 172
621.879 165
623.968 177.5
626.055 186.75
628.144 191.5
630.231 202
632.317 212.5
634.403 228.75
636.486 250.5
638.571 263.25
640.655 280
642.738 295.5
644.821 283
646.903 265.5
648.984 258.25
651.064 236.5
653.144 213.5
655.224 199
657.302 198.5
659.381 173
661.459 166.25
663.535 162
665.612 160.25
667.687 157
669.763 156
671.837 149.5
673.912 152.5
675.985 140.5
678.058 138.5
680.13 146.75
682.201 145.75
684.273 145
686.343 139.75
688.412 144.75
690.481 145
692.551 139.25
694.618 140
696.686 143.75
698.752 139.75
700.818 143
702.883 142.25
704.948 144.5
707.013 149.5
709.076 150.5
711.139 152.5
713.202 157
715.264 153.75
717.326 146.75
719.385 148.5
721.445 148
723.505 149
725.564 132.25
727.623 140.5
729.68 132
731.737 136.5
733.794 130.5
735.849 131.75
737.905 132
739.959 129
742.014 131
744.067 128.75
746.12 126
748.172 125.75
750.224 121
752.275 129
754.325 119
756.376 127
758.424 125.25
760.473 128.5
762.521 122.75
764.569 124.25
766.616 116.5
768.662 138
770.707 126.25
772.752 130.25
774.797 131
776.841 132.75
778.884 138
780.927 136
782.969 135
785.01 142.75
787.051 148
789.092 141.75
791.132 159
793.171 139
795.209 153
797.247 157.25
799.285 172.25
801.322 158.75
803.357 177.25
805.393 179.75
807.428 183.25
809.463 198
811.497 198.75
813.529 203.5
815.563 222
817.594 237.75
819.625 232.75
821.657 256.25
823.687 264
825.717 281.75
827.746 286.25
829.774 269
831.801 275.25
833.83 257
835.856 239.75
837.882 238.75
839.908 228.25
841.932 200
843.957 201
845.982 179
848.005 177
850.027 168.75
852.05 158.25
854.07 152
856.091 143.5
858.111 141
860.131 141.25
862.15 133.75
864.169 123.5
866.187 127
868.204 125
870.221 125.5
872.238 114.75
874.252 109.5
876.268 114
878.283 112.25
880.296 119.25
882.31 120.75
884.322 119
886.335 118.5
888.345 117.25
890.356 106
892.367 117.5
894.376 106.5
896.386 115
898.395 117
900.402 108
902.409 105.25
904.417 108.5
906.423 115.5
908.429 110.75
910.434 109.5
912.438 112.75
914.442 111.5
916.445 113.5
918.448 112
920.451 111.75
922.452 109.25
924.453 113
926.454 107
928.454 103.25
930.454 111.75
932.451 106.5
934.45 109
936.448 109.5
938.445 106.75
940.441 107
942.437 108.25
944.433 105.25
946.427 99
948.422 99.25
950.415 106.5
952.408 103.75
954.4 100.75
956.393 104
958.383 98.75
960.374 101.75
962.365 91.5
964.354 97.25
966.342 104.25
968.332 100.25
970.319 97
972.306 94
974.293 89
976.279 91.25
978.265 88
980.25 90.75
982.234 96
984.218 86
986.202 81
988.184 92
990.166 81
992.147 87.5
994.128 83
996.109 81.5
998.089 89.75
1000.07 84.5
1002.05 79.5
1004.02 79.5
1006 82
1007.98 79
1009.96 78.25
1011.93 75.5
1013.91 77.5
1015.88 77
1017.86 80
1019.83 80
1021.8 82.25
1023.77 86.75
1025.75 76.25
1027.72 82.25
1029.69 78.75
1031.66 80
1033.63 75.5
1035.6 82.5
1037.57 81.5
1039.53 77
1041.5 76
1043.47 82.5
1045.43 81.25
1047.4 74.5
1049.36 81.75
1051.33 83.25
1053.29 75.75
1055.26 78
1057.22 74.5
1059.18 79.75
1061.14 76.5
1063.11 77.75
1065.06 76.75
1067.03 74.5
1068.98 84.75
1070.94 76.75
1072.9 72
1074.86 70
1076.82 72.5
1078.77 81
1080.73 76.25
1082.69 74.75
1084.64 76.5
1086.59 77.75
1088.55 78.5
1090.5 78
1092.45 76.75
1094.41 72.75
1096.36 69
1098.31 76.75
1100.26 75.5
1102.21 81
1104.16 76.25
1106.11 79.25
1108.06 77.25
1110 83
1111.95 79.25
1113.9 77.5
1115.84 77.25
1117.79 80
1119.73 81.5
1121.68 75
1123.62 73.25
1125.57 81
1127.51 83.25
1129.45 75.25
1131.39 81.25
1133.33 81.25
1135.27 79.5
1137.21 80.5
1139.15 87.75
1141.09 82
1143.03 85.75
1144.97 90
1146.9 83
1148.84 83.75
1150.78 85.75
1152.71 88
1154.65 77.5
1156.58 78
1158.52 86.5
1160.45 88
1162.38 90.5
1164.31 88.25
1166.25 88.25
1168.18 84.5
1170.11 87.5
1172.04 78.75
1173.97 85
1175.9 87.25
1177.83 85.75
1179.75 88.5
1181.68 81
1183.61 92
1185.53 89.25
1187.46 84.75
1189.38 88.5
1191.31 83
1193.23 81.5
1195.16 85.25
1197.08 83.25
1199 83
1200.92 85.25
1202.84 88
1204.76 83.75
1206.68 91.25
1208.6 87
1210.52 85.5
1212.44 86.5
1214.36 84.5
1216.28 82.25
1218.19 85
1220.11 90.75
1222.03 81.5
1223.94 81
1225.86 80
1227.77 77.5
1229.68 82
1231.6 78.5
1233.51 86.5
1235.42 79
1237.33 76.5
1239.24 74.75
1241.15 77.5
1243.06 77
1244.97 79
1246.88 73.25
1248.79 61.75
1250.7 72.75
1252.6 71.5
1254.51 70
1256.42 70.75
1258.32 67.75
1260.23 67.25
1262.13 66
1264.04 71.5
1265.94 67.25
1267.84 68.25
1269.74 66.5
1271.64 66.75
1273.55 66
1275.45 64
1277.35 67
1279.25 61.75
1281.14 64.5
1283.04 65
1284.94 62.75
1286.84 59.75
1288.74 64
1290.63 63.5
1292.53 59.75
1294.42 57
1296.32 60.75
1298.21 66.5
1300.11 55.5
1302 57
1303.89 58.75
1305.78 59
1307.67 64
1309.57 58.25
1311.46 60
1313.34 62.75
1315.23 59
1317.12 59
1319.01 58.5
1320.9 62
1322.79 59
1324.67 64.75
1326.56 63.5
1328.45 62.5
1330.33 60.25
1332.21 62.5
1334.1 61.25
1335.98 62.5
1337.86 60.5
1339.75 57.5
1341.63 62.5
1343.51 60.5
1345.39 61
1347.27 64.5
1349.15 60
1351.03 57.5
1352.91 62.75
1354.79 61
1356.66 60.25
1358.54 63.5
1360.42 56.75
1362.29 70
1364.17 64.5
1366.04 61
1367.92 59
1369.79 71.25
1371.67 62
1373.54 63.5
1375.41 62.75
1377.28 58.75
1379.15 63.25
1381.03 62.5
1382.9 60.5
1384.76 63.75
1386.63 67.75
1388.5 66
1390.37 62
1392.24 63.5
1394.11 63.5
1395.97 63
1397.84 71
1399.7 57.75
1401.57 66.5
1403.43 62.75
1405.3 66.5
1407.16 63.75
1409.02 60.5
1410.89 59.75
1412.75 57
1414.61 67.5
1416.47 64
1418.33 63.5
1420.19 62.25
1422.05 62.75
1423.91 65
1425.77 62.5
1427.62 63.25
1429.48 66.25
1431.34 58.75
1433.19 54.5
1435.05 57.75
1436.9 59
1438.76 61.5
1440.61 59
1442.47 59.75
1444.32 59.25
1446.17 59.25
1448.02 56.25
1449.87 59.75
1451.73 58.5
1453.58 55.25
1455.42 61.5
1457.27 61.25
1459.12 59
1460.97 62.5
1462.82 66
1464.67 59
1466.51 58.25
1468.36 55.75
1470.2 58
1472.05 61
1473.89 60.75
1475.74 61
1477.58 58
1479.42 58.25
1481.27 60.75
1483.11 56.25
1484.95 57.25
1486.79 60.5
1488.63 61.75
1490.47 62
1492.31 57.75
1494.15 61.25
1495.99 64.75
1497.83 63.75
1499.66 59.75
1501.5 56.5
1503.34 59
1505.17 61.75
1507.01 65.25
1508.84 64.75
1510.68 61.5
1512.51 67.75
1514.35 65
1516.18 61
1518.01 69.5
1519.84 66
1521.67 64.5
1523.5 68
1525.33 70.75
1527.16 65
1528.99 68
1530.82 73.5
1532.65 70.25
1534.48 68
1536.3 66.5
1538.13 67.25
1539.96 74
1541.78 70.5
1543.61 69.5
1545.43 67.25
1547.26 69
1549.08 67.5
1550.9 69.5
1552.73 71.25
1554.55 70.5
1556.37 76.25
1558.19 66
1560.01 75.5
1561.83 66
1563.65 71.5
1565.47 72.5
1567.29 73.5
1569.11 77.75
1570.92 72
1572.74 73.75
1574.56 70.25
1576.37 73
1578.19 70.25
1580 71
1581.82 72.25
1583.63 72.75
1585.45 75.75
1587.26 74.75
1589.07 71.25
1590.88 72.5
1592.69 70.5
1594.51 76.25
1596.32 69
1598.13 70.5
1599.94 73.75
1601.74 74.75
1603.55 72.75
1605.36 74.25
1607.17 69
1608.97 65.5
1610.78 69.5
1612.59 69
1614.39 67.75
1616.2 66.75
1618 68.5
1619.81 67.25
1621.61 69
1623.41 64.25
1625.21 71.75
1627.02 63.25
1628.82 60
1630.62 61
1632.42 62
1634.22 64.5
1636.02 61.5
1637.82 59
1639.61 71.25
1641.41 61.75
1643.21 56
1645.01 62.5
1646.8 57
1648.6 57.75
1650.39 55.5
1652.19 58.25
1653.98 58
1655.78 57.25
1657.57 52
1659.36 57
1661.16 56.25
1662.95 61.5
1664.74 63.75
1666.53 61
1668.32 52.5
1670.11 56.75
1671.9 55
1673.69 59
1675.48 53.25
1677.26 55
1679.05 58.75
1680.84 53
1682.63 52.5
1684.41 50.5
1686.2 52.75
1687.98 56.5
1689.77 53
1691.55 53
1693.33 52.5
1695.12 52
1696.9 50.25
1698.68 54.5
1700.46 54.75
1702.24 56.5
1704.02 54.5
1705.8 55.25
1707.58 57
1709.36 56.5
1711.14 50.5
1712.92 54.5
1714.7 58.25
1716.47 54.75
1718.25 48.5
1720.03 49.75
1721.8 56.5
1723.58 51.5
1725.35 53
1727.13 52.25
1728.9 47
1730.67 48.75
1732.44 57.5
1734.22 50
1735.99 52.5
1737.76 53
1739.53 49.75
1741.3 45.75
1743.07 50.75
1744.84 49.5
1746.61 50.5
1748.38 47.5
1750.14 48.75
1751.91 48.75
1753.68 49.5
1755.44 56.25
1757.21 49
1758.98 51
1760.74 47.75
1762.5 51
1764.27 50
1766.03 48.5
1767.79 52
1769.56 44.5
1771.32 52.75
1773.08 48
1774.84 51.75
1776.6 49.5
1778.36 50.5
1780.12 45.25
1781.88 51.25
1783.64 48
1785.4 51.25
1787.15 50.75
1788.91 50.5
1790.67 50.25
1792.42 47.5
1794.18 54.25
1795.93 45
1797.69 48.25
1799.44 47
1801.2 45.75
1802.95 51
1804.7 49.25
1806.46 45
1808.21 51.5
1809.96 47.75
1811.71 48
1813.46 49.75
1815.21 46.5
1816.96 47.25
1818.71 51.25
1820.46 52
1822.2 45.5
1823.95 49.5
1825.7 46.5
1827.44 47.25
1829.19 47.25
1830.94 49.5
1832.68 46.5
1834.42 50
1836.17 49.75
1837.91 52
1839.66 51.5
1841.4 50.75
1843.14 47.25
1844.88 53
1846.62 41.75
1848.36 46.5
1850.1 50
1851.84 47
1853.58 47.5
1855.32 47.5
1857.06 50.25
1858.8 52
1860.54 50.75
1862.27 50.25
1864.01 52.25
1865.74 48
1867.48 44.75
1869.22 51.5
1870.95 49.75
1872.68 46.5
1874.42 50.5
1876.15 52
1877.88 50.25
1879.61 50.25
1881.35 45
1883.08 52.5
1884.81 45
1886.54 42.5
1888.27 49.5
1890 50.25
1891.73 50.5
1893.45 48
1895.18 48.75
1896.91 45
1898.64 46
1900.36 52.75
1902.09 50.5
1903.81 50
1905.54 52
1907.26 49
1908.99 52
1910.71 45.25
1912.43 49.75
1914.16 51.75
1915.88 45.25
1917.6 46
1919.32 44
1921.04 44.75
1922.76 48
1924.48 45.25
1926.2 47
1927.92 41.5
1929.64 50.25
1931.36 47
1933.08 51.75
1934.79 48.25
1936.51 47.25
1938.23 47
1939.94 48.75
1941.66 54.25
1943.37 44.5
1945.08 49.25
1946.8 52.5
1948.51 48.5
1950.22 45.5
1951.94 47.75
1953.65 48.25
1955.36 49.75
1957.07 52.5
1958.78 47.5
1960.49 49.25
1962.2 47
1963.91 46.75
1965.62 47.75
1967.33 51.25
1969.03 55
1970.74 46.5
1972.45 46.5
1974.15 51.75
1975.86 47.5
1977.56 51.75
1979.27 49.25
1980.97 47.75
1982.68 48.5
1984.38 50
1986.08 46.75
1987.79 46.75
1989.49 48.25
1991.19 51.25
1992.89 56.5
1994.59 44.75
1996.29 48.5
1997.99 49.25
1999.69 47.25