#------------------------------------------------------------------------------ #$Date: 2018-04-12 12:43:50 +0300 (Thu, 12 Apr 2018) $ #$Revision: 432 $ #$URL: svn://172.16.1.111/rod/cif/3/50/02/3500213.rod $ #------------------------------------------------------------------------------ # # This file is available in the Raman Open Database (ROD), # http://solsa.crystallography.net/rod/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500213 loop_ _publ_author_name 'El Mendili, Y' _publ_section_title ; Raman spectrum of commercial aluminum carbide ; _journal_name_full 'Personal communication to ROD' _journal_year 2018 _chemical_compound_source 'commercial powder Chemos, 97% 12656-43-8' _chemical_formula_structural 'Al4 C3' _chemical_formula_sum 'C3 Al4' _chemical_name_mineral 'aluminum carbide' _space_group_IT_number 160 _symmetry_space_group_name_Hall 'P 3* -2' _symmetry_space_group_name_H-M 'R 3 m :R' _cell_angle_alpha 22.54 _cell_angle_beta 22.54 _cell_angle_gamma 22.54 _cell_formula_units_Z 1 _cell_length_a 8.52 _cell_length_b 8.52 _cell_length_c 8.52 _cod_original_formula_sum 'Al4 C3' _raman_determination_method experimental _[local]_chemical_compound_color yelow _[local]_chemical_compound_state Solid _raman_measurement_device.location ENSICAEN _raman_measurement_device.company 'Thermo Scientific' _raman_measurement_device.model DXR _raman_measurement_device.optics_type microscope _raman_measurement_device.microscope_system dispersive _raman_measurement_device.microscope_objective_magnification 20 _raman_measurement_device.microscope_numerical_aperture 0.25 _raman_measurement_device.excitation_laser_type other _raman_measurement_device.excitation_laser_wavelength 780 _raman_measurement_device.configuration simple _raman_measurement_device.resolution 4 _raman_measurement_device.power_on_sample 1 _raman_measurement_device.direction_polarization unoriented _raman_measurement_device.spot_size 1.3 _raman_measurement_device.diffraction_grating 900 _raman_measurement.environment Air _raman_measurement.environment_details ; The sample was measured in air. ; _raman_measurement.temperature 300 _raman_measurement.pressure 100 _raman_measurement.background_subtraction no _raman_measurement.background_subtraction_details ; No background subtraction method was applied. ; _raman_measurement.baseline_correction no _raman_measurement.baseline_correction_details ; No baseline correction method was applied. ; _raman_measurement.datetime_initiated 2018-03-20 _raman_measurement.integration_time 60 _rod_data_source.file Al4C3.rod _rod_data_source.block 3500020 _rod_database.code 3500213 loop_ _raman_complementary.id _raman_complementary.method 1 EDX loop_ _raman_measurement_device_calibration.id _raman_measurement_device_calibration.standard 1 neon_lamp loop_ _rod_related_entry.id _rod_related_entry.code _rod_related_entry.database _rod_related_entry.uri _rod_related_entry.description 1 2310414 COD http://www.crystallography.net/cod/2310414.html ; no XRD analysis data. ; loop_ _raman_spectrum.raman_shift _raman_spectrum.intensity 4.917182e+001 0.000000e+000 5.013597e+001 3.095841e-002 5.110012e+001 2.520921e-002 5.206428e+001 2.002770e-002 5.302843e+001 1.726327e-002 5.399258e+001 2.212425e-002 5.495674e+001 3.539907e-002 5.592089e+001 4.610620e-002 5.688504e+001 5.254477e-002 5.784920e+001 5.495100e-002 5.881335e+001 5.282236e-002 5.977750e+001 4.270959e-002 6.074165e+001 2.831548e-002 6.170581e+001 1.809957e-002 6.266996e+001 1.478214e-002 6.363412e+001 1.516785e-002 6.459827e+001 1.640257e-002 6.556242e+001 1.809344e-002 6.652657e+001 1.994786e-002 6.749073e+001 2.164979e-002 6.845488e+001 2.305253e-002 6.941904e+001 2.441664e-002 7.038319e+001 2.647632e-002 7.134734e+001 2.973489e-002 7.231149e+001 3.265139e-002 7.327565e+001 3.304853e-002 7.423980e+001 3.187301e-002 7.520395e+001 3.076652e-002 7.616811e+001 2.908162e-002 7.713226e+001 2.730227e-002 7.809641e+001 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